SCR技术制备半固态合金非枝晶组织形成机制

采用单辊搅拌冷却技术制备A2017半固态合金,对半固态合金非枝晶的形成及演变过程进行了研究.结果表明,随着合金熔体浇注温度的降低或者辊靴行腔高度的减小,半固态合金组织逐渐从粗大的枝晶转变为细小的等轴晶.从辊靴行腔入口到出口,靠近靴子面侧半固态合金组织依次为枝晶、退化枝晶和等轴晶,而靠近工作辊面侧合金组织主要为细小的等轴晶和球形晶.合金组织的演变过程为合金熔体首先在靴子和工作辊内表面凝固形核并长大成枝晶,在工作辊的剪切搅拌作用下,枝晶从辊靴表面破碎脱落进入熔体,在工作辊对高固相率半固态合金的剪切搅拌下,枝晶进一步发生断裂破碎最终形成细小的等轴晶和球形晶.     

单辊剪切/冷却工艺对LY11半固态合金组织的影响[

利用自行设计的单辊剪切/冷却(SCR)试验机对LY11合金进行了半固态凝固实验,研究了工艺条件对LY11半固态合金组织的影响.结果表明,辊-靴间隙宽度的适当范围为2～3 mm;浇注温度影响半固态合金坯料内部晶粒的大小与形状,浇注温度在730～750     

倾斜式冷却剪切流变对半固态合金组织的影响

倾斜式冷却剪切制备半固态合金过程中,合金组织逐渐由粗大的树枝晶向细小的球形晶演变,组织形成过程与枝晶的破碎以及整体爆发形核机制有关.倾角、冷却板长度、浇注温度、冷却板表面性质对合金组织具有很大的影响.倾斜式冷却剪切流变很好改善了1Cr18Ni9Ti不锈钢组织与常规铸造的Al-10Mg合金的羽毛晶组织.     

SCR工艺参数对A2017半固态合金组织的影响

采用自行设计的SCR实验机制备A2017半固态合金，研究了SCR工艺参数对A2017半固态合金组织的影响。实验结果表明，合金液浇注温度和轧辊冷却水流量共同影响辊靴间隙中半固态合金的固相率，降低浇注温度或者增大冷却水流量，辊靴间隙高固相率合金区间增长，晶粒尺寸变小；减小辊靴间隙或者提高轧辊转速提高合金层流剪切强度，利于枝晶破碎；增大出口半固态浆料冷却速率能有效抑制晶粒继续生长，保留其完整的非枝晶半固态组织。合金液浇注温度为760～780℃，辊靴间隙为4～6mm，轧辊冷却水流量200～300ml／s条件下，SCR技术可获得浆料状A2017半固态合金，凝固后坯料为均匀、细小的非枝晶等轴晶组织，晶粒大小在40～50μm之间，SCR技术是一种制备半固态加工坯料的理想方法。     

低压脉冲电流下AZ91D镁合金半固态组织形成机理研究

在不同凝固阶段合金的半固态组织和脉冲电流热效应的实验研究基础上,探讨了低压脉冲电流下AZ91D镁合金半固态组织的形成机制。结果表明:在合金的液相线以下开始脉冲放电,二次枝晶臂分离需要较长的时间,一次枝晶臂难以球化;从合金的液相线以上开始脉冲放电,不会析出粗大的枝晶,二次枝晶臂分离比较容易。脉冲电流降低了半固态合金的冷却速度,同时造成了合金熔体强烈的温度起伏;随着脉冲电压的增加,半固态合金的冷却速度逐渐减小,熔体的瞬时平均温升逐渐增加。初始形核率的提高和二次枝晶臂的根部熔断是低压脉冲电流下球状或颗粒状初生α-Mg形成的重要机制。     

新型倾斜板技术制备半固态铝合金坯料和浆料

采用自行设计的波浪型倾斜板,在斜板冷却条件下制备了组织和触变性能优良的半固态合金坯料。而在斜板加热条件下制备出了组织优良的半固态合金浆料。在采用波浪型的倾斜板制备半固态合金过程中,在熔体爆发形核与枝晶破碎的共同作用下,形成了细小球形的半固态合金组织,浇注温度、冷却强度、斜板倾角和斜板表面材质是影响半固态合金组织的主要因素。得出了本试验条件下制备AlMg3合金半固态坯料的浇注温度范围为660~690℃;制备AlSi6Mg2合金半固态坯料的浇注温度范围为660~680℃;制备AlSi6Mg2半固态合金浆料的合理工艺条件为:斜板预热温度为300℃时,合金浇注温度为680℃。     

倾斜式冷却剪切工艺条件对半固态合金组织的影响

采用自制的倾斜式冷却/剪切试验装置,对制备1Cr18Ni9Ti不锈钢与Al-Mg合金半固态坯料过程中,工艺条件对合金组织的影响进行了研究.结果表明,合金组织逐渐由粗大的树枝晶向细小的球形晶演变,组织形成过程与枝晶的破碎以及整体爆发形核机制有关.倾角、冷却板长度、浇注温度对合金组织具有重要影响.在本试验条件下,最佳倾角与冷却板长度为α=45°,L=650 mm,t=660～690 ℃为制备Al-Mg合金半固态坯料的最佳工艺参数.倾斜式冷却剪切流变显著改善了1Cr18Ni9Ti不锈钢组织与常规铸造的Al-10Mg合金的羽毛晶组织.     

EMS-DC法制备的半固态ZL101A铝合金的组织与性能

研究了EMS DC法工艺参数对半固态ZL1 0 1A合金组织的影响 ,阐明了浇注温度 (中间包温度 )、拉坯速度、冷却速度与合金组织形貌的关系。研究表明 :在 0 .0 8～ 0 .0 9T的磁感应强度作用下 ,当铝合金在固液两相区的冷却速度小于 0 .3℃ /s时 ,即能得到较理想的非树枝晶组织。在优化各工艺参数的基础上 ,形成了半固态ZL1 0 1A合金的水平半连续铸造中试生产技术 ,其连铸坯铸态和热处理态强塑性综合指标分别为 430 .4和 497.4。     

控制浇注A1-Si合金的半固态铸造

采用控制浇注方法在金属模中浇注A1-7Si-0.35Mg合金,研究浇注温度对材料半固态组织及其半固态成形性能的影响.随着浇注温度的降低(从725 ℃到625 ℃),原始铸造组织从粗大的树枝晶,转变为细小等轴晶,最后变为细小的菊状晶.原始铸造组织随后经部分重熔和580 ℃保温进行组织演化,最后进行半固态成形.采用较高浇注温度制备的坯料只充满一半铸模,并伴有严重的固液分离和其他铸造缺陷.而低浇注温度坯料能实现完全充填,而且无缺陷.半固态铸件的质量主要取决于成形时半固态浆料的组织,而这一组织又是取决于原始铸造组织和随后的重熔热处理.本文重点讨论浇注温度对原始铸造组织,重熔组织演化和最后半固态铸件质量的影响.试验结果表明,对于A1-Si-Mg合金,由625～650 ℃低温浇注形成坯料,加上适当的重熔保温处理,可以得到高质量的半固态铸件.     

倾斜式冷却剪切流变对Al-Mg合金组织的影响

倾斜式冷却剪切流变制备半固态Al-Mg合金过程中，合金在冷却板表面非均匀形核，并受到重力的剪切作用，合金组织逐渐从粗大等轴晶网络演化为细小的球形晶；在660—690℃浇注得到了细小球形的Al-1％Mg合金组织。倾斜式冷却剪切流变技术很好的改善了常规铸造高Mg铝合金中出现的羽毛晶组织，合金组织由粗大的羽毛晶向细小的球形晶转化。     

Microstructure formation mechanism and properties of AZ61 alloy processed by melt treatment with vibrating cooling slope and semisolid rolling

A melt treatment with a vibrating cooling slope and a semisolid rolling process to produce an AZ61 alloy strip was proposed. The microstructure formation mechanism and the properties of the AZ61 alloy produced by the proposed process were investigated. Due to the high cooling rate and stirring action caused by the vibration cooling slope, the nucleation rate was greatly improved, which caused the formation of fine spherical or rosette primary grains. During the rolling process, the solid fraction increased from the entrance to the exit of the roll gap, and under the shearing action of the roller, the distribution of solute in the melt was homogenous, and the primary grains grew further. When the casting temperature was 680 °C, a strip with a cross section of 4 mm×160 mm was produced and a homogeneous microstructure was obtained. The ultimate tensile strength of the AZ61 alloy strip produced by the proposed method reached 242 MPa, and the corresponding elongation to failure was 4%, which were better than those achieved in previous similar studies.     

ZK60-2Ca镁合金近液相线铸造研究

用近液相铸造方法制备了ZK60-2Ca半固态坯料。对其组织演变进行了研究,发现由于Zr的特殊细化作用,ZK60-2Ca合金直接获得球形或近球形的组织,无需经过枝晶球化过程。通过用不同冷却速率的铸模浇铸考察了冷却速率对铸造组织的影响,并对近液相铸造时静置时间对微观组织的影响进行了研究。结果表明,随浇铸温度的降低和静置时间延长至60 min,晶粒逐渐细化并趋于均匀,晶粒尺寸达21?m,且圆度为1.29。随冷却速率的增加,晶粒细化并出现球化趋势。并对组织演变的机理进行了探讨。     

Microstructure evolution and properties of Mg-3Sn-1Mn (wt%) alloy strip processed by semisolid rheo-rolling

The high cooling rate caused by the sloping plate and stirring action caused by the vibration and metal flow lead to a high nucleation rate as well as two primary grain growth patterns, direct globular growth as well as dendrite growth and subsequent breakage, which causes the formation of fine spherical or rosette primary grains. The change of the primary grain shape is not obvious in the roll gap. However, solid fraction increases from the entrance to the exit of the roll gap. The spherical or rosette grains were remained eventually. When the casting temperature is 670 °C, and the vibrating amplitude is 1.5 mm, the strip with a cross section of 4 mm×160 mm was produced. Homogeneous microstructure was obtained. Mechanical properties of the present product were higher than that of Mg-3Sn-1Mn (wt%) alloy casting with the addition of 0.87 wt% Ce.     

Deformation mechanism of tension of 2024Al alloy at semi-solid state

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半固态灰铸铁的制备与显微组织

建立了一种不需搅拌和其它附加处理的半固态灰铸铁制备技术 ,用浇注前合理调整熔体温度或调温 适当快冷的铸造方法 ,并配以合适的凝固冷却速度 ,成功地制备了球状初生奥氏体圆整、尺寸细小、分布均匀的半固态亚共晶灰铸铁 ,得到了最佳工艺条件 ,并用铸铁金相计算机辅助检测系统 ,对初生奥氏体的形状系数和等效直径进行了测量与统计分析 ,定量描述了半固态组织的特性     

Continuously extending extrusion forming of semisolid A2017 alloy by SRS process

A self-made single-roll stirring (SRS) machine was used to manufacture semisolid A2017 alloy, the mechanismof A2017 alloy formation was investigated. It was shown that A2017 dendrites growing on the rough roll surface arecrashed into fragments by the roll, which move and grow freely then contribute the formation of finer spherical microstruc-ture. When casting at 710-750 ℃, fine and homogeneous spherical or elliptical grains of A2017 alloy were obtained. Ex-tending forming mould has been designed and was installed at the exit of roll-shoe gap. A2017 alloy was formed by ex-tending continuously at the semisolid state on SRS machine. Through controlling pouring temperature, semisolid formingand extending extrusion was combined organically. A2017 product with fine surface and rectangular transection of 14mmx25 mm was obtained. By contrast to the national standard, the fracture strength and elongation of A2017 products pro-duced from extending semisolid extrusion have been improved with an increase of 100 MP     

Microstructure formation mechanism and properties of a Mg-3Sn-1Mn (wt%) magnesium alloy processed by a novel semisolid continuous shearing and rolling process

A novel semisolid Continuous Shearing and Rolling (CSR) process for producing a Mg-3Sn-1Mn (wt%) alloy strip is developed, and the microstructure formation mechanism and properties of the Mg-3Sn-1Mn (wt%) alloy processed by this process are investigated. At a casting temperature of 690°C and a roll speed of 0.052 m·s^?1, a Mg-3Sn-1Mn (wt%) alloy strip with a cross section size of 4×160 mm was produced by the proposed process. Under strong cooling and shearing actions, eruptive nucleation, direct globular grain growth and dendrite arm breakage took place during the process, which caused formations of fine spherical grains. The grain size and roundness of the Mg-3Sn-1Mn (wt%) alloy strip increased with increasing increments of the casting temperature. In this perspective, roll speed obviously affects grain shape. The ultimate tensile strength and elongation of the Mg-3Sn-1Mn (wt%) alloy strip reached 205.93 MPa and 7.2%.     

AlSi7Mg合金半固态压铸件热处理强化机理研究

对AlSi7Mg合金(A356)半固态压铸件和液态压铸件进行了不同工艺的固溶与时效热处理，分析了其显微组织与疏松度，测定了硬度、拉伸强度及延伸率等力学性能。实验得出，铝合金半固态压铸件原始态的力学性能优于液态压铸件，并且半固态压铸件时效强化效果尤其明显，拉伸强度可达330MPa以上，延伸率10％以上。这主要是由于半固态压铸件比液压件具有更加致密，且为球状的非树枝晶组织。铝合金半固态压铸件时效强化，机理主要归于弥散析出Mg2Si强化相。     

固溶后冷却方式对Inconel X-750合金组织和性能的影响

采用SEM、TEM、EDAX和相分析等分析手段,研究Inconel X-750合金固溶后不同冷却方式下组织和性能的变化。结果显示:水冷和油冷抑制合金中γ′相的析出,时效后均析出球形的γ′相。炉冷后合金中析出一次立方体形γ′相和二次球形γ′相,时效后再次析出球形γ′相;水冷和油冷后晶界上无碳化物析出,时效后晶界上均析出细小针状M₂₃C₆。炉冷后合金晶界上析出块状M₂₃C₆,时效后碳化物尺寸略微长大,形状基本不变;炉冷+时效后合金的强度最高,水冷+时效后合金的冲击性能最好。     

镁合金ZK60-RE半固态坯的微观组织演变

采用常规铸造法和等径道角挤压分别制备了镁合金ZK60-RE半固态坯;用金相显微镜研究了2种半固态坯料在等温热处理过程中的微观组织演变。结果表明：与传统铸造方法制备的半固态坯相比,采用等径道角挤压制备的半固态坯的晶粒细小、圆整,适合于半固态成形。在等温热处理过程中,2种坯料晶粒粗化的机制是合并长大和Ostwald长大。铸态坯料晶粒液相来源于非平衡凝固时在晶内产生的共晶组织,以及在随后的合并长大过程中晶粒所包裹的液相。随着保温时间的延长,铸态坯料的晶粒尺寸变化情况是：增大、减小然后又增大;而挤压态坯料的晶粒尺寸呈单一增大趋势。