Preparation and pool boiling characteristics of copper nanofluids over a flat plate heater

The copper nanoparticles of average size of 10 nm have been prepared by the sputtering method and characterized through atomic force microscopy (AFM), X-ray diffraction (XRD) and transmission electron microscopy (TEM). The pool boiling heat transfer characteristics of 0.25%, 0.5% and 1.0% by weight concentrations of copper nanoparticles has been studied. Different copper based nanofluids were prepared in both, distilled water and distilled water with 9.0 wt% of sodium lauryl sulphate anionic surfactant (SDS). The pool boiling heat transfer data were acquired for the boiling of nanofluids over a 30 mm square and 0.44 mm thick stainless steel plate heater. The experimental results show that for the critical heat flux of pure water is 80% higher than that of water–surfactant fluid. Also, it was found that the critical heat flux for 0.25%, 0.5% and 1.0% concentrations of copper nanoparticles in copper–water nanofluids are 25%, 40% and 48% higher than that of pure water. But in the case of copper–water with surfactant nanofluids comparing with pure water, the CHF decreases to 75%, 68%, and 62% for respective concentrations of copper nanoparticles. The heat transfer coefficient decreases with increase of nanoparticles concentration in both water–copper and water–copper with surfactant nanofluids.     

Stabilizer effect on CHF and boiling heat transfer coefficient of alumina/water nanofluids

We measured the critical heat flux (CHF) and boiling heat transfer coefficient (BHTC) of water-based Al₂O₃ (alumina) nanofluids. To elucidate the stabilizer effect on CHF and BHTC of alumina/water nanofluids, a polyvinyl alcohol (PVA) was used as a stabilizer. The plate copper heater (10 × 10 mm²) is used as the boiling surface and the concentration of alumina nanoparticle varies 0–0.1 vol.%. The results show that the BHTC of the nanofluids becomes lower than that of the base fluid as the concentration of nanoparticles increases while CHF of it becomes higher. It is found that the increase of CHF is directly proportional to the effective boiling surface area and the reduction of BHTC is mainly attributed to the blocking of the active nucleation cavity and the increase of the conduction resistance by the nanoparticle deposition on the boiling surface.     

Pool boiling heat transfer on the microheater surface with and without nanoparticles by pulse heating

We study the pool boiling heat transfer on the microheater surface with and without nanoparticles by pulse heating. Nanofluids are the mixture of de-ionized water and Al₂O₃ particles with 0.1%, 0.2%, 0.5% and 1.0% weight concentrations. The microheater is a platinum surface by 50 × 20 μm. Three types of bubble dynamics were identified. The first type of bubble dynamics is for the boiling in pure water, referring to a sharp microheater temperature increase once a new pulse cycle begins, followed by a continuous temperature increase during the pulse duration stage. Large bubble is observed on the microheater surface and it does not disappear during the pulse off stage. The second type of bubble dynamics is for the nanofluids with 0.1% and 0.2% weight concentrations. The microheater surface temperature has a sharp increase at the start of a new pulse cycle, followed by a slight decrease during the pulse duration stage. Miniature bubble has oscillation movement along the microheater length direction, and it disappears during the pulse off stage. The third type of bubble dynamics occurs at the nanofluid weight concentration of 0.5% and 1.0%. The bubble behavior is similar to that in pure water, but the microheater temperatures are much lower than that in pure water. A structural disjoining pressure causes the smaller contact area between the dry vapor and the heater surface, decreasing the surface tension effect and resulting in the easy departure of miniature bubbles for the 0.1% and 0.2% nanofluid weight concentrations. For the 0.5% weight concentration of nanofluids, coalescence of nanoparticles to form larger particles is responsible for the large bubble formation on the heater surface. The microlayer evaporation heat transfer and the heat transfer mechanisms during the bubble departure process account for the higher heat transfer coefficients for the 0.1% and 0.2% nanofluid weight concentrations. The shortened dry area between the bubble and the heater surface, and the additional thin nanofluid liquid film evaporation heat transfer, account for the higher heat transfer coefficient for the 0.5% nanofluid weight concentration, compared with the pure water runs.     

Sorption and agglutination phenomenon of nanofluids on a plain heating surface during pool boiling

The pool nucleate boiling heat transfer experiments of water (H₂O) based and alcohol (C₂H₅OH) based nanofluids and nanoparticles-suspensions on the plain heated copper surface were carried out. The study was focused on the sorption and agglutination phenomenon of nanofluids on a heated surface. The nanofluids consisted of the base liquid, the nanoparticles and the surfactant. The nanoparticles-suspensions consisted of the base liquid and nanoparticles. The both liquids of water and alcohol and both nanoparticles of CuO and SiO₂ were used. The surfactant was sodium dodecyl benzene sulphate (SDBS). The experimental results show that for nanofluids, the agglutination phenomenon occurred on the heated surface when the wall temperature was over 112 °C and steady nucleated boiling experiment could not be carried out. The reason was that an unsteady porous agglutination layer was formed on the heated surface. However, for nanoparticles-suspensions, no agglutination phenomenon occurred on the heating surface and the steady boiling could be carried out in the whole nucleate boiling region. For the both of alcohol based nanofluids and nano-suspensions, no agglutination phenomenon occurred on the heating surface and steady nucleate boiling experiment could be carried out in the whole nucleate boiling region whose wall temperature did not exceed 112 °C. The boiling heat transfer characteristics of the nanofluids and nanoparticles-suspensions are somewhat poor compared with that of the base fluids, since the decrease of the active nucleate cavities on the heating surface with a very thin nanoparticles sorption layer. The very thin nanoparticles sorption layer also caused a decrease in the solid–liquid contact angle on the heating surface which leaded to an increase of the critical heat flux (CHF).     

Effect of particle size on the convective heat transfer in nanofluid in the developing region

An experimental investigation on the convective heat transfer characteristics in the developing region of tube flow with constant heat flux is carried out with alumina–water nanofluids. The primary objective is to evaluate the effect of particle size on convective heat transfer in laminar developing region. Two particle sizes were used, one with average particle size off 45 nm and the other with 150 nm. It was observed that both nanofluids showed higher heat transfer characteristics than the base fluid and the nanofluid with 45 nm particles showed higher heat transfer coefficient than that with 150 nm particles. It was also observed that in the developing region, the heat transfer coefficients show higher enhancement than in the developed region. Based on the experimental results a correlation for heat transfer in the developing region has been proposed for the present range of nanofluids.     

Pool boiling characteristics of multiwalled carbon nanotube (CNT) based nanofluids over a flat plate heater

This paper is mainly concerned about the pool boiling heat transfer behavior of multi-walled carbon nanotubes (CNTs) suspension in pure water and water containing 9.0% by weight of sodium lauryl sulphate anionic surfactant (SDS). Three different concentrations of 0.25%, 0.5% and 1.0% by volume of CNT dispersed with water and water containing 9.0% by weight of sodium lauryl sulphate anionic surfactant (SDS) were prepared and boiling experiments were conducted over a stainless steel flat plate heater of size 30 mm² and 0.44 mm thickness. The test results exhibit that the addition of carbon nanotubes increases boiling heat transfer coefficients of the base fluids. At a given heat flux of 500 kW/m², the enhancement of heat transfer coefficient was found to be 1.5, 2.6 and 3.0 times of water corresponding to 0.25%, 0.5% and 1.0% concentration of CNT by volume in water, respectively. In water–CNT–surfactant nanofluid, it was found that 0.5% of CNT concentration gives the highest enhancement of 1.7 compared with water. In both water and water–surfactant base fluids, it was observed that the enhancement factor for 0.25% of CNT first increases up to the heat flux of 66 kW/m² and then decreases for higher heat fluxes. Further, the overall heat transfer coefficient enhancement in the water–CNT nanofluids is approximately two times higher than that in the water–CNT–surfactant nanofluids. With increasing heat flux, however, the enhancement was concealed due to vigorous bubble generation for both water–CNT and water–CNT–surfactant nanofluids. Foaming was also observed over the liquid-free surface in water–CNT–surfactant nanofluids during the investigation. No fouling over the test-section surface was observed after experimentation.     

Experimental study on condensation heat transfer inside a single circular minichannel

The measurement of the condensation heat transfer coefficient inside micro- and minichannels is still somewhat elusive due to the difficult task of getting accurate values of the heat transfer coefficients during the condensation process, particularly when studied within single minichannels. The present paper reports local heat transfer coefficients obtained from the measurement of the local heat flux and the direct measurement of the saturation and wall temperatures during condensation of R134a and R32 within a single circular 0.96 mm diameter minichannel. Except for the lowest mass velocity, the test results do not show significant discrepancy from the trends expected for macroscale tubes.     

Surface effects of ribbon heaters on critical heat flux in nanofluid pool boiling

This paper deals with a study of enhanced critical heat flux (CHF) and burnout heat flux (BHF) in pool boiling of water with suspended silica nanoparticles using Nichrome wires and ribbons. Previously the current authors and other researchers have reported three-digit percentage increase in critical heat flux in silica nanofluids. This study investigates the effect of various heater surface dimensions, cross-sectional shapes as well as surface modifications on pool boiling heat transfer characteristics of water and water-based nanofluids. Our data suggest that the CHF and BHF decrease as heater surface area increases. For concentrations from 0.1 vol% to 2 vol%, the deposition of the particles on the wire allows high heat transfer through inter-agglomerate pores, resulting in a nearly 3-fold increase in burnout heat flux at very low concentrations. The nanoparticle deposition plays a major role through variation in porosity. The CHF enhancement is non-monotonic with respect to concentration. As the concentration is increased, the CHF and BHF decrease prior to increasing again at higher concentrations. Results show a maximum of 270% CHF enhancement for ribbon-type heaters. The surface morphology of the heater was investigated using SEM and EDS analyses, and it was inferred that the 2 vol% concentration deposition coating had higher porosity and rate of deposition compared with 0.2 vol% case.     

Experimental investigation of oxide nanofluids laminar flow convective heat transfer

In the present investigation nanofluids containing CuO and Al₂O₃ oxide nanoparticles in water as base fluid in different concentrations produced and the laminar flow convective heat transfer through circular tube with constant wall temperature boundary condition were examined. The experimental results emphasize that the single phase correlation with nanofluids properties (Homogeneous Model) is not able to predict heat transfer coefficient enhancement of nanofluids. The comparison between experimental results obtained for CuO / water and Al₂O₃ / water nanofluids indicates that heat transfer coefficient ratios for nanofluid to homogeneous model in low concentration are close to each other but by increasing the volume fraction, higher heat transfer enhancement for Al₂O₃ / water can be observed.     

Estimation local convective boiling heat transfer coefficient in mini channel

The aim of this paper is to present an inverse heat conduction method used for determining the local convective boiling heat transfer coefficient in mini channel for pure water, copper nanofluid with using three different concentrations of nanoparticles: 5 mg/L, 10 mg/L and 50 mg/L. Sequential specification function method is used to solve the IHCP and estimate the space-variable convective heat transfer coefficient. The uncertainties in the estimated in heat transfer coefficient are calculated using Bias and Variance errors. The technique is used in a series of numerical experiments to provide the optimum experimental design for a boiling heat transfer investigation.     

Experimental investigation of the effect of particle deposition on pool boiling of nanofluids

Research on pool boiling of nanofluids has shown contradicting trends in the heat transfer coefficient (HTC). Such trends have been attributed, in part, to nanoparticle deposition on the heater surface. An experimental investigation of the transient nature of nanoparticle deposition and its effect on the HTC of pool boiling of nanofluids at various concentrations has been carried out. Pool boiling experiments have been conducted on a horizontal flat copper surface for alumina (40–50 nm) water based nanofluids at concentrations of 0.01, 0.1 and 0.5 vol.%. Nanofluids boiling experiments have been followed by pure water boiling experiments on the same nanoparticle-deposited (NPD) surfaces. This technique has been employed in order to separate the effect of nanoparticle deposition from the effect of nanofluids properties on the HTC. Contrary to what was expected, boiling of pure water on the NPD surface produced using the highest concentration nanofluid resulted in the highest HTC. A closer look at the nature of the NPD surfaces explained such trend. A new approach using a transient surface factor in Rohsenow correlation has been proposed to account for the transient nature of nanoparticle deposition. The applicability of such approach at different concentrations has been investigated.     

Thermo-physical properties of water based SiC nanofluids for heat transfer applications

The aim of current paper consists in the fabrication, characterization and preparation of water based on SiC nanofluids and the experimental investigation of their thermo-physical properties. Thermal conductivity, viscosity and surface tension of SiC/water nanofluids were measured for two two weight concentrations of nanoparticles 0.5 and 1.0 wt% respectively, within the range 20 °C to 50 °C. Concerning the thermal-properties of studied nanofluids, the experimental results show that the thermal conductivity increases with the increasing both of the weight concentration of the nanoparticles and temperature. Also, the dynamic viscosity of the SiC/water nanofluids increases with increasing nanoparticles concentration and decreases with the increasing temperature. Furthermore, the surface tension of studied nanofluids increases with the increase of the weight concentrations of the nanoparticles, but the results show that at a concentration of the nanoparticles of 0.5 wt%, the surface tension was lower than the surface tension of the water, while at 1.0 wt% nanoparticles, the surface tension of the nanofluids was close to the surface tension of the water. Measurements were compared with experimental data available in literature and theoretical models. Finally, SiC/water nanofluids were used as working fluid inside of the two-phase closed thermosyphon in order to study of the heat transfer from point of view both of operating temperature and the nanoparticles concentration.     

Pool boiling characteristics of nanofluid on flat plate based on heater surface analysis

Nucleate pool boiling of Al₂O₃ based aqueous nanofluid on flat plate heater has been studied experimentally. For boiling of nanofluid (< 0.1 vol.%) on heating surface with ratio of average surface roughness to average diameter of particles much less than unity when boiling continue to CHF, the heat transfer coefficient of nanofluid boiling reduces while critical heat flux (CHF) increases. CHF enhancement increased with volume fraction of nanoparticles. Atomic force microscope (AFM) images from boiling surface showed that after boiling of nanofluid the surface roughness increases or decreases depending on initial condition of heater surface. Changes in boiling surface topology during different regions of boiling, wettability and thermal resistance of heater surface owing to nanoparticles deposition cause to variations in nanofluids boiling performance.     

Pool boiling characteristics of low concentration nanofluids

The pool boiling behavior of low concentration nanofluids (?1 g/l) was experimentally studied over a flat heater at 1 atm. Boiling of nanofluids produces a thin nanoparticle film, on the heater surface, which in turn is believed to increase the critical heat flux. The present study also indicates that the nanoparticle deposition results in transient characteristics in the nucleate boiling heat transfer. Finally, this study investigates possible causes responsible for the deposition of nanoparticle on the heater surface. Experimental evidence shows that microlayer evaporation, during nanofluid boiling, is responsible for the nanoparticle coating formed on the heater surfaces.     

Heat transfer characteristics in double tube helical heat exchangers using nanofluids

In the present work a three-dimensional analysis is used to study the heat transfer characteristics of a double-tube helical heat exchangers using nanofluids under laminar flow conditions. CuO and TiO₂ nanoparticles with diameters of 24 nm dispersed in water with volume concentrations of 0.5–3 vol.% are used as the working fluid. The mass flow rate of the nanofluid from the inner tube was kept and the mass flow rate of the water from the annulus was set at either half, full, or double the value. The variations of the nanofluids and water temperatures, heat transfer rates and heat transfer coefficients along inner and outer tubes are shown in the paper. Effects of nanoparticles concentration level and of the Dean number on the heat transfer rates and heat transfer coefficients are presented. The results show that for 2% CuO nanoparticles in water and same mass flow rate in inner tube and annulus, the heat transfer rate of the nanofluid was approximately 14% greater than of pure water and the heat transfer rate of water from annulus than through the inner tube flowing nanofluids was approximately 19% greater than for the case which through the inner and outer tubes flow water. The results also show that the convective heat transfer coefficients of the nanofluids and water increased with increasing of the mass flow rate and with the Dean number. The results have been validated by comparison of simulations with the data computed by empirical equations.     

Effect of open microchannel geometry on pool boiling enhancement

Pool boiling enhancement through surface modification has garnered the attention of many researchers for extending the limits of heat flux dissipation. Simulated copper chips were used in a pool boiling setup with water boiling at atmospheric pressure. Heat transfer performance of different microchanneled surfaces was compared to that of a plain surface. The results of the study showed that the mechanism at work for the bubble dynamics was the ability of the surface to pull liquid through the channels to induce heat transfer. Geometrical trends were observed from the study as well with the wider and deeper channels and thinner finned surfaces showing the best heat transfer results. Without reaching the critical heat flux condition, the best performing chip dissipated a heat flux of 244 W/cm² corresponding to a record heat transfer coefficient of 269 kW/m² K.     

Boiling time effect on CHF enhancement in pool boiling of nanofluids

Using TiO₂–water nanofluids as the test liquid, pool boiling experiments were carried out to investigate the dependence of the nucleate boiling heat transfer, surface wettability and critical heat flux (CHF) on the boiling time in nanofluids. In the experiments performed at sufficiently high nanoparticle concentrations, the boiling heat transfer first degraded, then improved, and finally reached an equilibrium state. It was hence supposed that the present nanofluids had competing effects to deteriorate and enhance the nucleate boiling heat transfer. As for the surface wettability and CHF, the static contact angle asymptotically decreased whilst the CHF asymptotically increased with an increase in the boiling time. The maximum CHF enhancement measured in the present experiments was 91%, and strong correlation was found between the contact angle and the CHF. Although the boiling time needed to achieve the maximum CHF enhancement was less than a minute at high particle concentrations, a longer time of the order of 1 h was necessary at the lowest particle concentration tested in this work. This experimental result indicated that sufficient attention should be paid to the boiling time effect particularly in industrial applications of nanofluids to emergency cooling.     

Comparison study of liquid replenishing impacts on critical heat flux and heat transfer coefficient of nucleate pool boiling on multiscale modulated porous structures

The critical heat flux (CHF) and heat transfer coefficient of de-ionized (DI) water pool boiling have been experimentally studied on a plain surface, one uniform thick porous structure, two modulated porous structures and two hybrid modulated porous structures. The modulated porous structure design has a porous base of 0.55 mm thick with four 3 mm diameter porous pillars of 3.6 mm high on the top of the base. The microparticle size combinations of porous base and porous pillars are uniform 250 μm, uniform 400 μm, 250 μm for base and 400 μm for pillars, and 400 μm for base and 250 μm for pillars. Both the CHF and heat transfer coefficient are significantly improved by the modulated porous. The boiling curves for different kinds of porous structures and a plain surface are compared and analyzed. Hydrodynamic instability for the two-phase change heat transfer has been delayed by the porous pillars which dramatically enhances the CHF. The highest pool boiling heat flux occurring on the modulated porous structures has a value of 450 W/cm², over three times of the CHF on a plain surface. Additionally, the highest heat transfer coefficient also reaches a value of 20 W/cm² K, three times of that on a plain copper surface. The study also demonstrates that the horizontal liquid replenishing is equally important as the vertical liquid replenishing for the enhancement of heat transfer coefficient and CHF improvement in nucleate pool boiling.     

Entropy generation due to flow and heat transfer in nanofluids

Present study provides a theoretical investigation of the entropy generation analysis due to flow and heat transfer in nanofluids. For this purpose, the most common alumina–water nanofluids are considered as the model fluid. Since entropy is sensitive to diameter, three different diameters of tube in their different regimes have been taken. Those are microchannel (0.1 mm), minichannel (1 mm) and conventional channel (10 mm). To consider the effect of conductivity and viscosity, two different models have been used to represent theoretical and experimental values. It has been found that the reduced equation with the help of order of magnitude analysis predicts microchannel and conventional channel entropy generation behaviour of nanofluids very well. The alumina–water with high viscosity nanofluids are better coolant for use in minichannels and conventional channels with laminar flow and microchannels and minichannel with turbulent flow. It is not advisable to use alumina–water nanofluids with high viscosity in microchannels with laminar flow or minichannels and conventional channels with turbulent flow. Also there is need to develop low viscosity alumina–water nanofluids for use in microchannel with laminar flow. It is observed that at lower tube diameter, flow friction irreversibility is more significant and at higher tube diameter thermal irreversibility is more. Finally, for both laminar and turbulent flow, there is an optimum diameter at which the entropy generation rate is the minimum for a given nanofluid.     

Nanofluid stabilizes and enhances convective boiling heat transfer in a single microchannel

The flow boiling heat transfer in a single microchannel was investigated with pure water and nanofluid as the working fluids. The microchannel had a size of 7500 × 100 × 250 μm, which was formed by two pyrex glasses and a silicon wafer. A platinum film with a length of 3500 μm and a width of 80 μm was deposited at the bottom channel surface, acting as the heater and temperature sensor. The nanofluid had a low weight concentration of 0.2%, consisting of de-ionized water and 40 nm Al₂O₃ nanoparticles. The nanoparticle deposition phenomenon was not observed. The boiling flow displays chaotic behavior due to the random bubble coalescence and breakup in the milliseconds timescale at moderate heat fluxes for pure water. The flow instability with large oscillation amplitudes and long cycle periods was observed with further increases in heat fluxes. The flow patterns are switched between the elongated bubbles and isolated miniature bubbles in the timescale of 100 s. It is found that nanofluid significantly mitigate the flow instability without nanoparticle deposition effect. The boiling flow is always stable or quasi-stable with significantly reduced pressure drop and enhanced heat transfer. Miniature bubbles are the major flow pattern in the microchannel. Elongated bubbles temporarily appear in the milliseconds timescale but isolated miniature bubbles will occupy the channel shortly. The decreased surface tension force acting on the bubble accounts for the smaller bubble size before the bubble departure. The inhibition of the dry patch development by the structural disjoining pressure, and the enlarged percentage of liquid film evaporation heat transfer region with nanoparticles, may account for the heat transfer enhancement compared to pure water.