激光加工工艺参数对Al2O3陶瓷坯体成形性能的影响

研究了激光加工工艺参数对Al2O3陶瓷坯体成形性能的影响,利用正交试验分析法确定了其对成型性能的主要影响因素.结果表明:扫描速度、激光功率、成分配比、扫描间隔和气体压强对Al2O3陶瓷坯体成形性能的影响程度依次减小,最佳工艺参数优化结果为扫描速度25 mm/s、激光功率12mA、配比35v01％、扫描间隔0.1mm和气体压强0.4 MPa.     

工程陶瓷注射成型的研究与发展

综述了陶瓷注射成型目前的发展状况以及该成型方法的优点。详细论述了陶瓷粉体性质、有机载体组成特别是表面活性剂对于陶瓷喂料和注射成型所成坯体性质的影响。分析了混炼顺序、注射工艺参数、脱脂对陶瓷喂料的流变性以及所成型坯体性质的影响。     

陶瓷注射成型超临界CO2脱脂过程坯体孔洞结构分布

利用压汞仪、扫描电镜对陶瓷注射成型超临界CO2脱脂过程中不同阶段坯体孔洞结构和分布进行分析,研究陶瓷注射成型超临界流体脱脂行为和脱脂的动力学过程.结果显示随着脱脂时间的增加,陶瓷坯体中孔径和孔体积增大,孔尺寸分布明显拓宽.脱脂过程是由坯体表面不断深入到坯体内部,溶解和扩散是脱脂过程的两个关键因素.     

Fe-Ni-Cu-C合金粗粉注射成型工艺参数的优化

采用正交试验法研究了注射压力、注射温度、注射速度及其交互作用对注射成型坯质量的影响,评价了各参数对生坯质量影响的显著程度,优化了注射成型参数.试验结果表明,注射压力、注射温度、注射速度及注射压力与注射温度的交互作用对生坯抗弯强度影响显著,注射压力、注射温度及注射温度与注射速度的交互作用对生坯密度影响显著.注射压力增加,生坯密度和抗弯强度都增大;注射温度提高,生坯密度降低,注射温度在155～160 ℃之间时,生坯抗弯强度变化不大,超过160 ℃时抗弯强度明显降低.注射速度为60%时,生坯密度达到最大值.最佳注射成型工艺参数为:注射压力8 MPa,注射温度155 ℃,注射速度60%.     

陶瓷注射成型超临界CO2流体脱脂工艺研究

利用超临界CO2流体萃取技术从陶瓷注射成型坯体中萃取有机粘合剂。对陶瓷注射成型中所使用的有机载体组分进行研究,对陶瓷注射成型超临界CO2流体脱脂的工艺条件进行了探索,研究了不同萃取压力,温度及时间对萃取率和陶瓷坯体脱脂质量的影响。结果显示利用40％～50％(质量分数,下同)非极性分子有机物石蜡(PW)与30％～40％极性分子有机物聚丙烯(PP)及20％硬脂酸(SA)组成陶瓷注射成型熔体中的有机载体,在压力P=30MPa,温度T=58℃的超临界CO2流体中脱脂可在较短的时间内获得无缺陷的陶瓷注射成型生坯。     

ZrO_2陶瓷平面磨削力仿真分析与实验研究

研究工程陶瓷磨削参数对磨削力的影响,参数有金刚石砂轮线速度、磨削深度及工件进给速度,提高陶瓷加工效率和加工精度。以金刚石砂轮平面磨削ZrO_2陶瓷为例,通过正交实验法设计多组关于金刚石砂轮线速度、磨削深度和工件进给速度的磨削组合参数,利用平面测力仪测量不同磨削参数下的磨削力。同时,运用ABAQUS建立单颗金刚石磨粒磨削ZrO_2陶瓷的有限元模型,分析磨粒磨削陶瓷过程,将实验结果与仿真结果进行对比分析。金刚石砂轮线速度由30m/s增大到50m/s时,磨削力逐渐减小;平面磨削深度由5μm增大到15μm,磨削力逐渐增大;工件随着进给速度的增加,磨削力逐渐增大;实验结果与仿真结果基本一致。影响法向磨削力最大的因素是磨削深度,当平面磨削深度增大,法向磨削力也随之增大;砂轮线速度对切向磨削力的影响最大,随着线速度的增大,切向磨削力增大。研究结果对于提高工程陶瓷加工效率,改进加工质量具有重要的促进作用。     

高可靠性陶瓷部件胶态注射成型关键技术及装备

结合注射成型和凝胶注模成型技术的优点,发明了陶瓷胶态注射成型技术,实现了水基非塑性浆料的注射成型,并研制了胶态注射成型机,实现了浆料先分储后混合,能连续化自动注射成型.结果表明:通过调节工艺中的各项参数和添加适当的助剂,可以实现陶瓷浆料的可控固化;加入应力缓释剂调节高分子网络结构,能有效降低坯体中的内应力,制备出大尺寸陶瓷部件;利用胶态注射成型技术与设备,不仅能实现规模化大批量生产,而且产品具有较高的可靠性,具有广阔的应用前景.     

工艺参数对42CrMo钢激光淬火效果的影响

对42CrMo钢进行不同参数下的激光淬火处理,研究了激光淬火功率和扫描速度对42CrMo钢表面淬火硬度和淬火深度的影响规律,分析了在激光功率密度为定值时不同激光淬火参数下硬化性能的变化趋势。研究结果表明,激光功率的增大和扫描速度的减小均可以提高淬火层的深度和硬度;结合激光功率和扫描速度计算所得的能量密度参数与淬火效果存在较强相关性,在能量密度相同时,高功率高速度参数可以增加淬火硬度和深度,并提高加工效率。     

高性能氧化物陶瓷材料的注射成型

系统研究了高纯超细3Y-ZrO2和Al2O3陶瓷粉末的注射成型技术.主要研究了高纯超细3Y-ZrO2和Al2O3粉末,与有机载体混炼后的流变性,获得适于注射成型的悬浮体;注射成型的陶瓷的素坯特性.分析测试了脱脂烧结后3Y-ZrO2和Al2O3陶瓷体的体积密度,显微结构特征,抗弯强度等性能.并采用注射成型技术成功的制备出表面光洁、尺寸精确的光纤连接器陶瓷套筒、生物陶瓷牙桩、陶瓷刀片等高性能精密陶瓷部件.     

特厚板坯结晶器内液面波动的水模拟实验研究

以武重特厚板坯连铸结晶器为研究对象,采用1：1模型进行水模拟实验,引入新型点阵激光浪高测试系统,研究了拉坯速度、浸入式水口插入深度对结晶器液面波动的影响。实验结果表明：在相同插入深度下增加拉坯速度或相同拉坯速度下减小插入深度都会使液面波动增大,此次实验中拉速较插入深度对液面波动拥有更明显的影响。为更好的控制铸坯质量,在现有工况参数下建议使用0.2 m/min拉速和200 mm水口插入深度。     

磁电机轴套加工工艺探讨

本文对磁电机轴套的精铸成形加工工艺和摆辗成形加工工艺进行了分析,通过这两种工艺可以达到提高材料利用率,减少切削加工的目的.这两种加工技术生产效率更高,加工表面质量好,性价比高,符合现代绿色加工的发展趋势.     

Micro machining of pre-sintered ceramic green body

Ceramic materials are widely used in industrial products because of their excellent properties such as resistance to erosion, high temperature and wear. Those properties pose difficulty in processing ceramic materials to desired shapes and dimensions, especially in micro machining of ceramics using micro tools because of the low mechanical strength of tiny tools and the extreme hardness of ceramics. The machining of ceramic green body may be a solution to the problem. However, the low strength of ceramic green body results in low machining accuracy such as damage at the edges of micro features. In this paper, the pre-sintering of ceramic materials was used to enhance the material strength, and hence to improve the machining accuracy. Microstructures of pre-sintered ceramic green bodies at different temperatures were observed and analyzed. The mechanical strength of pre-sintered ceramics was measured. It was confirmed that the mechanical strength of ceramics increased with an increase of pre-sintering temperature. There was no obvious shrinkage after pre-sintering at below 850 °C. The edge damage of machined micro features was reduced significantly. The tool wear increased with the increase of pre-sintering temperature. Finally, a 3D micro feature was machined and the fully sintering shrinkage was compensated accurately.     

Low temperature processing of dense nanocrystalline yttrium-doped cerium oxide ceramics

Nanocrystalline cerium oxide ceramics of high homogeneity and nearly full density were prepared. The starting material was synthesized by the direct homogeneous precipitation method using hexamethylenetetramine (HMT). Two alternative routes for consolidation into green bodies were employed: (i) centrifugal casting of an electrostatically stabilized colloidal solution and (ii) cold isostatic pressing of dried ceria powder. The green bodies were sintered at temperatures between 700 and 1000°C. The sinter activities of both nanocrystalline materials were strongly enhanced if compared to microcrystalline ceria. Green bodies, which were generated by colloidal processing exhibited the highest sinter activities, associated with a unique pore structure. The effect of yttrium doping on the grain size after sintering at high temperatures was also investigated. The combination of yttrium doping and colloidal processing allowed for the synthesis of dense nanocrystalline cerium oxide ceramics by pressureless sintering.     

AZ91D镁合金半固态浆料制备的研究

采用AZ91D镁合金为试验原料，用自行研制的新型半固态浆料设备及直接流变成形装置为试验设备，研究不同温度、剪切速率下半固态组织的变化规律，并与常规铸造组织相比较。研究表明：适量提高剪切速率或降低温度，半固态组织的固相颗粒会变得细小、均匀和圆整。同时，对新型装置制备半固态组织的机理进行了研究。     

Laser machining of WC-Co green compacts for cutting tools manufacturing

Nowadays, conventional machining of WC-Co green compacts is used in industries in order to achieve desired dimensions, complex geometries and good surface quality. However, conventional machining presents some problems, namely tool wear, tool breakage, chatter, vibration and deflection besides mechanically induced damage to the compact. Laser machining is a promising approach to machine WC-Co green compacts, since it is performed without contact and allows great flexibility for producing several geometries, high material removal rate, good surface quality and precision, also for complex shapes. It also allows the production of details smaller than 0.2 mm, hardly manufactured by conventional machining, due to the brittle nature of cutting tools of very small dimensions. Due to the abovementioned reasons, laser machining presents a great potential for lowering the production costs of cemented carbide tools.This work addresses the laser machining of WC-Co green compacts, using a Nd:YAG laser and performing different strategies and combinations of laser parameters to obtain different types of profiles (grooves, areas and specific geometries).Results showed that an effective laser machining of WC-Co green compacts is attained when using laser power of 3 W, scan speed of 128 mm/s, 8 passages and line spacing of 0.08 mm. These parameters were effective for obtaining around 800 μm depth geometries, where the addition of a finishing step (1.5 W, 256 mm/s and 8 passages) improved the quality of the edge of the machined geometry. The laser machined compacts were sintered using a SinterHIP process and no undesirable phases were detected, as eta-phase or graphite.     

退火温度对离心铸造轧辊用高速钢材料组织和硬度的影响

采用四种不同的退火温度对离心铸造轧辊用高速钢材料进行退火热处理,并利用显微金相、SEM和硬度测试等方法对铸态和退火态离心铸造轧辊用高速钢材料进行检测分析.结果表明离心铸造轧辊用高速钢材料的退火温度为640℃时,组织接近平衡状态,为进一步的淬火热处理做好了准备,同时硬度大幅下降,改善了切削加工性能.     

SOEC电解质与氢电极的流延制备、共烧结及性能

采用流延成型技术同时制备致密固体电解质与多孔阳极半电池坯体,然后采用共烧结技术烧结出半电池.系统地研究了8YSZ陶瓷浆料与氢电极NiO/YSZ浆料的流变学特性.通过DTA和TG曲线确定了半电池的排胶工艺.用扫描电镜观察了半电池的显微结构.在800、850和900 ℃下测试了电池电解性能曲线,且在850、900和950 ℃电解模式下测试了电解质的欧姆阻抗.     

激光切割机用横梁的无模铸造工艺优化设计研究

激光切割机作为现代机械加工中重要的特种加工设备,其Y轴横梁结构复杂,制造难度大。为避免横梁结构砂铸过程中出现气孔、缩松、浇不足等缺陷,设计了双侧底注式浇注系统。结果表明,采用无模铸造成形技术设计了铸造型芯,采用Procast软件仿真优化了浇冒口工艺,最终确定了激光切割机横梁的铸造工艺方案。     

微量硼对铂的组织和性能影响

采用真空熔铸法制备不同硼含量铸锭,并加工成不同丝径的样品,利用光学显微镜、扫描电镜、电子拉力试验机等分析手段对其物理性能和微观结构进行了研究。结果表明,硼在铂中形成间隙固溶体,铂的晶格常数增大,产生晶格畸变,阻碍位错移动,铂的强度得到明显强化,硼与铂形成合金后,使铂的晶粒得到细化,硼在铂中起到强化作用的同时也使铂的脆性增加。     

Aqueous tape casting of PMN-PT powder prepared by the partial oxalate route

Aqueous tape casting of PMN-PT powder, prepared by the partial oxalate route, using PVA and glycerol as a binder and a plasticizer has been studied. The amount of PVA and glycerol required for forming green tape with good strength and flexibility has been optimized. The tape cast PMN-PT sintered to near theoretical density (>99% TD) at lower temperature (1200 °C) are compared to the samples prepared by uni-axial pressing (1270 °C). Flat PMN-PT tapes with good surface finish could be prepared by binder removal and sintering of the green tapes. The piezoelectric properties of the sintered tapes are comparable to that of PMN-PT ceramics reported in literature.