DE-AIRING AS CORRECTIVE IN DRYING1

The physics of mechanical removal of water from clay involves character of pores, adsorption capillarity and it also involves air filled cavities. Theory of clay particle system when plastic is set forth and argument is made for the effect of air on water removal and on drying shrinkage.     

Using acoustic emission to quantify damage in restrained fiber-reinforced cement mortars

This paper describes the use of acoustic emission (AE) for monitoring early-age cracking in restrained fiber-reinforced mortars. A steel-testing frame was used to prevent the length reduction associated with drying. AE sensors placed on both unrestrained and restrained specimens detected a high degree of activity that may be attributed to surface microcracking caused by moisture gradients that cause the surface to shrink more rapidly than the core. It was found that as the concrete neared the age of visible cracking, the acoustic waves generated in the restrained specimens had a greater amplitude and duration. For this reason, acoustic energy was utilized for these investigations. An increase in acoustic energy was detected before cracks were observed in the restrained specimens. It is believed that the role of fiber reinforcement is twofold. First, fibers arrest cracks thereby preventing unstable crack propagation, and second, they restrain the crack from opening preventing the cracking from becoming visible until a later age.     

Optimization of Radiant-Convective Drying of a Porous Medium by Design of Experiment Methodology

The major aim of this study was to improve tools to optimize the thermal drying of a porous medium. This article was devoted to the study of the radiant-convective drying of a material (cellular concrete) while respecting some thermal constraints. A numerical program had been previously developed and experimentally validated to model the thermal and hygroscopic behavior of the product. Design of experiments methodology (DOE) was used to obtain a behavioral reduced model that allows the operating optimums to be calculated quickly. Three characteristics of a drying operation were analyzed using response surface methodology: the drying time, the total energy used in the process, and the specific moisture extraction rate. The effects of all the drying parameters (initial moisture content, infrared power, air temperature, velocity, and humidity) were studied. The optimal conditions were determined for convective and infrared-convective drying.     

Investigation of Strut Crack Formation in Open Cell Alumina Ceramics

An investigation was made into the source of strut cracking during the fabrication process of open cell ceramics that are produced by coating a polymeric foam. Several sources for the stress that produces these cracks were considered, viz., differential drying, thermal expansion mismatch between the polymer and the green ceramic coating, and the gas pressure produced by pyrolysis of the organic skeleton. Thermogravimetric analysis of the polymeric foam was used to estimate the gas evolution rate associated with the pyrolysis process, but this was found to be very low compared to the pressures required to cause strut damage. SEM observations on samples taken by interrupting the fabrication procedure showed the cracks were not produced during drying but rather at a temperature near the melting/decomposition point of the polymer and prior to pyrolysis. It was then deduced that the differential thermal expansion between the polymer and the ceramic coating was the source of the stress. The strut cracking is observed to occur primarily in the region of the highly curved strut edges of the polymer foam, at which the ceramic coating is often rather thin. Techniques to change the processing procedure to overcome the strut cracking are discussed.     

Evaluation of Soybean Seedcoat Cracking During Drying:PART I. Using Drying Tests

In this study, seedcoat cracking during heated air drying was investigated in five varieties of Minnesota grown soybeans. Effects of initial moisture contents, drying temperatures and time on cracking levels were evaluated. Digital image analysis (DIA) was employed to measure initial sizes and shapes of soybeans in order to evaluate the influence of physical properties of mature seeds on cracking frequency.

Seedcoat cracking rates increased significantly with increase in initial moisture content of the soybeans. drying temperature and time. Rapid water loss at higher initial moisture contents led to greater seedcoat cracking. Variety.growing location. and sizc of soybeans had significant influence on seedcoat cracking. Statistical analysis indicates that interactions between various factors had significant influence on seedcoat cracking.     

Computer model of drying behaviour of ceramic green bodies with particular reference to moisture content dependent properties

A numerical model was developed to predict the drying behavior of ceramic green bodies. Resolution of the simultaneous heat and mass transfer equations involved finite elements and the Backward Euler method. Based on experimental data, the model uses equivalent moisture diffusivity, water activity, thermal conductivity and heat capacity as input parameters which depend on moisture content. In particular, the equivalent moisture diffusivity is a key parameter controlling water transport from the body interior to the surface. A simple method was used to estimate the effect of shrinkage on drying rate during the initial drying stage. Predictions of the internal moisture distribution, drying rate and surface temperature as a function of time gave good agreement to experiment for green bodies of alumina paste. External conditions of convection coefficient and relative humidity are shown to sensitively control drying rate and surface temperature evolution during the constant rate period.     

Evaluation of Soybean Seedcoat Cracking During Drying:PART I. Using Drying Tests

ABSTRACT

In this study, seedcoat cracking during heated air drying was investigated in five varieties of Minnesota grown soybeans. Effects of initial moisture contents, drying temperatures and time on cracking levels were evaluated. Digital image analysis (DIA) was employed to measure initial sizes and shapes of soybeans in order to evaluate the influence of physical properties of mature seeds on cracking frequency.

Seedcoat cracking rates increased significantly with increase in initial moisture content of the soybeans. drying temperature and time. Rapid water loss at higher initial moisture contents led to greater seedcoat cracking. Variety.growing location. and sizc of soybeans had significant influence on seedcoat cracking. Statistical analysis indicates that interactions between various factors had significant influence on seedcoat cracking.     

Optimization of Radiant-Convective Drying of a Porous Medium by Design of Experiment Methodology

The major aim of this study was to improve tools to optimize the thermal drying of a porous medium. This article was devoted to the study of the radiant-convective drying of a material (cellular concrete) while respecting some thermal constraints. A numerical program had been previously developed and experimentally validated to model the thermal and hygroscopic behavior of the product. Design of experiments methodology (DOE) was used to obtain a behavioral reduced model that allows the operating optimums to be calculated quickly. Three characteristics of a drying operation were analyzed using response surface methodology: the drying time, the total energy used in the process, and the specific moisture extraction rate. The effects of all the drying parameters (initial moisture content, infrared power, air temperature, velocity, and humidity) were studied. The optimal conditions were determined for convective and infrared-convective drying.     

Moisture Movement and Readsorption Phenomena in Dried Clay Articles

Readsorption of moisture occurs when dried ceramic articles are exposed to an atmosphere bearing water vapor with a partial pressure greater than that of the moisture remaining in the specimens. This readsorption is accompanied by a variable amount of expansion. It is suggested that stresses arising from differential expansion between the moist outside and the drier core are the cause of readsorption cracking or permanent loss of strength. Evidence is presented that diffusion of water vapor through a clay mass does not follow Fick's law, and the effect of this behavior on moisture and stress gradients within the piece is discussed. Calculations of the surface area from readsorption data yield values similar to those obtained by conventional methods despite simplified calculations based on Fick's law. A method of determining the tensile strength which is believed not to have been previously used for clay testing is described.     

Modeling and Numerical Simulation of Clays Cracking During Drying

During drying or desiccation of clay-type materials, some stresses appear. Usually they are compressional inside of the material and tensional close to the surface. If the tensional stresses exceed the material strength, the clay cracks. This article is devoted to the modeling and numerical simulation of this phenomenon. The proposed model consists of two parts. The mass transfer is described by a simple diffusion equation together with convective boundary conditions. In the mechanical part it is assumed that the clay is composed of small particles linked together by cohesive forces. These forces are described with the use of mesh models. Two models are proposed: elastic (mesh consists of springs) and viscoelastic one (mesh consists of Maxwell elements). Four types of clays were tested experimentally to obtain the model parameters. The tested materials were selected with respect to different mineralogical compositions that determine the water-bonding ability. Simulations of the convective drying of bricks made of these clays were performed. It was shown that the degree of cracking depends on the quartz content of the clay. The obtained results were compared with experimental ones and good agreement between simulations and experiment was obtained. Additionally, the inner forces caused by drying are analyzed and discussed in this work.     

Stress fissuring and process duration during rough rice convective drying affected by continuous and stepwise changes in air temperature

During rough rice drying, gradients of moisture content and glass transition temperature cause thermal and mechanical stresses inside the kernel. These stresses eventuate to kernel fissuring during the milling process. In this study, convective drying of Hashemi (long grain) rough rice was applied to investigate the effect of continuous and stepwise changes in air temperature on stress cracking index and process duration. Toward this objective, the concepts of glass transition and analysis of moisture contents distributions within the rice kernel were determined through a numerical modeling of mass transfer. For stepwise temperature change, the drying experiments were conducted at temperatures above the glass transition temperature. Results indicated that the stress cracking index under stepwise temperature change conditions (i.e., within the rubbery state) was reduced compared to the continuous mode probably due to a drip in the moisture content gradients created inside the kernels during the drying process. Moreover, the drying duration significantly was shortened when the kernel was dried within the rubbery state due to faster diffusion moisture within the kernel.     

Shrinkage cracking in Roman cement pastes and mortars

Roman cements were key materials used in the architecture of the nineteenth and early twentieth centuries. Fine cracks, caused by restrained shrinkage during drying, are a distinct characteristic of all Roman cement stuccoes. Today, cracking has become an important barrier preventing broader acceptance of Roman cement as a material by the restoration and construction sector. Drying shrinkage and tensile properties of Roman cement pastes and mortars submitted to various curing and drying regimes were determined as key parameters controlling cracking. A higher volume of aggregate in the mortar mix and a moderate curing time produce optimum Roman cement mortars from the standpoint of reducing the risk of cracking. Fast drying produced significant microcracking due to moisture gradients and differential shrinkage across the specimens. Stress relaxation observed during the long-time loading of the materials reduced their vulnerability to cracking.     

A Small-Scale Pneumatic Conveying Dryer of Rough Rice

This article studies the possibility of reducing the high initial moisture content of wet rough rice using a small-scale low-cost pneumatic conveying dryer as a first stage dryer. The parameters investigated are final moisture content, surface temperature of rough rice, head rice yield, drying rate, power consumption per unit mass of evaporated water, and physical characteristics of rice. Parametric effects of the following variables are examined: velocity of drying air from 20 to 30 m/s, feed rate of rough rice from 150 to 350 kg/h, initial moisture content from 22 to 26% (wet basis), and drying air temperature from 35 to 70°C. From the experimental results, it is found that this drying method can be used for fresh rough rice with an initial moisture content of over 24% (wet basis). The drying process is able to lead to very rapid drying without any grain quality problems such as cracks in the rice kernel. The moisture content can be reduced to approximately 18% (wet basis) or about 5–6% of the initial moisture content within 3–4 s. The optimal drying air temperature is in the range of 50 to 60°C. A comparison of pneumatic conveying drying data obtained from the present study with fluidized bed drying data reported in the open literature is also discussed.     

A Small-Scale Pneumatic Conveying Dryer of Rough Rice

This article studies the possibility of reducing the high initial moisture content of wet rough rice using a small-scale low-cost pneumatic conveying dryer as a first stage dryer. The parameters investigated are final moisture content, surface temperature of rough rice, head rice yield, drying rate, power consumption per unit mass of evaporated water, and physical characteristics of rice. Parametric effects of the following variables are examined: velocity of drying air from 20 to 30 m/s, feed rate of rough rice from 150 to 350 kg/h, initial moisture content from 22 to 26% (wet basis), and drying air temperature from 35 to 70°C. From the experimental results, it is found that this drying method can be used for fresh rough rice with an initial moisture content of over 24% (wet basis). The drying process is able to lead to very rapid drying without any grain quality problems such as cracks in the rice kernel. The moisture content can be reduced to approximately 18% (wet basis) or about 5-6% of the initial moisture content within 3-4 s. The optimal drying air temperature is in the range of 50 to 60°C. A comparison of pneumatic conveying drying data obtained from the present study with fluidized bed drying data reported in the open literature is also discussed.     

EFFECT OF REPEATED WETTING AND DRYING ON PHYSICAL PROPERTIES OF A CLAY BODY*

Specimens of fine-grained, red-firing clay, which had been fired to temperatures corresponding to various stages of vitrification, were subjected to 200 cycles each of wetting at 100°F. and drying at 100°F. and 60% of relative humidity. This treatment, simulating weathering in mild climates, caused (1) a permanent gain in weight which was greater for the softer specimens; (2) a moisture expansion for the softer specimens but none for those near vitrification; (3) a fairly uniform decrease in modulus of elasticity for all specimens; and (4) a decrease in modulus of rupture for the softer specimens but an increase in strength for those that were completely vitrified. The data indicate that moisture expansion and a decrease in strength of soft-fired clay bodies, caused by repeated wetting and drying, may be eliminated by proper vitrification.     

A MATHEMATICAL MODEL FOR PARALLEL FLOW DRYER FOR SLABS WITH HIGH THERMAL DIFFUSIVITY

An analytical model for the process is developed. The thermal diffusivity of the drying slabs is assumed infinite and the moisture diffusivity constant during the entire drying process.

With specified initial and boundary conditions, the mathematical model yields a two-part solution for the diffusion equation. The first part is valid for the initial drying during which the surface moisture content exceeds the value of fiber saturation. This part of the solution is used until the surface moisture content drops to the fiber saturation value. The moisture profile at the end of this period is used as the initial condition for the second period of drying which takes place under hygroscopic conditions.

Two simplifying assumptions are adapted for the hygroscopic region: 1. The dependence between the surface temperature and the moisture content is linear. 2. Constant (average) absorption heat is used during this second drying period.

For both parts of the solution, the surface moisture gradient is proportional to the local temperature difference between the drying air and the slab surface. This temperature difference can be expressed by means of a water mass balance equation for the part of the dryer between the slab in-feed and the point considered and by using the thermodynamic properties of the humid air.     

Evaluation of Soybean Seedcoat Cracking During Drying:PART II. Using MRI

MRI techniques were developed and employed for non-destructive and noninvasive study of seedcoat cracking in low moisture soybean kernels during heated air drying. Proton density image and transient moisture distribution profile of a single soybean kernel can be obtained using MRI. These MRI techniques proved to be particularly useful for the continuous observation of initiation and propagation of seedcoat cracking during the entire period of drying process without interruption.

The proton density images of soybean kernels showed that seedcoat cracking was initiated perpendicular to the long axis of the kernel near the hilum. The transient moisture distribution profiles in soybean kernels during drying indicate that moisture gradient developed during drying was higher in the seedcoat than in the cotyledon. Drying temperature and initial average moisture content were positively correlated with the soyhean seedcoat crackig. The location of the     

A MATHEMATICAL MODEL FOR PARALLEL FLOW DRYER FOR SLABS WITH HIGH THERMAL DIFFUSIVITY

An analytical model for the process is developed. The thermal diffusivity of the drying slabs is assumed infinite and the moisture diffusivity constant during the entire drying process.

With specified initial and boundary conditions, the mathematical model yields a two-part solution for the diffusion equation. The first part is valid for the initial drying during which the surface moisture content exceeds the value of fiber saturation. This part of the solution is used until the surface moisture content drops to the fiber saturation value. The moisture profile at the end of this period is used as the initial condition for the second period of drying which takes place under hygroscopic conditions.

Two simplifying assumptions are adapted for the hygroscopic region: 1. The dependence between the surface temperature and the moisture content is linear. 2. Constant (average) absorption heat is used during this second drying period.

For both parts of the solution, the surface moisture gradient is proportional to the local temperature difference between the drying air and the slab surface. This temperature difference can be expressed by means of a water mass balance equation for the part of the dryer between the slab in-feed and the point considered and by using the thermodynamic properties of the humid air.     

Evaluation of Soybean Seedcoat Cracking During Drying:PART II. Using MRI

ABSTRACT

MRI techniques were developed and employed for non-destructive and noninvasive study of seedcoat cracking in low moisture soybean kernels during heated air drying. Proton density image and transient moisture distribution profile of a single soybean kernel can be obtained using MRI. These MRI techniques proved to be particularly useful for the continuous observation of initiation and propagation of seedcoat cracking during the entire period of drying process without interruption.

The proton density images of soybean kernels showed that seedcoat cracking was initiated perpendicular to the long axis of the kernel near the hilum. The transient moisture distribution profiles in soybean kernels during drying indicate that moisture gradient developed during drying was higher in the seedcoat than in the cotyledon. Drying temperature and initial average moisture content were positively correlated with the soyhean seedcoat crackig. The location of the     

Modeling convective drying of wet cake

This study analyzed convective drying of wastewater sludge cakes with three-dimensional cake structures probed using an X-ray micro-computerized tomography scanner (micro-CT), considering the development of cracks and cake morphology. The presence of artificial cracks on cake surface assist drying, but those occurred naturally cannot. The cake surface is noted far from saturation over drying. Moreover, the cracks transport easily moisture to cake surface, hence yielding high surface humidity (and rates) for drying. Comprehensive drying model has to incorporate real boundary conditions for success modeling.