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1.
黄恒超  沈家瑞 《功能材料》1996,27(4):335-338
研究用二氧化硅负载n-β(氨乙基)-γ(氨丙基)三乙氧基硅烷[NH2(CH2)2NH(CH2)3Si(OEt)3]作为分散颗粒制备的电流变(ER)流体的流变行为。结果发现,流体具有宾汉流体的特点。以硅油为分散介质,含20%(W/V)分散颗粒的流体,不添加任何活化剂,在剪切速率(r)为8.066s-1时,电场强度(E)从0升至1.50kV/mm,表观粘度(ηa)从0.35Pa·s增大到26.5Pa·s。r提高,ηa降低。改变电场强度、分散颗核含量、分散介质种类和添加极性分子,可以改变流体的剪切应力和表观粘度,但不能改变流型。  相似文献   

2.
温和条件下介孔分子筛MCM-41的修饰与表征   总被引:12,自引:0,他引:12  
在温和条件下,以3-氨丙基三乙氧基硅烷为偶联剂,修饰介孔分子筛 MCM-41(Si/Al=35),成功地将有机官能团引入到介孔分子筛孔道中,制备了一种无机一有机复合材料MCM-(CHNH,以 XRD、FTIR、DTA-TGA、 N吸附-脱附和 HREM表征了复合材料;结果表明:有机基团-(CHNH不仅进人孔道、修饰了MCM-41的孔壁,而且使介孔分子筛MCM-41保持了有序的孔道结构.  相似文献   

3.
本文以SiCl4-NH3、SiCl4-O2、SiCl4-N2-H2、TiCl4-NH3-H2、TiCl4-N2-H2、TiCl4-O2、AlCl3-O2等为体系,运用均匀成核理论,研究了平衡常数Kp、过饱和比S及临界核半径,r*等因素对气相反应法中超细粉末的形成及粉末结构状态的影响.结果表明,当2r*大于某物质的晶格常数时,用气相反应法得到的该物质的超细粉末一般为晶体粉末,反之则得到无定形粉末.  相似文献   

4.
(Si-,Al-)陶瓷化木材的化学方法   总被引:36,自引:0,他引:36  
以 AlCl3.6H2O为原料,制备高盐基度碱式氯化铝 Al2(OH)nCl6-n,作为催化剂及网络形成剂参与陶瓷前驱体中TEOS、GPTMS的水解、缩聚反应.将其注入木材并热处理,得到高性能的(AI-, Si-)陶瓷化木材  相似文献   

5.
在等离子体化学气相沉积系统(PECVD)中,使用高氢稀释硅烷(SiH4)加乙烯(C2H4)为反应气氛制备了纳米硅碳(nc-SiCx^2H)薄膜,随着(C2H4+SiH4)/H2(Xg)从5%时,由于H蚀刻效应的减弱,薄膜的晶态率从48%下降到8%,平均晶粒尺寸在3.5-10nm。当Xg≥6%时,生成薄膜为非晶硅碳(a-SiCx^2H)薄膜。nc-SiCx^2H薄膜的电学性质具有与薄膜的晶态率紧密相  相似文献   

6.
常压MOCVD制备MgO薄膜的研究   总被引:1,自引:0,他引:1  
曾建明  王弘 《功能材料》1996,27(4):342-346
本文首次报道用常压金属有机化学气相沉积(AP-MOCVD)在Si(100),SiO2/Si(100)和Pt/Si(100)衬底上外延高质量的MgO薄膜。研究了衬底温度与薄膜的取向性关系和MgO薄膜的潮解特性。高纯magnesiumacetylacetonate[bis(2,4-pentanetane-diono)magnesium][Mg(CH2COCH2COCH3)2]作为金属有机源,扫描电镜(SEM),透射电镜(TEM)和X-RAY衍射实验显示,在较低的衬底温度(~480℃)下一次淀积成单晶膜。薄膜均匀,致密,结晶性和取向性很好,衬底温度(Ts)在400℃到680℃之间,在Si(100)衬底上生长的MgO薄膜都具有[100]取向,在Si(100)、SiO2/Si(100)和Pt/Si(100)衬底上生长的MgO薄膜也都具有[100]取向。  相似文献   

7.
采用(CH3)2SiCl2和N2H4反应产物为先驱体,在H2,NH3气条件下,用CVD法制备Si/C/N的纳米微粉,在制备Si/C/N纳米微粉的过程中通过高温炉-气相色谱联用技术分析了裂解逸出的气体,用化学法分析了微粉中元素组成变化,讨论了先驱体H2,NH3气体条件下的裂解机理及微粉的形成机理。  相似文献   

8.
Al2O3和Y2O3包覆的SiC复合粒子制备   总被引:9,自引:0,他引:9  
本文利用非均匀成核法,将Al(OH)3和Y(OH)3均匀地包覆在SiC粒子表面,制备出被覆Al2O3和Y2O的SiC复合粒子,包覆Al(OH)3的SiC粒子,其等电点IEP的pH=3.4移至pH=7.3,再用Y(OH)3包覆表面被覆Al(OH)3的SiC复合粒子后,其等电点IEP又从pH=7.3移至pH=8.6dadk。  相似文献   

9.
本文探讨了Si及α-Al2O3超细粉对Al2O3-ZrO2-C系材料显微结构的影响.认为在Al2O3-ZrO2-C系材料中同时加入Si和α-Al2O3超细粉,Si粉除了与C生成了SiC纤维外,其反应产物SiO2还与α-Al2O3超细粉及ZrO2生成了莫来石(A3S2)和Al2O3-ZrO2-SiO2(AZS)固溶体,这些新生成的矿物相对试样的显微结构产生重要的作用.  相似文献   

10.
本文以SiC板粒、ZrOCl2-8H2O、AlCl3和Y(MO)3为原料,利用共沉淀和热压烧结工艺,制备SiC板粒/Y-TZP和(含Al2O3)SiC板粒/Y-TZP复合材料.测试了材料的室温和高温力学性能.研究了添加Al2O3对SiC板粒/Y-TZO复合材料的影响.结果表明,SiC板粒/Y-TZP复合材料与Y-TZP陶瓷相比,其室温强度和韧性出现明显下降,高温强度也没有改善;而在SiC板粒与Y-TZP复合的基础上,添加Al2O3可明显提高材料的强度和断裂韧性,同时,材料的高温强度也获得显著改善.  相似文献   

11.
Standards are the basis for production enterprises to organize production, ex-factory inspection, trade (delivery) and technical exchanges, product certification, quality arbitration and supervision.……  相似文献   

12.
Zusammenfassung Bei der Gestaltung von Ernteprozessen — beispielsweise des Prozesses Mähdrusch, Körnertransport und -abnahme — als transportverbundene Fließarbeitsverfahren mit mindestens zwei verschiedenen Arbeitsmitteln gibt es einen großen Optimierungsspielraum. Solche Prozesse sind mehrstufige Bedienungsprozesse mit gemischter Anordnung der Bedienungseinrichtungen. Außerdem besitzen sie stark ausgeprägte räumliche Aspekte. Es wird vor allem gezeigt, welche Merkmale solcher Prozesse in Simulationsmodellen abgebildet sein müssen, welche Zielgrößen in Abhängigkeit von welchen Einflußgrößen unter Berücksichtigung welcher Prozeßbedingungen ermittelt werden sollten und wie der Bewertungsprozeß zur Ermittlung der gewünschten Informationen gestaltet werden muß.  相似文献   

13.
正Responding to ISO’s appeal for survey for the to-be-developed ISO Strategy Plan for 2016-2020,SAC hosted a special workshop over the needs and comments of various fi elds on June 8 in Beijing.The workshop was attended by ISO President-elect and Ansteel General Manager Zhang Xiaogang,SAC Vice-Administrator Yu Xinli,and 30 experts from  相似文献   

14.
正The review group of Asia Pacific Laboratory Accreditation Cooperation(APLAC)carried out a 4-day peer review of the proficiency testing provider(PTP)for China National Accreditation Service for Conformity Assessment(CNAS)from July 28 to 31,2014.CNAS passed the PTP review with excellent performance.Two senior peer reviewers of APLAC made a comprehensive,rigorous and detailed review of CNAS’s PTP accreditation activities,and made the on-spot inspection of the review groups in Shanghai and Shenzhen respectively.  相似文献   

15.
新闻(英文)     
正China and Greece Sign the Standardization Cooperation Agreement Witnessed by Chinese Premier Li Keqiang and Greek Prime Minister Antonis Samaras,AQSIQ Minister Zhi Shuping and ELOT Chairman and Executive Director Angelos Tolkas signed the SAC-ELOT Standardization Cooperation Agreement.The Agreement is one of the critical cooperation documents signed during Li Keqiang’s visit in Greece,encouraging China and Greece to  相似文献   

16.
正The Chinese Premier Li Keqiang's recent trip to the UK has reinforced the China-UK comprehensive strategic partnership;just as the British Prime Minister David Cameron put it,"the relationship is gaining in strength,depth and understanding"after a bucket of business deals being inked worth more than 30 billion US dollars.From the first agreement signing in 2004 to the new agreement of mutual standards recognition and adoption in  相似文献   

17.
正A national directory of standards complexes for strategic emerging sectors was recently developed and released jointly by 12governmental departments,namely,SAC,NDRC,MOST,MIIT,MEP,MOA,AQSIQ,State Forest Administration,State Administration of Science and Technology for National Defense,State Oceanic Administration and National Railway Administration.  相似文献   

18.
正Four new national standards on air pollutant emission control offi cially issued by the Ministry of Environment Protection(MEP)together with AQSIQ and SAC has been brought into force from July 1,2014.The Emission standard for air pollutants of coal-burning,oil-burning and gasfi red boilers,which is the strictest emission standard historically,will tackle the stubborn pollution problem of boilers and waste incineration in most of China’s regions.  相似文献   

19.
《新型炭材料》2014,(6):460
New Carbon Materials is a bimonthly journal published with the permission of the Ministry of Science and Technology and of the State News and Publication Agency.The journal is sponsored by the Institute of Coal Chemistry,Chinese Academy of Sciences,and is published by Science Press.Aims and Scope  相似文献   

20.
正Recently,National Copyright Administration of China(NCAC)has rewarded 215 organizations and 179 individuals for their outstanding efforts on investigating standards copyright infringement and piracy in 2013.Hua Jianhua,the Deputy-Director of National Standards Copyright Protection Workgroup Office won a third prize of the national individual award.In 2012,SAC set up the national standards copyright protection working group,and developed policies to crack down standards infringement and piracy behaviors and to strengthen standards copyright protection.  相似文献   

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