Flip chip attachment on flexible LCP substrate using an ACF

In this study the reliability of a flip chip bonding process using anisotropic conductive adhesives (ACA) was evaluated. The flexible substrates used were made of liquid crystal polymer (LCP), which is an interesting new material having excellent properties for flexible printed circuit boards. The test samples were prepared using two different anisotropic conductive films (ACF) having the same fast-cure resin matrix, but different conductive particles. The reliability of the test samples was studied by accelerated environmental tests. In the constant humidity test the temperature was 85 °C and the relative humidity was 85%. The temperature cycling test was carried out between temperatures of −40 °C and 85 °C. To determine the exact time of a failure the resistance of each test sample was measured using continuous real-time measurement. A clear difference between the behaviour of the conductive particles was seen in the test. While the adhesive having polymer particles had only one failure during testing, the adhesive having nickel particles had a considerable number of failures in both tests. Cross sections of the samples were made to analyze the failure mechanisms.     

Anisotropic conductive film flip chip joining using thin chips

In this study, flip chip interconnections were made on very flexible polyethylene naphthalate substrates using anisotropic conductive film. Two kinds of chips were used: chips of normal thickness and thin chips. The thin chips were very thin, only 50 μm thick. Due to the thinness of the chips they were flexible and the entire joint was bendable. The reliability properties of the interconnections established with these two different kinds of chips were compared. In addition, the effect of bending of the chip and joint area on the joint reliability was studied. Furthermore, part of the substrates was dried before bonding and the effect of that on the joint performance was investigated.The pitch of the test vehicles was 250 μm and the chips had 25 μm high gold bumps. For resistance analysis there were two four-point measuring positions in each test vehicle. For finding the optimal bonding conditions for the test vehicles, the bonding was done using two different bonding pressures, of which the better one was chosen for the final tests.Furthermore, the test vehicles were subjected to thermal cycling tests between −40 and +125 °C (half-an-hour cycle) and to a humidity test (85%/85 °C). Part of the test vehicles were bent during the tests. Finally, the structures of the joints were studied using scanning electron microscopy.     

Development of chip-on-flex bonding using Sn-based bumps and non-conductive adhesive

We developed a reliable and low cost chip-on-flex (COF) bonding technique using Sn-based bumps and a non-conductive adhesive (NCA). Two types of bump materials were used for the bonding process: Sn bumps and Sn–Ag bumps. The bonding process was performed at 180 °C for 10 s using a thermo-compression bonder after dispensing the NCA. Sn-based bumps were easily deformed to contact Cu pads during the bonding process. A thin layer of Cu₆Sn₅ intermetallic compound was observed at the interface between Sn-based bumps and Cu pads. After bonding, electrical measurements showed that all COF joints had very low contact resistance, and there were no failed joints. To evaluate the reliability of COF joints, high temperature storage tests (150 °C, 1000 h), thermal cycling tests (−25 °C/+125 °C, 1000 cycles) and temperature and humidity tests (85 °C/85% RH, 1000 h) were performed. Although contact resistance was slightly increased after the reliability test, all COF joints passed failure criteria. Therefore, the metallurgical bond resulted in good contact and improved the reliability of the joints.     

Study of the effect of reflow time and temperature on Cu–Sn intermetallic compound layer reliability

In terms of various reflow time and temperature, an analysis of Cu–Sn intermetallic compound (IMC) layer reliability is presented in this paper. Temperature cycling test data reported in existing publications for the solder paste material of 63Sn/37Pb eutectic alloy is used to model the probability distribution functions of solder joint lifetime due to the IMC layer fatigue. The relationship of the IMC layer thickness as a function of reflow time and temperature is studied. A reliability and mean time to failure function of the IMC layer in terms of various reflow time and temperature are presented. Calculation suggests that to achieve a higher IMC layer reliability, a shorter reflow time and a lower reflow temperature should be used, while lowering reflow temperature may be more efficient than controlling reflow time. In general, a reflow temperature ranged by 240–280 °C should be avoided. For a specified reliability goal, how to choose proper reflow time and temperature is discussed.     

Effects of different bonding parameters on the electrical performance and peeling strengths of ACF interconnection

The effects of different bonding parameters, such as temperature, pressure, curing time, bonding temperature ramp and post-processing, on the electrical performance and the adhesive strengths of anisotropic conductive film (ACF) interconnection are investigated. The test results show that the contact resistances change slightly, but the adhesive strengths increase with the bonding temperature increased. The curing time has great influence on the adhesive strength of ACF joints. The contact resistance and adhesive strength both are improved with the bonding pressure increased, but the adhesive strengths decrease if the bonding pressure is over 0.25 MPa. The optimum temperature, pressure, and curing time ranges for ACF bonding are concluded to be at 180–200 °C, 0.15–0.2 MPa, and 18–25 s, respectively. The effects of different Teflon thickness and post-processing on the contact resistance and adhesive strength of anisotropic conductive film (ACF) joints are studied. It is shown that the contact resistance and the adhesive strength both become deteriorated with the Teflon thickness increased. The tests of different post-processing conditions show that the specimens kept in 120 °C chamber for 30 min present the best performance of the ACF joints. The thermal cycling (−40 to 125 °C) and the high temperature/humidity (85 °C, 85% RH) aging test are conducted to evaluate the reliability of the specimens with different bonding parameters. It is shown that the high temperature/humidity is the worst condition to the ACF interconnection.     

Highly reliable, fine pitch chip on glass (COG) joints fabricated using Sn/Cu bumps and non-conductive adhesives

We have developed a reliable and ultra-fine pitch chip on glass (COG) bonding technique using Sn/Cu bumps and non-conductive adhesive (NCA). Sn/Cu bumps were formed by electroplating and reflowed, forming dome shaped Sn bumps on Cu columns. COG bonding was performed between the reflowed Sn/Cu bumps on the oxidized Si wafer and ITO/Au/Cu/Ti/glass substrate using a thermo-compression bonder. Three different NCAs were applied during bonding. Bonding temperature was 150 °C for NCA-A and NCA-B, and 110 °C for NCA-C. The electrical properties of COG joints were evaluated by measuring the contact resistance of each joint through the four-point probe method. All joints were successfully bonded and the electrical measurement showed that the average contact resistance of each joint was approximately 30 mΩ, regardless of NCA types. The COG joints were subjected to a series of reliability tests: high temperature storage test (85 °C, 160 h); thermal cycling test (−40 °C/+85 °C, 20 cycle); and a temperature and humidity test (50 °C/90%, 160 h) were sequentially performed to evaluate the reliability of the COG joints. The contact resistance measurement showed that there were no failed bumps in all specimens and all joints passed the criterion after reliability test.     

A two-layer high density printed circuit board and its reliability

The fabrication and reliability of a two-layer high density PCB test vehicle are reported in this paper. The test board consisted of two copper layers that were sequentially built up on one side of a FR4 substrate and interconnected through a photovia dielectric layer. Various test structures were fabricated for reliability testing. Thermal cycling, 85°C/85%RH ageing, and multiple reflow excursions were performed to test the reliability of electrical continuity and insulation. Peel strength was measured after fabrication as well as after 150°C annealing and reflow excursions. Initial results have revealed that photovias may be more reliable than conventional through vias.     

Board level reliability assessment of chip scale packages

A large program had been initiated to study the board level reliability of various types of chip scale package (CSP). The results on six different packages are reported here, which cover flex interposer CSP, rigid interposer CSP, wafer level assembly CSP, and lead frame CSP. The packages were assembled on FR4 PCBs of two different thicknesses. Temperature cycling tests from −40°C to +125°C with 15 min dwell time at the extremes were conducted to failure for all the package types. The failure criteria were established based on the pattern of electrical resistance change. The cycles to failure were analyzed using Weibull distribution function for each type of package. Selected packages were tested in the temperature/humidity chamber under 85°C/85%RH for 1000 h. Some assembled packages were tested in vibration condition as well. In all these tests, the electrical resistance of each package under testing was monitored continuously. Test samples were also cross-sectioned and analyzed under a Scanning Electronic Microscope (SEM). Different failure mechanisms were identified for various packages. It was noted that some packages failed at the solder joints while others failed inside the package, which was packaging design and process related.     

Reliability modeling of Sn–Ag transient liquid phase die-bonds for high-power SiC devices

In this work, a novel foil-based transient liquid phase bonding process has been used to mount the SiC Schottky diodes. The Sn–Ag TLP interlayer material was produced in the form of preforms of multilayer foils, using electrochemical deposition. The foils were designed to keep the overall composition of Ag and Sn about 80% and 20% respectively. The optimized TLP bonding process parameters were used during the assembly process. The die-attachment characterizations revealed that resulting intermetallic compounds (Ag₃Sn and ζ) have melting point beyond 480 °C. The die-attachment produced low bending stresses, while heated from 30 °C to 400 °C. The reliability of Sn–Ag TLP bonded samples was studied during passive temperature cycling and during active power cycling. During power cycling, the crack rates were determined by measuring the crack lengths of the TLP bonded joints after failure. The failure criteria were set to be an increase of diode's forward voltage by 10% since the start of the power cycling tests. The thermo-mechanical simulations were performed to determine the damage parameter i.e. strain range amplitude ∆ ε_p. Based on mechanical characterization of the TLP bonded layers, a plastic material model was used. The crack propagation rates were modeled using Paris' Law. Based on comparisons with state-of-the-art silver sintering technique, it can be stated that the TLP bonding is a promising die-attachment technique and its power cycling reliability is similar to silver sintering.     

Effect of voids on the reliability of BGA/CSP solder joints

Voids in solder joints have been considered as a defect in electronics assembly. The factors that affect void formation are complex and involve the interaction of many factors. There are no established standards for void size and void area in a solder joint for it to be deemed defective. Inspection criteria have been very subjective. The effect of voids on the reliability of solder joint may depend not only on the size, but also on frequency and location. This study is focussed on investigating the effect of voids on the reliability of solder joints. The size, location and frequency effects on the reliability were studied. Testing was done by mechanical deflection testing (torsion) system and air to air thermal cycling (−40 °C/125 °C). Failures were analyzed for the failure modes by cross sectional analysis. The results indicate that voids reduce the life of the solder joint. Voids which are greater than 50% of the solder joint area, decrease the mechanical robustness of the solder joints. Small voids also have an effect on the reliability, but it is dependent on the void frequency and location.     

Effects of process conditions on reliability, microstructure evolution and failure modes of SnAgCu solder joints

In this study, microstructure evolution at intermetallic interfaces in SnAgCu solder joints of an area array component was investigated at various stages of a thermal cycling test. Failure modes of solder joints were analyzed to determine the effects of process conditions on crack propagation. Lead-free printed-circuit-board (PCB) assemblies were carried out using different foot print designs on PCBs, solder paste deposition volume and reflow profiles. Lead-free SnAgCu plastic-ball-grid-array (PBGA) components were assembled onto PCBs using SnAgCu solder paste. The assembled boards were subjected to the thermal cycling test (−40 °C/+125 °C), and crack initiation and crack propagation during the test were studied. Microstructure analysis and measurements of interface intermetallic growth were conducted using samples after 0, 1000, 2000 and 3000 thermal cycles. Failures were not found before 5700 thermal cycles and the characteristic lives of all solder joints produced using different process and design parameters were more than 7200 thermal cycles, indicating robust solder joints produced with a wide process window. In addition, the intermetallic interfaces were found to have Sn–Ni–Cu. The solder joints consisted of two Ag–Sn compounds exhibiting unique structures of Sn-rich and Ag-rich compounds. A crystalline star-shaped structure of Sn–Ni–Cu–P was also observed in a solder joint. The intermetallic thicknesses were less than 3 μm. The intermetallics growth was about 10% after 3000 thermal cycles. However, these compounds did not affect the reliability of the solder joints. Furthermore, findings in this study were compared with those in previous studies, and the comparison proved the validity of this study.     

A quantitative method of reliability estimation for surface mount solder joints based on heating factor Qη

A novel method of reliability analysis on thermal fatigue failure for surface mount solder joints, based on the heating factor Q_η, is presented, by which quantitative reliability estimation and prediction of solder joints suffering from cyclic thermal stress can be done. Based on the typical lifetime data of thermal cycling test, the relationship of the mean time to failure (MTTF) as well as the reliability of solder joints as an explicit function of Q_η is deduced and presented in a unified mathematic form. Numerical calculations are performed, and the result shows that the MTTF decreases quickly with the increases in heating factor and then slowly approximates to a constant value when Q_η  1500 s °C. The solder joint reliability in terms of thermal cycle degrades in an analogical fashion for different heating factors. For any given thermal cycle, calculation suggests that to obtain a higher reliability, a lower heating factor should be controlled during soldering. The presented method gives an applicable solution and can be used for online reflow control in industry. On the one hand, an ideal reflow profile can be achieved by properly controlling heating factor during soldering to meet the given reliability goal. On the other hand, the life expectancy of solder joints can be approximately estimated and predicted from a known reflow profile with a specified heating factor. Finally, for a specified reliability goal, how to properly choose and control heating factor during soldering to achieve reliable solder joints is discussed.     

Solder joint reliability of TFBGA assemblies with fresh and reworked solder balls

In this article, the solder joint reliability of thin and fine-pitch BGA (TFBGA) with fresh and reworked solder balls is investigated. Both package and board level reliability tests are conducted to compare the solder joint performance of test vehicle with fresh and reworked solder balls. For package level reliability test, ball shear test is performed to evaluate the joint strength of fresh and reworked solder balls. The results show that solder balls with rework process exhibit higher shear strength than the ones without any rework process. The results also exhibit that the different intermetallic compound (IMC) formation at solder joints of fresh and reworked solder balls is the key to degradation of shear strength. For board level reliability tests, temperature cycling and bending cyclic tests are both applied to investigate the fatigue life of solder joint with fresh and reworked solder balls. It is observed that package with reworked solder ball has better fatigue life than the one with fresh solder ball after temperature cyclic test. As for bending cyclic test, in addition to test on as-assembled packages, reworked and fresh samples are subjected to heat treatment at 150 °C for 100 h prior to the bending cyclic test. The purpose is to let Au–Ni–Sn IMC resettle at solder joints of fresh solder ball and examine the influence of Au–Ni–Sn IMC on the fatigue life of solder joints (Au embrittlement effect). The final results confirm that reworked solder balls have better reliability performance than fresh one since Au embrittlement dose exist at fresh solder ball.     

The effect of reflow process on the contact resistance and reliability of anisotropic conductive film interconnection for flip chip on flex applications

The work presented in this paper focuses on the effect of reflow process on the contact resistance and reliability of anisotropic conductive film (ACF) interconnection. The contact resistance of ACF interconnection increases after reflow process due to the decrease in contact area of the conducting particles between the mating I/O pads. However, the relationship between the contact resistance and bonding parameters of the ACF interconnection with reflow treatment follows the similar trend to that of the as-bonded (i.e. without reflow) ACF interconnection. The contact resistance increases as the peak temperature of reflow profile increases. Nearly 40% of the joints were found to be open after reflow with 260 °C peak temperature. During the reflow process, the entrapped (between the chip and substrate) adhesive matrix tries to expand much more than the tiny conductive particles because of the higher coefficient of thermal expansion, the induced thermal stress will try to lift the bump from the pad and decrease the contact area of the conductive path and eventually, leading to a complete loss of electrical contact. In addition, the environmental effect on contact resistance such as high temperature/humidity aging test was also investigated. Compared with the ACF interconnections with Ni/Au bump, higher thermal stress in the Z-direction is accumulated in the ACF interconnections with Au bump during the reflow process owing to the higher bump height, thus greater loss of contact area between the particles and I/O pads leads to an increase of contact resistance and poorer reliability after reflow.     

低银无铅焊膏板级封装工艺和焊点可靠性试验

针对低Ag无铅焊膏的市场需求,研究开发了一种适用于99.0Sn0.3Ag0.7Cu低Ag无铅焊膏用松香型无卤素助焊剂(WTO—LF3000),配制了相应的无铅焊膏(WTO—LF3000—SAC0307),并对其板级封装工艺适应性及焊点可靠性进行了考察,用测试后样品的电气可靠性作为接头可靠性评价条件。结果表明:所开发的低Ag无铅焊膏熔点和润湿性符合产品实际要求。配制的焊膏印刷质量良好,焊点切片观察其孔隙率<25%,满足行业标准IPC—A—610D之要求。样品分别经跌落、震动和温度循环试验后,无焊点脱落等现象,电气功能正常。     

Long time reliability study of soldered flip chips on flexible substrates

Due to the requirements of new light, mobile, small and multifunctional electronic products the density of electronic packages continues to increase. Especially in medical electronics like pace makers the minimisation of the whole product size is an important factor. So flip chip technology becomes more and more attractive to reduce the height of an electronic package. At the same time the use of flexible and foldable substrates offers the possibility to create complex electronic devices with a very high density. In terms of human health the reliability of electronic products in medical applications has top priority.In this work flip chip interconnections to a flexible substrate are studied with regard to long time reliability. Test chips and substrates have been designed to give the possibility for electrical measurements. Solder was applied using conventional stencil printing method. The flip chip contacts on flexible substrates were created in a reflow process and underfilled subsequently.The assemblies have been tested according to JEDEC level 3. The focus in this paper is the long time reliability up to 10,000 h in thermal ageing at 125 °C and temperature/humidity testing at 85 °C/85% relative humidity as well as thermal cycling (0 °C/+100 °C) up to 5000 cycles. Daisy chain and four point Kelvin resistances have been measured to characterise the interconnections and monitor degradation effects.The failures have been analysed in terms of metallurgical investigations of formation and growing of intermetallic phases between underbump metallisation, solder bumps and conductor lines. CSAM was used to detect delaminations at the interfaces underfiller/chip and underfiller/substrate respectively.     

Reliability and RF performance of BGA solder joints with plastic-core solder balls in LTCC/PWB assemblies

In this paper board-level reliability of low-temperature co-fired ceramic (LTCC) modules with thermo-mechanically enhanced ball-grid-array (BGA) solder joint structure mounted on a printed wiring board (PWB) was experimentally investigated by thermal cycling tests in the 0–100 °C and −40 to 125 °C temperature ranges. The enhanced joint structure comprised solder mask defined (SMD) AgPt pad metallization, eutectic solder and plastic-core solder balls (PCSB). Similar daisy-chained LTCC modules with non-collapsible 90Pb10Sn solder spheres were used for a reference test set. The reliability of the joint structures was analyzed by resistance measurements, X-ray microscopy, scanning acoustic microscopy (SAM) and SEM/EDS investigation. In addition, a full-wave electromagnetic analysis was performed to study effects of the plastic-core material on the RF performance of the LTCC/BGA package transition up to millimeter-wave frequencies. Thermal cycling results of the modules with PCSBs demonstrated excellent fatigue performance over that of the reference. In the harsher cycling test, Weibull’s shape factor β values of 7.9 and 4.8, and characteristic lifetime θ values of 1378 and 783 were attained for the modules with PCSBs and 90Pb10Sn solder spheres, respectively. The primary failure mode in all test assemblies was fatigue cracking in eutectic solder on the ceramic side.     

Study of micro-BGA solder joint reliability

A new reflow parameter, heating factor (Q_η), which is defined as the integral of the measured temperature over the dwell time above liquidus, has been proposed in this report. It can suitably represent the combined effect of both temperature and time in usual reflow process. Relationship between reliability of the micro-ball grid array (micro-BGA) package and heating factor has been discussed . The fatigue failure of micro-BGA solder joints reflowed with different heating factor in nitrogen ambient has been investigated using the bending cycle test. The fatigue lifetime of the micro-BGA assemblies firstly increases and then decreases with increasing heating factor. The greatest lifetime happens at Q_η near 500 s °C. The optimal Q_η range is between 300 and 750 s °C. In this range, the lifetime of the micro-BGA assemblies is greater than 4500 cycles. SEM micrographs reveal that cracks always initiate at the point of the acute angle where the solder joint joins the PCB pad.     

Microstructure evolution of eutectic Sn-Ag solder joints

Laser and infrared reflow soldering methods were used to make Sn-Ag eutectic solder joints for surface-mount components on printed wiring boards. The microstructures of the joints were evaluated and related to process parameters. Aging tests were conducted on these joints for times up to 300 days and at temperature up to 190°C. The evolution of microstructure during aging was examined. The results showed that Sn-Ag solder microstructure is unstable at high temperature, and microstructural evolution can cause solder joint failure. Cu-Sn intermetallics in the solder and at copper-solder interfaces played an important role in both the microstructure evolution and failure of solder joints. Void and crack formation in the aged joints was also observed.     

Thermo-mechanical reliability analysis of a RF SiP module based on LTCC substrate

The RF SiP module based on LTCC substrate has attracted considerable attention in wireless communications for the last two decades. However, the thermo-mechanical reliability of this 3D LTCC architecture has not been well-studied as common as its traditional ceramic package structure. A practical RF SiP module based on LTCC substrate was presented and its thermo-mechanical reliability was analyzed in this paper, with emphasis on the reliability of heat reflow process, the operating state and fatigue of second-level solder joints. The configuration and assembly process of the SiP module were briefly introduced at first, and qualitative analysis was made according to the reliability problem that may occur in the manufacturing process and the operating state. Through FEM simulation, this paper studied the warpage and stress variation of the RF SiP module, as well as parametric studies of some key package dimensions. Solder joint reliability under temperature cycling condition was also analyzed in particular in this paper. The results show that for the heat reflow process and operating state, the maximum warpage is both on the top LTCC substrate, but the maximum stresses are on the outermost solder ball and the kovar column at the corner, respectively. There is a large residual stress on the critical solder ball at the end of the reflow process and the key package dimensions has little effect on it. The thickness of top LTCC substrate has a significant impact on the thermal deformation and thermal stress, followed by the height of kovar columns. The reason for the considerable thermal stress on the kovar column is the non-uniform of temperature distribution. The key to reducing thermal deformation and stress in the operating state is the employment of effective cooling measures. It is found by comparison that the reliability of critical solder joints can be greatly improved by adding suitable underfill.