Mechanical behavior of heat-treated spruce (Picea abies) wood at constant moisture content and ambient humidity

The mechanical behavior of heat-treated spruce wood was investigated in relation to the mass loss that occurs during thermal treatment. At constant wood moisture content, the strength, failure strain and toughness of wood were reduced by the heat-bath treatment, decreasing with increasing mass loss. The stiffness was unaffected up to a mass loss of about 3%, and thereafter it decreased. The mechanical properties, however, are not only dependent on the mass loss but also on the relative humidity in the heating atmosphere. As a function of mass loss, the inelastic ductility and the inelastic toughness were the lowest when wood was heated in a dry climate, as compared to a moist climate. On the other hand, the mechanical properties of heat-treated wood were tested at constant ambient humidity. In such circumstances, the failure strain and the toughness were still reduced, but the strength and the stiffness were actually improved up to a mass loss of about 2%–3%. The improvement is due to the lower equilibrium moisture content of heat-treated wood when placed in service conditions. As a function of mass loss, wood heated at intermediate relative humidity (in the vicinity of 50%) exhibited the best mechanical behavior, which surprisingly included inelastic ductility. This is believed to be due to some irreversible hydrogen bonding.     

Influence of fungal decay by different basidiomycetes on the structural integrity of Norway spruce wood

The potential influence of diverse decay patterns caused by different brown rot causing basidiomycetes on the structural integrity of wood was investigated. Therefore, decayed Norway spruce (Picea abies Karst.) specimens representing a wide range of mass loss, caused by four different brown-rot fungi and one white-rot fungus, were applied to a high-energy multiple impact (HEMI)-test series. The relationship between the resistance to impact milling (RIM) and the mass loss by fungal decay could be subdivided into three areas: 1. Prior to measurable mass loss, a strength reduction was detectable due to the depolymerisation of wood cell wall components. 2. Between 0 and 25–30% mass loss, RIM decreased with increasing mass loss. 3. Above 30% mass loss, RIM increased again due to gluing effects of the fungal mycelium. The influence of the different brown rot fungi on the structural integrity of the wood differed slightly, but partly significantly.     

Effect of heat treatment on the wettability of white ash and soft maple by water

Heat treatment of wood has attracted a lot of attention both in Europe and recently in North America as an environmentally-friendly wood-protection method. The untreated wood is hydrophilic (high affinity for water). During the heat treatment, wood becomes more and more hydrophobic (low affinity for water) with increasing heat treatment temperature. As a result, it becomes more resistant to biological attacks. Furthermore, it becomes dimensionally more stable compared to untreated wood. Its hardness increases. As the wood becomes more hydrophobic, its wettability by water decreases. The effect of heat treatment is different for each species. Studying the wetting characteristics of heat treated wood gives a good indication of the heat treatment effects on certain wood properties which are related to its degree of hydrophobic character. The aim of this work was to study the characteristics of dynamic wetting process for two different heat-treated North American wood species white ash (Fraxinus americana) and soft maple (Acer rubrum). Contact angle measurements before and after heat treatment showed a significant increase in wood hydrophobicity. Advancing contact angles of a water drop were in all cases higher for heat-treated wood than for untreated wood.     

Eigenschaften von extrudierten Holz-Kunststoff-Werkstoffen auf Basis von Refiner-(TMP-)Fasern und Hanffasern

At present, wood particles (wood flour) with a low aspect ratio are mostly used as fillers in wood-plastic composites (WPC). Reinforcement of WPC and improved strength properties may be achieved by using real wood fibres with a high aspect ratio. WPC based on 70% (wt.) refiner (TMP) wood fibres and mechanically processed hemp fibres were extruded in a two-step process. Eleven compounds based on the two natural fibre types were prepared using a thermokinetic mixer and extruded in a conical, counter-rotating twin-screw extruder. Additional formulation components were polypropylene fibres, maleic anhydride-modified polypropylene (MAPP) and lubricant. It was determined that compounding in a thermokinetic mixer is a useful step for processing of WPC with refiner and hemp fibres as little fibre damage occurred. However, during extrusion, both natural fibre types were severely shortened due to strong shear forces, and homogeneous dispersion of fibres in the matrix was not achieved. WPC based on hemp fibres displayed the best strength properties of the formulations tested. Current extruder screw and die configurations need to be modified to achieve improved fibre reinforcement and to create new, structurally demanding applications for WPC. Using dynamic mechanical analysis, fibre-matrix adhesion of WPC was investigated, and activation energies for glass transition of selected formulations were calculated. Activation energy for formulations containing MAPP was higher than for WPC without MAPP. This indicates that better fibre-matrix adhesion was achieved in formulations with MAPP.     

CT-scanning and modelling of the capillary water uptake in aspen, oak and pine

This study utilises Computer Tomography (CT-scanning) to characterize the capillary water uptake in wood specimens. CT-scanning makes it possible to study the capillary rise of water as a function of height in wood specimens after a specific exposure time. The study has also included the development of a theoretical model, which determines the capillary characteristics of wood in relation to its structure. The model developed was tested using experimental results, considering the capillary suction height and the water content change after a specific time as boundary values. A comparison between the theoretical model and the experimental results shows that not all the cells in the wood samples take part in the capillary water transport. It also appears that there is a structural resistance to capillary flow.     

An assessment of Malaysian wooden furniture manufacturers’ readiness to embrace chain of custody (COC) certification

Although Malaysia is a major producer and exporter of wood products in the world, the status of wood products certification in the industry is relatively unknown. Therefore, a study was carried out to assess the status of chain of custody certification among wooden furniture manufacturers using a structured questionnaire to interview firms who had participated at the annual Malaysian International Furniture Fair (MIFF). Results collated indicate that the readiness to adopt chain of custody certification among wooden furniture manufacturers was low. The lack of price premiums, limited market potential and high cost was cited as the primary reasons deterring furniture manufacturers from adopting chain of custody certification. Furthermore, the use of plantation wood resources, such as Rubberwood (Hevea brasiliensis), perceived to be certified wood resources, reflects the lack of understanding among the manufacturers. This study shows that an increasing adoption of chain of custody certification among wooden furniture manufacturers in Malaysia can be realized in the market organisation, especially with regards to price premiums and market requirements.     

Verklebung von Buchenholz für tragende Holzbauteile

The load bearing capacity of glulam could be enhanced by using lamella of European beech (Fagus sylvatica??L.). Essential requirements for the production of those beams are adhesives which allow for a durable und reliable bonding of lamella. The paper shows to what extent commercially available MUF and PU adhesives and adapted bonding parameters ensure gluing of European beech timber for load-bearing timber structures. Both beech wood containing heartwood and beech wood without heartwood were included in the study. With regard to technical approval, the chosen test methods were resistance to delamination according to EN??302-2 (2002) and shear test of glue line according to EN??392 (1995). From the two tested MUF systems it was evident, that delamination decreased by increasing the closed assembly time. The requirements of EN??301 (2006) were fulfilled for adhesive type??I and??II. Without any limitations beech wood containing heartwood could be glued using MUF-1. On the other hand, the results of the PU adhesive were insufficient. Light-optical micrograph examinations show that long assembly times secure the formation of a glue line. It was assumed that the curing process is retarded by beech wood. No relationship was found between the results of the shear strength test and the delamination test. For quality control of glulam the delamination test is recommended. Based on the positive results an application for technical approval of glulam consisting of beech was made. For this reason beech-glulam can be generally utilized in service class??1.     

Effect of radiata pine juvenile wood on the physical and mechanical properties of oriented strandboard

This work analyzes the impact of radiata pine (Pinus radiata D. Don) juvenile wood on the physical and mechanical properties of oriented strandboards (OSB). Radiata pine logs were obtained from 10 trees of a 26-year old managed stand located in the 8th Region of Chile. The experimental design considered the proportion of juvenile wood and strand orientation as independent variables. OSB panels of 0.4 m×0.4 m×12 mm were produced and tested. The results show that the juvenile wood proportion has a significant impact on the physical and mechanical properties of OSB. Strands orientation had a significant impact on all the properties studied with the exception of the modulus of elasticity in bending. However, this impact was small in all cases and would not change panel grade with the exception of linear expansion. In this case, panels made from tangential strands showed a higher linear expansion. According to these results, radiata pine juvenile wood can be used for the manufacturing of OSB up to a proportion of 70% of the oven-dry wood weight without significant losses of the physical and mechanical properties if the juvenile wood strands are located in the surface layers.     

Influence of vibration coupling between bandsaw frame and feed-carriage system on sawdust spillage and surface quality of workpiece during sawing

Productivity, surface quality, and recovery are three parameters that compete for attention during lumber production. The well known phenomenon of improved surface quality with decreasing workpiece feed rate has been reported by several researchers. This paper reports on experimental results from the relationship between workpiece feed rate or bite per tooth and the surface roughness of Japanese Sugi (Cryptomeria japonica) using a bandsaw machine whose feed-carriage is coupled to the bandsaw frame. The volume of sawdust produced during sawing was determined using an electronic balance. Equation was developed to determine the kerf-losses. It was observed that as the workpiece feed rate increased, or as the bite per tooth increased, the saw blade vibration decreased and the volume of sawdust also decreased contrary to expected results. Furthermore it was observed that with increasing workpiece feed rate the surface roughness decreased contrary to expected results. On the other hand, when the carriage feed rate increased the saw blade deviation also increased as expected. The research findings clearly suggest that when there is vibration coupling between the feed-carriage and the entire bandsaw frame, the amplitude of the saw blade vibration and the surface roughness decrease as the bite per tooth increases. Thus the bandsaw machine whose frame is coupled to the feed-carriage is a promising technique for increasing lumber recovery and improving upon surface quality.     

The effects of composition and carbon dioxide injection time on the properties of wood-cement composites

The effects of wood fiber/cement ratio, water/cement ratio and carbon dioxide injection time on the carbonation reaction and strength of wood-cement composites were evaluated. Increasing fiber content usually led to stronger composites and lower carbonation degree while increasing water amount decreased strength of composites in most cases. Either insufficient water or excessive water reduced carbonation reaction rate. There was a significant interaction effect between fiber content and water content, which had to be considered in optimizing the variables. Prolonging carbon dioxide injection time gradually increased carbonation degree, but did not affect the ultimate strength of composites. Process optimization was conducted according to the effects of the considered variables on the strength of composites. The validation experiment confirmed that the estimated optimal strength could be approximately obtained. Carbonated wood-cement composites performed much better than uncarbonated ones in conventional and accelerated ageing tests.     

A semi-automatic method to determine the wood failure percentage on shear test specimens

An alternative method to quantitatively determine the wood failure percentage on shear test specimens was developed, experimentally tested and successfully applied to specimens with typical combinations of adhesive types and wood species used by the glulam industry in Switzerland. The method consists of a staining technique for a better differentiation of wood fibers and adhesive, and an image processing procedure for a standardized estimation of the fractured surface ratio covered by wood fibers and adhesive, respectively. The semi-automatic method allows for a more objective determination of wood failure percentage and is suitable for quality control in the glulam industry.     

Bonding performance of heat treated wood with structural adhesives

Bonding of untreated, intermediate (hydro-thermolysed) and heat treated wood with melamine-urea-formaldehyde (MUF), phenol-resorcinol-formaldehyde (PRF) and polyurethane (PUR) adhesives was studied. An industrial heat treatment process (Plato ^®) was used, which included two separate heat treatment stages and a drying stage in-between. Laminated beams having four lamellas were prepared from untreated and treated timber for mechanical testing of the bond lines. The results of the tests showed that heat treatment affected the shear strength and the delamination of the laminated wood depending on the adhesive system used for bonding. The PUR and MUF adhesives performed in a rather similar way, and better than the PRF adhesive. The shear strength of laminated wood bonded with the waterborne MUF and PRF adhesives decreased for the specimens made of hydro-thermolysed timber and decreased further for the specimens made of fully heat treated timber. The difference in adhesive bond shear strength between untreated, intermediate and fully treated wood was less obvious in the case of the PUR adhesive. Delamination of the PRF bond line decreased drastically for all the specimens made of heat treated timber.     

Dimensional changes of beech wood resulting from three different re-wetting treatments

Several physical-mechanical properties of wood are evaluated from specimens in the green condition. Air-dry samples are often simply re-wetted by direct immersion in order to raise the moisture content above the fiber saturation point. It is assumed that this treatment has no effect on the properties of wood and is equivalent to the green condition. The purpose of this study was to evaluate the influence of water re-wetting processes on the dimensional properties in beech wood. Matched samples were subjected to three different full-water saturation treatments ranging from a four step mild procedure to a one-step drastic procedure. Results showed that the re-wetting process had a significant effect on swelling and shrinkage of beech wood.     

Wood surface discolouration due to simulated indoor sunlight exposure

Wood surface colour is a very important quality criterion in the utilisation of wood, especially in indoor applications. In this study, an attempt was made to analyse wood surface discolouration due to artificial indoor light irradiation of the most frequently traded wood species in Europe altogether. Sixteen wood species, twelve hardwood and four softwood species, were exposed for 120 hours to a xenon-arc lamp equipped with a 3 mm window glass filter, in order to simulate natural sunlight behind a window glass. Eleven wood species were chosen and further exposed to irradiation for up to 600 hours. Colour measurements were performed by means of a colorimeter device on exposed and non-exposed areas of the samples. Using the CIE-L*a*b* colour measuring system, wood surface discolouration was measured and calculated according to ?L*, ?a*, ?b* and ?E* values. An idea of the different behaviour of these species and how they relate to each other could be given.     

Up-milling and down-milling wood with different grain orientations – theoretical background and general appearance of the chips

Peripheral milling with up-milling and down-milling techniques is very well known from a geometrical point of view. However, in processing anisotropic materials such as wood these geometrical aspects imply relevant differences when machining. In fact milling anisotropic materials leads to different cutting geometries when up-milling or down-milling and when changing the depth of cut. This results in a relative orientation of the grain depending on the process adopted. In this paper the geometrical interactions between tool and wood grain have been analysed theoretically and supported by experimental evidence. To achieve this result, Douglas fir has been processed with different depths of cut and grain orientations, the resulting chips have been collected and analysed. The experiments show how a shift of the cutting phenomenon and the chip type can be observed to support the theoretical background.     

Wood shrinkage: influence of anatomy, cell wall architecture, chemical composition and cambial age

The influence of microfibril angle (MfA), density and chemical cell wall composition on shrinkage varied between the longitudinal and tangential directions as well as between wood types, namely compression wood (CW), mature wood (MW) and juvenile wood (JW). At the same MfA, CW exhibited a lower tangential shrinkage than JW, indicating the influence of the chemical composition on wood shrinkage. The chemical composition measured via FTIR micro-spectroscopy has been shown in conjunction with density to be an alternative to MfA data for shrinkage predictions. This was particularly true for wood of young cambial age for which the MfA did not correlate to shrinkage. The results indicate a possibility to reduce distortion of sawn timber by segregation using infrared (IR) and X-ray in-line measurements.     

Reliability of proof-loaded Norway spruce

Strength grading of structural timber is a prerequisite for the use of timber in load-bearing constructions. The grading methods used in production today are mainly based on estimation of the modulus of elasticity (MOE) determined from measurements of either flatwise bending stiffness or resonant vibrations. By using proof-loading techniques, the yield can be increased and the reliability of the graded material can be improved. Unfortunately, this technique can cause damage to some of the graded material. This paper deals with the quantification and severity of damage caused by proof-loading of Norway spruce (Picea abies) timber. A total of 410 specimens were loaded in cyclic bending with increasing load level in each cycle until failure. The maximum loads during the tests were compared to the failure loads of a reference sample. If the failure load was lower than the maximum load, the specimen was assumed to have been damaged in the previous load-cycle and was defined as a rogue. The technique used is similar to the technique used for example in Australia. The results obtained fit well with the results obtained from Australian species. Examination of the MOE indicates no damage in the specimens at stress levels below 75% of the strength. Damage is in this case defined as a decrease in the MOE. Regarding Norway spruce grown in Sweden it can be concluded that the problem of damage due to proof-loading is small for timber graded to strength classes C24 or C30. For both classes the number of rogues can be expected to be less than 5%. For timber graded to higher strength classes the problem of damage due to proof-loading will increase.     

Delaminierungseigenschaften und Scherfestigkeiten von verklebten rotkernigen Buchenholzlamellen

The paper deals with investigations on dry shear strength and delamination behavior of gluelines between beech wood laminations showing no or distinct red heartwood. The investigations covered 36 parameter combinations comprising besides the red heartwood two widths of the laminations, two different adhesive families and two delamination procedures related to verification of adhesive type I or II. The tests revealed no influence of red heartwood on shear strength which for all parameter combinations exceeded almost throughout 10 N/mm². In contrary thereto the delamination tests revealed a distinct dependency of the glueline integrity on red heartwood and width of the adherents. No parameter combination conformed to the requirements of adhesive type I. In case of laminations without red heartwood the requirements of adhesive type II were met. Gluelines between two laminations with red heartwood showed throughout very pronounced delamination above 50%. The integrity of gluelines versus delamination represents one of the essential normative requirements for adhesives used in glued load bearing wooden elements. This proof was not possible for gluelines of beech wood laminations with red heartwood when applying today’s European delamination test procedures and performance requirements developed and established for gluelines of softwood laminations.     

Thermal conductivity and water vapour transmission properties of wood-based materials

For several wood-based materials (plywood, OSB, melamine faced board (MFB), particle board and fibre board), the thermal conductivity was determined as a function of the temperature (ranging between 10 and 30 °C) and also the moisture content (from an oven-dry sample up to a moisture content at 80% RH). Furthermore, the water vapour resistance factor of these materials as well as of the coating (at MFB) and the diffusion coefficient were determined under dry cup (performance at low humidity dominated by vapour diffusion) and wet cup (performance at high humidity with liquid water and vapour transport) conditions. Thermal conductivity increases with rising temperature, moisture content and density. Moreover, a clear decrease of thermal conductivity was found with decreasing particle size at the same density level, from solid wood over plywood and particle board to fibre board. The water vapour resistance factor of the wood-based materials increases with rising density and decreases with increasing moisture content. An influence of the particle and fibre board thickness was also revealed. In contrast to the remaining materials, an increase of the water vapour resistance factor with increasing moisture content was measured for the coating. The diffusion coefficient decreases with rising density and moisture content.     

Ring width, latewood proportion and dry density in stems of Pinus brutia Ten.

This study examined basic characteristics of stem wood produced in Pinus brutia Ten. reforestations in Northeastern Greece. Sixteen dominant trees growing at good and medium site qualities were felled at 14–22 years. Site quality classification was based on site quality surrogates and confirmed by using site index curves that were created for a neighbouring area. Discs were taken at three stem positions (base, middle, top) to study variations in ring width, latewood proportion and dry density. Generally, at both good and medium sites, ring width was found to increase towards the top of the stems while latewood proportion and dry density showed a negative relationship with stem height. Radial variability trends were similar at all heights, and at both sites, revealing a rapid increase for ring width in the first 3–6 annual rings followed by a decrease towards the bark, a gradual increase for latewood proportion and no specific change for dry density. Comparisons between wood material produced during the same growth period (2005–2001) showed statistically significant differences among sampling heights in all cases except for dry density in medium sites. At the base of the stems, mean ring width and dry density were significantly (P?≤0.05) higher at good sites (3.6 mm and 0.53 g/cm³) than at medium sites (3.0 mm and 0.50 g/cm³). However, the differences between the sites are of small magnitude and therefore have limited practical impact on wood processing. The availability of such data is useful in utilising small-dimension timber of brutia pine.