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实验重点探讨了高含量碳对除尘灰样品中镁、铝、钾、钙、铬、锰、铜、钡、铅、镉、锌等元素测定的影响,并解决了除碳的问题。样品使用马弗炉高温除碳,采用盐酸-硝酸-氢氟酸-高氯酸消解样品灰分,选择了镁、铝、钾、钙、铬、锰、铜、钡、铅、镉、锌等元素的分析谱线和扣背景模式,建立了使用电感耦合等离子体原子发射光谱法(ICP-AES)测定高碳除尘灰中镁、铝、钾、钙、铬、锰、铜、钡、铅、镉、锌等元素的方法。在仪器最佳工作条件下,各元素校准曲线线性相关系数r均大于0.999 5,方法检出限在1.08~26.01 mg/kg之间。方法应用于除尘灰实际样品中镁、铝、钾、钙、铬、锰、铜、钡、铅、镉、锌的测定,结果的相对标准偏差(RSD,n=11)为0.90%~7.1%,目标元素的加标回收率为90%~117%;按照实验方法测定除尘灰中镁、铝、钾、钙、锌,结果与火焰原子吸收光谱法(FAAS)的测定结果相吻合。 相似文献
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采用11种与因瓦合金成分含量相接近的镍基合金标准样品绘制校准曲线,建立了基本不需要样品处理即可对因瓦合金中14种元素(C、Si、Mn、P、S、Ni、Cr、Mo、Cu、Al、Nb、Ti、Co、Fe)同时测定的辉光放电光谱法。确定辉光光谱仪检测因瓦合金的最佳条件:模块电压和相电压分别为8.22 V和3.82 V;功率为70 W;冲洗时间为80 s;积分时间为60 s。以各元素质量分数为横坐标,其对应的光谱强度为纵坐标绘制校准曲线,各元素校准曲线的相关系数均在0.99以上。采用实验方法对因瓦合金实际样品进行分析,结果显示:Cr、Ni、Mo、Ti、Fe的质量分数均大于0.3%,各元素测定值的相对标准偏差(RSD,n=11)均不大于1%;C、Si、Mn、P、S、Cu、Al、Nb、Co的质量分数均小于0.3%,各元素测定值的RSD(n=11)均小于5%。将实验方法应用于对因瓦合金样品中14种元素的测定,测得结果与滴定法测定Ni和Fe、高频燃烧红外吸收法测定C和S、电感耦合等离子体原子发射光谱法测定Si、Mn、P、Cr、Mo、Cu、Al、Nb、Ti和Co元素的结果基本一致。 相似文献
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《不锈(市场与信息)》2009,(24):1-2
国家拟出台进一步加强淘汰落后产能工作的通知,协调发改委、工信部、环保部、国土部、商务部、海关总署、财政部、央行、银监会、质检总局、安监总局、工商总局、电监会、能源局等,以严厉措施,重点完成电力、煤炭、钢铁、水泥、有色、焦炭、造纸、皮革、 相似文献
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Bimaterial interfaces present in diffusion-bonded (and in-situ) composites are often not flat interfaces. The unevenness of the interface can result not only from interface reaction products
but also from long-range waviness associated with the surfaces of the component phases bonded together. Experimental studies
aimed at determining interface mechanical properties generally ignore the departure in the local stress due to waviness and
assume a theoretically flat interface. Furthermore, the commonly used testing methods involving superimposed tension often
renders the interface so extremely brittle that if microplastic effects were present it becomes impossible to perceive them.
This article examines the role of waviness of the interface and microplastic effects on crack initiation. To do this, a test
was selected that provides significant stability against crack growth by superimposing compressive stresses. Mode II interface
fracture was studied for NiAl/Mo model laminates using a recently developed asymmetrically loaded shear (ALS) interface shear
test. The ALS test may be viewed as opposite of the laminate bend test. In the bend test, shear at the interface is created
via tension on one surface of the bend, while in the ALS test, shear is created by compression on one side of the interface relative
to the other. Normal to the interface, near the crack tip, an initially compressive state is replaced by slight tension due
to Poisson’s expansion of the unbonded part of the compressed beam. 相似文献
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Q Geng 《Canadian Metallurgical Quarterly》1993,60(1):35-53
In the impression-taking procedure for the distal extension removable partial denture, the pressure produced at the interface of the soft mucosal tissue and the impression material is the most important factor for the stability of the saddle under functional load. However, a review of the literature revealed little information about the displacement of the soft tissue caused by the impression pressure. In the present study, to investigate the influence of various impression procedures on the magnitude of the soft tissue displacement more precisely, a new three-dimensional deformation measurement system was devised. Compared to the previous studies, the greatest advantage of the system is that the hardened impression material can be surveyed directly without substituting a dental stone. It was found that, in the investigation using a partially edentulous simulated model, the amount of the subsidence in the soft tissue was increased as the thickness of the spacer of the impression tray was reduced or the seating speed of the tray was fast. Especially in the buccal area, a large amount of vertical displacement was present compared to the midridge and lingual area. Thus it was suggested that many factors are associated with the form of soft tissue under impression loading. 相似文献
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JA Shaw 《Canadian Metallurgical Quarterly》1995,10(4):438-447
A prosthetic tibial component has been designed with features for fixation to bone using a combination of acrylic cement and ingrowth interfaces. This hybrid concept affords the component the immediate stability of cement fixation and the potential long-term stability of biologic fixation. The ingrowth interfaces (coupled with the central stem) are intended to shield the cement interface beneath the tibial tray from the tensile liftoff forces that result from eccentric loading, while avoiding the fretting and osteolysis associated with screw fixation. A disassembly capability allows the tray to be removed from the stemmed anchorage assembly, facilitating component extraction and limiting bone loss. A clinical and radiographic review of 50 consecutive primary total knee arthroplasties with a mean follow-up period of 35 months revealed stable interfaces with no progressive radiolucencies and minimal remodeling changes. The mean Knee Society knee score was 92.2. At final follow-up evaluation, 88.6% of patients noted no or mild (occasional) pain. Retrieval of three prosthetic knees with chronic sepsis showed extensive ingrowth into the porous interfaces and an osteointegrated bony sleave around the smooth central stem. 相似文献
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文章利用三维建模软件对结构复杂的卡罗塞尔卷取机大转盘进行了建模。在此基础上,利用有限元分析软件ANSYS对大转盘进行了最恶劣工况下的力学分析,直观展现了大转盘存在的应力、应变,为掌握卡罗塞尔卷取机的力学性能提供了可靠的理论分析依据。 相似文献
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The development of dendrites from an initially flat, stationary solid/liquid interface in a transparent material was observed
and photographed. It was found that the dendrites originated from preferred areas on the interface immediately adjacent to
grain boundaries, subboundaries, and trapped foreign particles. The built-in large-amplitude distortions of the interface
adjacent to these imperfections initiated dendritic growth under conditions which did not produce dendritic growth on imperfection-free
regions of the interface. It is concluded that considerations of the stability of planar interfaces must take into account
the influence of the imperfections which are present in almost all solids. 相似文献
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基于ZnO结瘤下SiC塔盘导热性能研究探讨 总被引:5,自引:0,他引:5
为了研究韶关冶炼厂铅塔燃烧室SiC塔盘的外壁在存在ZnO结瘤层下的导热性能 ,根据ZnO结瘤层的不同厚度 ,并结合对塔盘的热工测试 ,对铅塔燃烧室烟气向ZnO结瘤层的外表面的辐射传热以及通过ZnO结瘤层导入塔盘内的热量进行了详细的分析和推导 ,结果发现 :随着ZnO结瘤层的增加 ,ZnO结瘤层外表面的温度升高 ,而沿ZnO结瘤层传入塔盘内的热量急剧减少。当ZnO结瘤层厚度为 3 0mm时 ,传入塔盘内的热量为未结瘤时的 3 0 3 4%。这种情况将在很大程度上减少锌蒸气的产量以及降低锌蒸气的质量 相似文献
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A coordinate measurement machine with laser probe was used to measure the vertical distortion of the casts produced by use of three types of impression materials (irreversible hydrocolloid, condensation silicone, and addition silicone) and two types of trays (stock and custom trays). Results indicated that all impression groups showed positive vertical distortion (ranging from 0.00566 to 0.30299 mm) at the edentulous ridges and palatal area. The amount of the vertical distortion was greatest at the palatal area and was followed by the high edentulous ridge and the low edentulous ridge. Addition silicone, with either custom tray or stock tray, was the most accurate impression material. Condensation silicone was more accurate than irreversible hydrocolloid in custom tray impression. However, in stock tray impression the irreversible hydrocolloid was more accurate than the condensation silicone. The results suggest that, with careful manipulation, irreversible hydrocolloid with stock tray impression may provide a satisfactory cast for fabricating the framework of a distal extension removable partial denture. 相似文献
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R Largo D Gómez-Garre S Santos C Pe?aranda J Blanco P Esbrit J Egido 《Canadian Metallurgical Quarterly》1999,55(1):82-90
The effect of a meniscal bearing on knee laxity in anterior cruciate ligament-sacrificing total knee arthroplasty was evaluated in 7 cadaver knees using a knee testing device that measured knee flexion angle as well as laxity to medial-lateral, anterior-posterior [AP], and rotational loads. A standard fixed tibial component and mobile tibial components (AP sliding, rotationally sliding, and AP and rotationally sliding) were used to evaluate AP, rotational, and varus-valgus stability and maximal flexion and extension with the neutrally positioned and malrotated tibial tray. The AP movable components increased AP laxity, and the fixed component decreased rotational laxity significantly when compared with the normal knees. The rotationally movable components did not change knee laxities significantly even when the tibial tray was malrotated. No significant difference among the components was detected when the maximal flexion and extension angles were compared in the neutrally positioned tibial tray. Malrotation of the tibial tray decreased the maximal extension angle in the fixed component. This study showed that the rotationally movable component can achieve near-normal laxity regardless of tibial tray rotation, but AP mobility of the bearing produces AP laxity that could lead to implant failure. 相似文献