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水煤浆气化有效气含量与粉煤气化相比,有一定差距,主要原因是水煤浆浓度偏低,气化时带进多余的水而造成。提高水煤浆浓度是提高水煤浆气化有效气含量的关键。介绍了近年来国家水煤浆工程技术研究中心开发的气化水煤浆提浓新技术,包括分级研磨制浆技术和间断粒度级配制浆技术。介绍了两种制浆技术的原理及工艺流程,工业应用及中石化联合会的科技成果鉴定表明,与常规制浆工艺采用同种煤制备的煤浆浓度相比,分级研磨制浆技术煤浆质量分数提高3个百分点左右;间断粒度级配制浆技术煤浆质量分数提高6~8个百分点。 相似文献
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《中氮肥》2019,(2)
水煤浆浓度是多元料浆气化装置的关键工艺指标之一,水煤浆浓度的高低在很大程度上决定着水煤浆气化装置的运行效率与经济性。而水煤浆浓度的提升是一项涉及面广、影响因素较多的系统工程。从水煤浆的基本特性(流变特性、稳定性、煤炭颗粒粒度分布及含量等)入手,分析原料煤煤质、煤炭颗粒粒度级配、制浆工艺与设备、制浆添加剂及辅助剂等对水煤浆浓度的影响。在总结3种煤浆提浓工艺特点的基础上,陕西陕化煤化工集团有限公司在其多元料浆气化装置低压煤浆泵出口通过增设1条煤浆回流管线(并设置相应的冲洗水管线)将部分产品水煤浆返回磨机进行二次研磨,制备出高浓度、低粘度、流变性能良好的水煤浆——水煤浆浓度由60.0%提至62.8%、水煤浆粘度基本稳定在600~1 200 cP,并克服了生产中出现的一些问题,实现了系统的稳定运行。 相似文献
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水煤浆黏度的几种影响因素分析 总被引:6,自引:4,他引:2
研究了矿物质、粒度分布和搅拌强度对水煤浆黏度的影响.结果表明,实验使用的3种矿物质——高岭土、氧化铝和碳酸钙在降低水煤浆的黏度方面效果都比较明显,其中高岭土最显著,可以使黄陵水煤浆的黏度降低59.5%左右.适当的粒度级能有效改善浆体黏度,剪切率为116.5s-1时,枣庄煤级配制备的水煤浆的黏度值在820mPa·s~900mPa·s之间,而神准混煤级配制备的煤浆黏度值更低,处于500mPa·s~670mPa·s之间.同时搅拌强度的增加在一定范围内可以有效降低煤浆的黏度. 相似文献
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《耐火材料》2018,(3)
为了研究不同研磨设备及研磨工艺参数对粉体团聚体的解聚效果,以d50=1.355μm的氧化锆粉体为研究对象,研究了研磨设备和工艺参数对氧化锆料浆粒度的影响。首先,分别采用立式球磨机、立式珠磨机和卧式砂磨机为研磨设备,以φ2 mm的氧化锆球作为研磨介质,以m介质∶m物料=5∶1的介质物料比研磨15 h后,检测研磨后氧化锆料浆的粒度。结果表明,卧式砂磨机的研磨效果最优,研磨后氧化锆料浆的d50=0.303μm。然后,采用卧式砂磨机为研磨设备,以φ2 mm的氧化锆球作为研磨介质,选择介质物料比(m介质∶m物料)、料浆固含量(w)、线速度和研磨时间作为试验因素,进行四因素三水平(m介质∶m物料分别为4∶1、5∶1和6∶1,料浆固含量(w)分别为35%、45%和55%,线速度分别为5、10和15 m·s-1,研磨时间分别为20、25和30 h)正交试验,检测研磨后氧化锆料浆的粒度。结果表明:采用卧式砂磨机为研磨设备,当介质物料比(m介质∶m物料)为4∶1,料浆固含量(w)为45%,线速度为10 m·s-1,研磨时间为25 h时,研磨效果最佳,研磨后氧化锆料浆的d50约为0.3μm。 相似文献
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在对彬长矿区侏罗纪煤进行煤质分析和灰成分分析的基础上,探讨了煤的粒度、级配、添加剂类型与加入量、料浆流变性能等参数对煤成浆性的影响,确定了基于该煤样用于气化的高浓度水煤浆实验室最佳配方。 相似文献
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李峰军 《煤炭加工与综合利用》2014,(4):70-72
棒磨机的钢棒装填量和钢棒的级配直接影响水煤浆的粒度分布,而粒度分布又是影响水煤浆粘度的重要因素之一,通过水煤浆成浆性试验摸索棒磨机的钢棒装填量及级配,从而生产出浓度、粘度、粒度分布合格的水煤浆。 相似文献
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《化学工业与工程技术》2016,(2):12-14
以宁东煤为研究对象,采用正交试验法进行了煤粉粒度分布对水煤浆成浆性能影响的分析研究。自制了不同颗粒区间的煤粉,并将各种粒径的煤粉配制成相同浓度的水煤浆,以水煤浆的黏度和流动性作为试验指标,探讨了不同粒度级配对宁东煤成浆性的影响。采用超声衰减粒度仪进行了粒度分布测定,并得到了分布曲线。试验结果表明:双峰级配的煤粉粒度级配合理,大颗粒和小颗粒之间相互填充,煤粉堆积效率达到最大,煤粉空隙中的水量最小,表现为浆体的黏度低、流动性好。 相似文献
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棒磨机的钢棒充填量及钢棒级配直接影响水煤浆的粒度分布,而粒度分布又是影响煤浆成浆性能的主要因素。通过工业试验摸索棒磨机的钢棒充填量及级配,从而生产出粒度分布合格的水煤浆。 相似文献
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群青颜料的球磨及改性研究 总被引:1,自引:0,他引:1
采用实验室自制球磨机,以乙醇为溶剂对群青颜料进行球磨,制备了不同粒径的群青颜料色浆,用于随后的改性研究.分析了球磨时间、球料比、色浆浓度、分散剂用量、磨球大小和级配对群青颜料粒径及其分布的影响.用硅烷偶联剂3-氨丙基三乙氧基硅炕(APTEs)对不同粒径群青颜料进行表面改性,探讨了改性颜料粒径大小与体系稳定性、印花性能的关系.实验结果表明,颜料粒径越小,体系分散稳定性越好;改性后颜料耐酸性随粒径减小而降低;印花织物的干摩擦牢度随粒径减小而升高,但湿摩擦牢度随粒径减小有降低的趋势. 相似文献
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为了研究粒度级配对神华煤成浆特性的影响,通过筛分和干法调浆,探讨了不同粒度分布煤粉的成浆性,结果表明:在添加剂用量为0.3%(干基/干煤)时,具有连续级配特征的原始煤粉可制备出质量分数为61%的煤浆;利用筛分法,分别去除原始煤粉中0.045 mm以下、0.045 mm^0.15 mm、0.15 mm^0.3 mm和0.045 mm^0.3 mm部分,得到4种具有不连续级配特征的样品,其所制煤浆流变性发生了较大变化,其中去除0.045 mm^0.3 mm部分的样品的成浆质量分数提高了3个百分点,在黏度符合要求的前提下流动性大幅提高;连续级配和非连续级配的煤浆均存在黏度与流动性不统一的现象,当级配中粗细颗粒粒径差较大且细颗粒含量达到一定值时,这种现象更加明显。采用粒度级配技术制浆,其细颗粒含量存在一个合理的区间。 相似文献
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Effect of ball size and powder loading on the milling efficiency of a laboratory-scale wet ball mill
Alumina powder was wet-milled by zirconia balls with varying diameter at varying rotation speed, and the resultant particle size of the milled powder was analyzed. At a given rotation speed, there exists an optimum ball size to yield minimum particle size of alumina. The optimum ball diameter decreases as the rotation speed increases. This result has been interpreted in light of the competition between the reduced kinetic energy of the smaller balls (a negative source for milling efficiency) and the increased number of contact points of the smaller balls (a positive source), which yields the optimum ball diameter at an intermediate size. As the rotation speed increases, kinetic energy of the balls increases, which, in turn, shifts the optimum ball size toward a smaller value. As the powder loading increases from 1 to 35 g at a given rotation speed and ball size, the milling efficiency decreases monotonically. 相似文献
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Nano powder of natural clinoptilolite zeolite was mechanically prepared by using a planetary ball mill. Statistical experimental design was applied to optimize wet and dry milling of clinoptilolite zeolite. To determine appropriate milling conditions with respect to the final product crystallinity, particle size and distribution, different milling parameters such as dry and wet milling durations, rotational speed, balls to powder ratio and water to powder ratio (for the wet milling) were investigated. Laser beam scattering technique, scanning electron microscopy and X-ray diffraction analyses were carried out to characterize samples. Results showed that larger than 1 mm particle size of clinoptilolite powder may mechanically be reduced into the size range of less than 100 nm to 30 μm by means of planetary ball milling. 相似文献
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Nafiseh Rezaei Rutendo Leah Mutambanengwe Brant Anthony Peppley 《Ceramics International》2021,47(11):15464-15470
Tantalum carbide (TaC) is investigated as a potential support for oxygen evolution reaction electrocatalysts. It is ball milled with zirconia balls for 7 and 14 days. The particle size and surface area of the ball milled TaC are analyzed using scanning electron microscopy and nitrogen physisorption methods, respectively. After 14 days of ball milling, the TaC shows smaller particle size and larger surface area compared to after 7 days of ball milling and unmilled TaC. The long-term electrochemical stability of the ball milled TaC is evaluated under oxygen evolution reaction conditions using cyclic voltammetry and chronoamperometry. The ball milled support at a fixed voltage of 1.6 V is shown to be stable up to 5000 cycles. Chronoamperometric measurement also shows the ball milled TaC remains stable over the 70 h of the test. 相似文献
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Two types of ball milling methods, wet planetary ball milling and dry tumbling ball milling, were used to grind fused silica powders for the preparation of silica-based suspensions in this experiment. The effect of surface hydration and particle shape caused by the two milling methods on the slurry rheology was investigated. The results showed that, with similar particle size distribution, the viscosity of the suspensions prepared from the powders milled by wet ball milling ranged from 275 mPa s to 311 mPa s within 20 min and the suspension exhibited a continuous shear thickening behaviour whereas the viscosity of the suspensions prepared from the powders milled by dry ball milling ranged from 69 mPa s to 74 mPa s and the suspension exhibited a shear thinning behaviour first, and then exhibited a slightly shear thickening behaviour. The reasons were attributed to the differences in surface hydration and particle shape. It was postulated that the two factors affected the slurry rheology through the modification of particle interactions during the flow of high concentration suspensions. 相似文献
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针对伊泰煤制油有限公司160kt/a煤制油项目气化装置制浆工艺存在的煤浆粒度级配不合理、煤浆浓度偏低等实际问题,对煤浆提浓工艺及细磨机结构进行优化和改进,实现了煤浆提浓系统及关键设备的稳定可靠运行,煤浆浓度和气化炉运行指标明显改善。 相似文献
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