Dual-motion fretting behavior of mandibular cortical bone against pure titanium

Dual-motion fretting tests of flat cortical bone specimens from fresh human mandible against pure titanium (TA2) ball were carried out on a modified test rig with tilt angle of 45°. The imposed maximal loads varied from 100 to 200 N. Dynamic characteristics of dual-motion fretting tests were analyzed in combination with micro-examinations via optical microscopy (OM), laser confocal scanning microscopy (LCSM) and scanning electron microscopy (SEM) together with energy dispersive X-ray spectrum (EDX). Two types of F-D curves (the trapezoid and elliptic mode) were recorded during the tests. The examination showed that the wear scars of the dual-motion fretting were asymmetric, and the tangential component of dual-motion fretting was in the mixed fretting regime. Under the lower imposed load, only some detachment of particles and scratches without cracking were observed even after 5×10⁴ cycles. The main wear mechanisms of the dual-motion fretting damage were the abrasive and adhesive wear. Under higher imposed loads, the cracks initiated and propagated mainly at the high stress side of contact edges. The wear mechanisms of the dual-motion fretting of cortical bone under higher imposed loads were the combination of the adhesive wear, abrasive wear, cracking and lubrication of the human bone tissue debris. And the lubrication of the debris played an important role during the dual-motion fretting processes.     

On the mechanisms of various fretting wear modes

According to relative motion directions for a ball-on-flat contact, there are four fundamental fretting wear modes, e.g., tangential, radial, torsional and rotational modes. In this paper, the mechanisms of these four fundamental fretting wear modes, particularly for the later three modes, have been reviewed from results obtained by the authors in combination with results from literature. Some general features have been reported. Differences both in running and degradation behavior have been discussed in detail. Results showed that some similar laws for three fretting regimes (partial slip regime, mixed regime and slip regime), fretting maps (running condition fretting map and material response fretting map), wear and cracking mechanisms obtained from the classic mode (i.e. tangential fretting) were also identified and useful to characterize the other modes. Nevertheless, the occurrence of relative slip for the radial fretting, the formation of mixed regime for the torsional fretting, the evolution of surface morphology for the rotational fretting were quite different compared to that of the classical fretting mode.     

Investigation of micro-cracking behaviors of human femur cortical bone during radial fretting

Radial fretting tests on human femur cortical bone with a ball-on-flat configuration were carried out in vitro under different normal contact loads. The kinetics behaviors and damage characteristics of the cortical bone were analyzed using the load versus displacement (F-D) curves. The fretting scars were examined using laser confocal scanning microscopy (LCSM) and scanning electron microscopy (SEM). A nano-indenter was used to characterize the mechanical property of the osteon of the cortical bone. Morphologies showed that the primary damage form was due to micro-cracking. Around the osteon, three kinds of micro-crack configurations were observed; i.e. annular cracks—located at the concentric lamellae; radial cracks—initiated from the Harversion canal; and interstitial cracks—initiated and propagated between the interstitial lamellae. Plenty of interstitial cracks occurred in the wear scar, which indicated that the interstitial tissue was the weak zone in the structure of cortical bone. In addition, the contact stresses under the radial fretting condition were calculated by the finite element method analysis (FEMs) and the behaviors of cracking were explained. The results demonstrated that the stress concentration that occurred around the Harversian canal and osteon system resulted in a better resistance than that from the interstitial tissue. The concentric lamellae presented a better radial-fretting resistance and contact fatigue resistance than that from the interstitial lamellae.     

人体皮质骨/纯钛接触副径向微动损伤研究

对新鲜人股骨皮质骨对纯钛球(直径10mm)接触副,在12mm/min加载速度下,分别以最大法向载荷100,200,300,400N进行径向微动实验研究。在动力学特性分析的基础上,用激光共聚焦显微镜和扫描电镜观察皮质骨表面的磨痕形貌。结果显示:随着载荷的增加,股骨皮质骨表现出不同的界面变形行为,损伤随之加重,而且裂纹的产生存在一个临界载荷;裂纹在骨表面主要有4种生长方式,以沿粘合线生长最常见。讨论了减缓骨/种植体界面径向微动损伤的措施,表明降低界面应力和种植体表面改性有利于减缓骨/种植体界面径向微动损伤。     

An experimental study on radial fretting behaviour

A new test apparatus has been developed for radial fretting test. Main experimental conditions are as follows: the amplitude of normal load from 200 to 800N, the number of cycles from 1 to 3×10⁵ cycles. Three contact pairs (a 52100 ball against 52100, 1045, 1045 steel with TiN coating) were used for the test. Variations of normal load vs indentation depth between two contact surfaces have been analyzed as a function of cycles. Contact degradation was examined through metallographic expertise on the flat specimen and radial fretting behaviour was compared in the paper.     

Characterization of friction-induced local convex topography under dual-rotary fretting

Dual-rotary fretting (DRF) is a complex fretting wear mode combining torsional fretting with rotational fretting. Two different typical friction-induced convex topographies (Type I and Type II) in contact area were showed, which are under the control of torsional and rotational fretting components, respectively. To investigate their evolution characteristics and formation mechanism, the convex topographies were analyzed by SEM, XPS, a nano-hardness tester and surface profilometry, etc. The results show that the convex topographies significantly depended on the test parameters and environmental conditions. The initiation and propagation of fretting fatigue cracks were found related with the convex topography under the fretting wear.     

Radial fretting fatigue damage of surface coatings

Radial fretting tests with a 52100 steel ball-on-flat contact have been carried out under different normal loads. TiN, MoS₂ and TiN+MoS₂ coatings on a 1045 steel flat were examined. The normal loads amplitude used were 200, 400 and 800 N at speeds of 12 and 1.2 mm/min. Dynamic analysis in combination with microscopic examinations by SEM and EDX have been performed. It was observed that the vertical stiffness increased with the increase of loading speed and number of cycles. The metallographic examinations showed that little damage was observed for the MoS₂ coating, which exhibited excellent radial fretting fatigue resistance. For the TiN coating, micro-cracks appeared at the lower load while delamination occurred at the higher load. For the TiN+MoS₂ composite coating, the vertical stiffness increased but accompanied by some micro-cracks. As a result of the study, the radial fretting test is proposed as one possible new method to evaluate coating life.     

An experimental study torsional fretting behaviors of LZ50 steel

Four simple fretting modes are defined according to relative motion: tangential, radial, rotational, and torsional fretting. This paper presents a new test rig that was developed from a low-speed reciprocating rotary system to show torsional fretting wear under ball-on-flat contact. Torsional fretting behavior was investigated for LZ50 steel flats against AISI52100 steel balls under various angular displacement amplitudes and normal loads. The friction torques and dissipation energy were analyzed in detail. Two types of T–θ curves in the shape of quasi-parallelograms and ellipticals were found that correspond to gross and partial slips, respectively. The experimental results showed that the dynamic behavior and damage processes depend strongly on the normal loads, angular displacement amplitudes, and cycles. In this paper, the debris and oxidation behaviors and detachment of particles in partial and gross slip regimes are also discussed. Debris and oxidation are shown to have important roles during the torsional fretting processes. The wear mechanism of torsional fretting was a combination of abrasive and oxidative wear and delamination before third-body bed formation. The mechanism was then transformed into third-body wear after a great amount of debris formed.     

An experimental investigation on composite fretting mode

An apparatus for composite fretting tests on a steel ball opposite to the inclined steel flat with different inclined angles (60° and 45°) have been carried out. During the tests, the maximum imposed loads were varied from 200 N to 400 N and 800 N at a constant loading speed of 12 mm/min. Dynamic analysis in combination with microscopic examinations through optical microscopy, profilometery, and SEM have been performed. Composite fretting behaviour has been analyzed and compared with the conventional fretting.     

Development of a test device for the evaluation of fretting in point contact

Fretting wear and fatigue may occur between any two contacting surfaces, wherever short‐amplitude reciprocating sliding is present for a large number of cycles. A test device has been developed for the evaluation of fretting fatigue and wear in partial and gross slip conditions. Three similar sphere‐on‐plane contacts run at the same time. Normal force, tangential force or displacement amplitude and constant bulk stress can be controlled and measured separately. Reciprocating tangential displacement is produced with rotational motion, the amplitude and frequency of which can be adjusted and controlled accurately by an electric shaker. The number of load cycles for crack initiation and growth is determined with strain‐gauge measurements near the fretting point of contact. The contact surfaces are measured with 3D optical profilometer before fretting measurements to determine actual contact geometry. The measurements were done with quenched and tempered steel. The initial results indicate that cracks are mostly formed in partial slip conditions, whereas fretting wear is more heavily involved in gross slip conditions. The initiation of a crack occurs near the edge of the contact in the slip direction, where the calculated cracking risk has its maximum value in partial slip conditions. The number of cracks increases as the displacement amplitude, i.e. friction force, increases in partial slip conditions. Copyright © 2008 John Wiley & Sons, Ltd.     

表面粗糙度对微动摩擦特性的影响

通过实验研究,探讨了表面粗糙度对微动摩擦特性影响的作用。表面粗糙高时接触表面之间的摩擦系数会有明显增加,在微动状态下表面粗糙度对表面磨损影响不大。     

690合金材料的微动磨损特性研究

利用微动磨损试验机,在载荷50N以及位移幅值为60μm、100μm、150μm的工况下,研究了690合金材料在常温下的微动磨损行为及其动力学特性,采用激光共焦扫描显微镜(LCSM)和扫描电子显微镜(SEM)观察磨痕微观形貌。结果表明,载荷和位移幅值对微动特征有很大的影响,微动运行完全处于滑移状态。在滑移区,滑移磨损严重、磨痕面积大。690合金材料的磨损机制主要表现为磨粒磨损与剥层的共同作用。     

An investigation of the fretting behaviour of low friction coatings on steel

Three different low friction coatings on steel (electrolytically deposited cadmium, PTFE solid lubricant in epoxy resin and PTFE solid lubricant in polyimide resin) were studied in order to relate their fretting behaviour with mechanical properties. Particular importance was given to adhesion which was measured using a scratch test. Fretting tests were carried out on the steel substrate and on the coatings under the same conditions. The major parameters of the tribological system were identified and then quantified. The values of the parameters obtained for each coating were compared with the corresponding values for uncoated steel. The mechanical characteristics of the coatings and their fretting parameters were plotted using a polar diagram in order to give an overview of the fretting behaviour of each coating. Differences were noted and the corresponding parameters were identified. The influence of the adherence of the coating and of the fretting test load on the lifetime of the coating was determined.     

Laboratory fretting tests with thin wire specimens

Wire ropes, due to their construction and application, are prone to fretting damages. In order to know the wear behaviour of individual wires under fretting conditions, laboratory tests are required. The present work describes the preliminary fretting tests accomplished with thin steel wires to optimise the testing procedure. The tests were carried out with ‘crossed‐cylinders’ configuration varying the stroke and normal load. Afterwards, the fretted surfaces were characterised by means of an optical and scanning electron microscope, and a diamond stylus. No significant influence of selected parameters was detected and a good correlation was proved for on‐line measured parameters and off‐line obtained values. Copyright © 2007 John Wiley & Sons, Ltd.     

圆弧端齿结构微动疲劳试验加载装置的设计及实现

针对圆弧端齿结构三维微动疲劳试验难度大、成本高等问题,提出了一种二维等效加载方案,设计并实现了微动疲劳试验加载装置,建立了二维结构微动疲劳试验模型。对典型圆弧端齿结构的二维等效试件进行了微动疲劳试验,发现疲劳裂纹萌生于接触面的接触边缘,接触面出现大量微动磨屑,为典型的微动疲劳失效形式。试验结果表明,该微动疲劳试验加载装置可满足端齿结构微动疲劳试验要求,为微动损伤机理分析和微动疲劳寿命预测提供了试验数据支持。     

Radial fretting behaviours of dental ceramics

Radial fretting tests on a Si₃N₄ ceramics ball opposite to the two dental ceramics flats (Vita VMK95 and Cerec Vita Mark II) have been carried out. The test apparatus was developed from a tension-compression hydraulic machine. Maximum normal load (F_max) was varied from 100 to 800 N with a speed of 6 mm/min, and the number of cycles from 1 to 10⁵. The fretting scars were examined by optical microscope and laser confocal scanning microscope (LCSM). The results of kinetics behaviours showed that all loading and unloading curves of load (F)–displacement (D) curves were almost superposed in the whole fretting process for two dental ceramics under a lower normal load (), and all F–D curves opened, correspondingly some micro-cracks initiated and developed in contact area, when the normal load increased to a higher level (). Under lower normal load, the fretting scars displayed the worn zones in shape of annulus. The cracks in shape of homocentric circularity can be observed for Vita VMK95 at and for Cerec Vita Mark II at . Therefore, there is better radial fretting damage resistance for Cerec Vita Mark II. In the microslip zone, the microscopic analysis showed that the particles detached by the mechanism of delamination. It the meantime, the competing mechanisms of fatigue cracks and wear also were discussed in this paper.     

Design effects on the fretting wear behaviour of ball bearings

A change in design of a ball bearing is described based on the results of numerical and experimental analysis to reduce fretting wear. Increasing the radii of curvature of the inner and outer races by a small amount reduces the product of the relative slip δ and the tangential traction τ at the contact region, both of which are caused by Heathcote slip. This results in the consequent reduction in fretting wear because there is a good correlation between the amount of fretting wear and τδ. This prediction is confirmed experimentally by increasing the groove radius of the inner race from 4.02 to 4.21 mm for a ball of radius 3.97 mm.     

The lubrication effect of hyaluronic acid and chondroitin sulfate on the natural temporomandibular cartilage under torsional fretting wear

The aim of this study is to investigate the lubrication of hyaluronic acid (HA) and chondroitin sulfate (CS) on the condylar cartilage of the temporomandibular joint. The wear behaviour of bovine condyle cartilage was explored against a zirconia ball with different lubrications under torsional fretting mode. The worn cartilage morphologies were observed using scanning electron microscopy and hemotoxylin and eosin staining. The results indicated that HA or CS could significantly lower the friction torque and dissipated energy of fretting interface and reduce the damage of the articular cartilage surface compared to the control (phosphate‐buffered saline). The mixture (HA and CS) could provide better protection for the cartilage layer. Absence of good lubrication in overloading torsional fretting process caused excessive cartilage wear. High concentration and high molecular weight HA or CS acted as good boundary lubricants, and the lubrication effect of their mixture was better due to their synergistic function. Copyright © 2014 John Wiley & Sons, Ltd.     

Nanoscale fretting wear study by scanning probe microscopy

Nanoscale fretting wear was studied by using scanning probe microscopy (SPM) and a newly proposed unified approach of slip index. The production of SiO₂ colloidal probes and the SPM calibration are described. Partial and gross slip fretting with displacement amplitudes from 5 to 500 nm were used for the study. Friction coefficient and nanowear results are presented showing a substantial increase of the friction at the transition from partial to gross slip and a significant difference between damaged surfaces in the two fretting regimes.     

A study of tribopolymerisation under fretting contact conditions

The present study is aimed at determining whether or not tribopolymerisation can occur under conditions of fretting contact. Using a high contact stress system consisting of oscillating metal balls loaded against flat steel discs, effects of various monomers on friction, wear, and surface film formation were determined. Monomers were used at 1% concentration in hexadecane. Under the conditions used (90N load, 40 Hz frequency, 300 μm amplitude, for 1 hour), the monomers tested reduced friction or wear or both. Fourier Transform Infrared (FTIR) analysis of the test specimens showed that organic material is presented in the wear scars and depends on the metal system used, the monomer structure, location within the track, and the method of cleaning the surface after a test. With Al-on-steel, the addition of 1% styrene to hexadecane reduced volumetric wear of the disc by 65%; furthermore, positive FTIR evidence of polystyrene in the wear track was obtained. But adimer acid/glycol monomer formed metal soaps, no polymer, and had little effect on wear under these conditions. These results support the hypotheses that addition-type tribopolymerisation can be initiated by exoelectron emission. Additionally, it was found that not only does methyl methacrylate polymerise under the fretting conditions, but the polymer film formed also reacts with the friction contact surface. Taken as a whole, the results of this study of possible tribopolymerisation under fretting conditions support both major hypotheses, namely that: (i) for condensation-type monomers, the most important factor is the temperature of the rubbing surfaces. (ii) For addition-type monomers, it would appear that the effect of exoelectron emission can initiate surface polymerisation even at relatively low surface temperatures, e.g., 10–40°C above ambient. This is in agreement with the negative-ion-radical action mechanism (NIRAM) of boundary lubricant component. Finally, the results obtained in this study demonstrate that the principle of tribopolymerisation developed by Furey and Kajdas can be used as a novel and effective approach to designing specific molecular structures for boundary lubrication under various rubbing conditions.