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RP-HPLC法测定中成药中黄芩苷的含量 总被引:2,自引:0,他引:2
目的:采用高效液相色谱法测定复方鱼腥草片和清热解毒口服液中黄芩苷的含量,以测定其制剂的质量。方法:以C18化学键合硅胶柱分离黄芩苷,以甲醇-水-醋酸(49.5:50:0.5)为流动相,UV检测波长274nm进行测定。结果:理论塔板数以黄芩苷峰计算为2498;平均加样回收率为96.16%,RSD=2.24%(n=6)。黄芩苷的线性范围0.249~2.49μg,对照品浓度与峰面积呈良好的线性关系。结论:该法测定复方鱼腥草片和清热解毒口服液中的黄芩苷含量,快速,重复性好。 相似文献
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采用HPLC法建立了中药洗发水中活性成分黄芩苷含量的测定方法。色谱条件:以十八烷基键合相硅胶为填充剂,ODS-SP柱(150 mm×4.6 mm×5μm);以甲醇-0.4%磷酸(47∶53,体积比)为流动相;流速为1 mL/min;柱温为室温;检测波长为280 nm。结果发现,以黄芩苷对照品作标准曲线,在1.0~7.0μg的进样量范围内线性关系良好(r=0.9999);加样回收率为96.85%。测定方法简便、灵敏、准确可靠,可用于中药洗发水中黄芩苷的含量测定,为制定中药洗发水质量标准提供试验基础。 相似文献
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采用高效液相色谱法测定瘟疫消颗粒剂中黄芩苷的含量,以Symmetry C18(3.9mm×150,5μm)为色谱柱,甲醇-0.2%磷酸水溶液(45∶55)为流动相,检测波长:280nm;流速:1.0mL·min-1;柱温:25℃.结果表明黄芩苷在0.0248~0.124 mg·mL-1范围内有良好的线性关系(r=0.9993),平均回收率为96.93%(RSD=0.92%).测得瘟疫消颗粒剂中黄芩苷的含量为9.0mg·g-1.该测定方法简单,专属性强,结果准确,重现性良好,可用于瘟疫消颗粒剂的质量控制. 相似文献
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建立了高效液相色谱法检测化妆品中黄芩苷、黄芩素和汉黄芩素的方法。样品经磷酸甲醇溶液超声提取,以甲醇-磷酸溶液梯度洗脱和C18反相色谱柱分离,DAD检测器检测计算3种中药成分含量。黄芩苷在0.5~10μg/m L,黄芩素在0.5~10μg/m L及汉黄芩素在0.25~5μg/m L范围内浓度和278 nm紫外光吸收强度呈良好线性关系,相关系数大于0.999,方法检出下限分别为2、2和1 ng,方法回收率95.3%~112.7%,RSD为0.9%~5.2%。该方法适于快速、高效、准确对化妆品中黄芩苷、黄芩素和汉黄芩素进行测定。 相似文献
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研究了以水提酸沉法提取黄芩中黄芩苷的最佳提取工艺。考察了水的用量、提取温度、提取时间、酸沉等多种因素对黄芩苷收率的影响。实验结果表明,提取黄芩苷的最佳工艺条件为:水提取两次,两次液固比分别为10和5,时间分别为60 min和30 min,双层滤布过滤再离心分离,80℃加酸并保温60 min,酸沉静置3.0 h。在此条件下,黄芩苷收率可达11.85%。 相似文献
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Miao Lin Long Li Yi Zhang Long Zheng Ming Xu Ruiming Rong Tongyu Zhu 《International journal of molecular sciences》2014,15(7):12507-12522
Renal ischemia-reperfusion injury plays a key role in renal transplantation and greatly affects the outcome of allograft. Our previous study proved that Baicalin, a flavonoid glycoside isolated from Scutellaria baicalensis, protects kidney from ischemia-reperfusion injury. This study aimed to study the underlying mechanism in vitro. Human renal proximal tubular epithelial cell line HK-2 cells were stimulated by H2O2 with and without Baicalin pretreatment. The cell viability, apoptosis and oxidative stress level were measured. The expression of endoplasmic reticulum (ER) stress hallmarks, such as binding immunoglobulin protein (BiP) and C/EBP homologous protein (CHOP), were analyzed by western blot and real-time PCR. NF-E2-related factor 2 (Nrf2) expression was also measured. In the H2O2 group, cell viability decreased and cell apoptosis increased. Reactive Oxygen Species (ROS) and Glutathione/Oxidized Glutathione (GSH/GSSG) analysis revealed increased oxidative stress. ER stress and Nrf2 signaling also increased. Baicalin pretreatment ameliorated H2O2-induced cytotoxicity, reduced oxidative stress and ER stress and further activated the anti-oxidative Nrf2 signaling pathway. The inducer of ER stress and the inhibitor of Nrf2 abrogated the protective effects, while the inhibitor of ER stress and the inducer of Nrf2 did not improve the outcome. This study revealed that Baicalin pretreatment serves a protective role against H2O2-induced cytotoxicity in HK-2 cells, where the inhibition of ER stress and the activation of downstream Nrf2 signaling are involved. 相似文献
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2011年8月福建龙麟集团有限公司1号线入生料均化库胶带提升机出现异常,需停机一周左右维修。但当时生产任务极其紧张,无停窑条件。为此,提出了让出原料磨生料直接入窑煅烧的窑磨联机运行设想并得以实施,由于原燃材料准备充分,技术保证得当和生产管控到位,此次窑磨联机运行获得成功。这说明在特殊情况下,满足一定的生产条件时实行短期的窑磨联机运行维持生产也是一种选择。 相似文献
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依据2019年中国洗协表委会针对规模以上企业相关原料及产品产销数据统计,就目前行业主要原料及产品生产现状及市场进行分析,指出2019年国内表面活性剂行业传统原料及产品走势趋于平稳,规模化和集约化特征更加明显。 相似文献
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拉撑结构作为GB 150—2011的新增内容,很好地解决了按照GB 150—1998标准设计带支撑的凸形封头、平封头及筒体计算厚度过大的问题。根据GB 150—2011标准释义的解释,该部分内容的制定参照了ASME VIII-1 UG-47、UG-48、UG-50、UW-19、JIS B 8267和HG/T 20583—2011的相关内容。对GB150、ASME和JIS标准拉撑结构设计规范进行对比,找出其中的共同点和不同之处,方便设计人员更加清楚地理解拉撑结构设计要点。 相似文献
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The partition coefficients of baicalin were measured in ethylene oxide and propylene oxide(EOPO)/salt aqueous two-phase systems at 298.15K,It was found that most of baicalin partitioned into EOPO-rich phase.The partition coefficients of baicalin varied from 10 to 120.The effect of various factors,including tie-line lngth,salt composition,molecular weight of EOPO,and solution pH,on the partition behavior was investigated on EOPO/salt systems.Furthermore the partition coefficients of baicalin were correlated using the modified Diamond-Hsu model.Good agreement with experimental data is obtained.The average relative deviations are less than 5.0%. 相似文献
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偏灰偏火是煤气炉日常操作中的"常见病"。煤气炉出现偏灰偏火的危害很大,处理恢复的难度同样很大。采取主动措施预防是关键。从工艺、设备、操作、煤质等方面分析导致偏火偏灰的原因。 相似文献