共查询到11条相似文献,搜索用时 31 毫秒
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Zheyu Jiang Mohit Tawarmalani Rakesh Agrawal 《American Institute of Chemical Engineers》2022,68(12):e17929
Multi-feed, multi-product distillation columns are ubiquitous in multicomponent distillation systems. The minimum reflux ratio of a distillation column is directly related to its energy consumption and capital cost. Thus, it is a key parameter for distillation systems design, operation, and comparison. In this series, we present the first accurate shortcut based algorithmic method to determine the minimum reflux condition for any general multi-feed, multi-product (MFMP) distillation column separating any ideal multicomponent mixture. The classic McCabe-Thiele or Underwood method is a special case of this general approach. Compared with existing techniques, this method does not involve any rigorous tray-by-tray calculation, nor does it require guessing of key components. In this first part of the series, we present the mathematical model for a general MFMP column, derive constraints for feasible separation and minimum reflux condition, discuss their geometric interpretations, and present an illustrative example to demonstrate the effectiveness of our approach. 相似文献
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Mathematicals models representing several operating modes of a packed batch distillation column are detailed. In the first part, the authors consider steady-state operation with total reflux, where the axial and radial dispersion phenomena are superimposed on the plug flow of the liquid and vapour phases. The equations are solved by means of a finite element method based on the Galerkin criterion, and also by using a finite difference procedure. The numerical study of the steady-state operating mode, including both axial and radial dispersion phenomena, allows us to note that the last term can be, in most cases, neglected. On the other hand, the dynamic model analysis has shown that the axial dispersion phenomenon is always indispensable for accurately representing the column operation. 相似文献
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带中间贮槽的间歇精馏塔由2个分离段及其中间的贮槽组成。假定液体持液量和待分离的体系的相对挥发度均保持不变,建立了该塔的一个简化的模型,由此得到各组分在整个塔中的分布情况。在此基础上,又考察了各个操作参数对分离效果的影响。 相似文献
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全回流-全馏出与变塔压联合的间歇精馏过程 总被引:1,自引:0,他引:1
A novel operation of batch distillation-combination of varying colum pressure and total reflux-total efflux is studied experimentally. In the operation, the product is accumulated at the top of the column under total reflux and then drained off completely, and the column pressure is varying in the whole process. This process has been industrialized successfully with large profits. The conventional mode of batch distillation is improved by this method effectively: the separation eficiency and the yield of product are increased greatly, the operation time is shortened and the production cost is cut down. Moreover, the amount of condensation water is decreased and the over-high reboiler temperature is lowered. 相似文献
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间歇提馏塔的操作 总被引:6,自引:0,他引:6
A stripping batch distillation column is preferred when the amount of the light component in the feed is small and the products are to be recovered at high purity. The operation modes of a batch stripping are believed to be the same as those of a rectifier. However, the control system of a stripper is different. In this paper, we explore three different control methods with Hysys (Hyprotech Ltd. 1997) for a batch stripper. The main difference is the control scheme for reboiler liquid level: (a) controlled by reflux flow; (b) controlled by reboiler heat duty; (c)controlled by bottom product flow. The main characteristics of operating a batch stripper with different control scheme are presented in this paper. Guidelines are provided for the startup of a batch stripper, the effects of some control tuning parameters on the column performance are discussed. 相似文献