高Ti微合金钢热变形奥氏体的静态再结晶行为

在Gleeable-3800热/力模拟试验机上采用双道次压缩法,研究了一种高Ti微合金钢在奥氏体区变形后道次间隔时间内的静态软化行为,分析了变形温度和间隔时间对静态再结晶行为的影响规律,采用应力补偿法计算了静态再结晶分数。结果表明,变形温度、道次间隔时间对Ti微合金钢静态再结晶行为影响显著,变形温度越高,间隔时间越长,静态再结晶进行得越迅速;确定了Ti微合金钢的静态再结晶激活能为412.56 k J/mol,同时建立了静态再结晶动力学模型。     

钒和铌-钒低碳微合金钢的静态再结晶行为

采用MMS-300热力模拟试验机研究了钒和铌-钒微合金钢的静态再结晶规律,绘制了试验钢的静态再结晶软化率曲线,计算出试验钢的静态再结晶激活能并建立了静态再结晶动力学模型,结合沉淀析出物的微观形貌观察,分析了铌对钒微合金钢静态再结晶行为的影响规律。结果表明,铌-钒钢的静态再结晶激活能要显著高于钒钢,在800~950℃变形保温60 s以上的试验条件下,铌-钒钢发生了形变诱导析出,细小的碳氮化物弥散分布在位错及晶界上,使得软化率曲线在此范围内出现"平台",说明铌既限制了静态再结晶的发生,又阻碍了软化行为的进行。     

Nb-Ti微合金钢的静态再结晶行为

 通过双道次压缩试验研究了Nb-Ti微合金钢的静态再结晶行为,确定了应变诱导沉淀析出前Nb-Ti微合金钢的静态再结晶激活能,并建立了静态再结晶动力学模型。采用面积法及积分-能量法计算的软化率,很好地反映了微合金钢的静态再结晶行为及应变诱导沉淀析出行为。应变诱导沉淀析出的鼻尖温度在900～925℃之间,静态再结晶的临界温度（SRCT）高于950℃。     

含铌微合金钢低温区静态软化行为

 通过两道次压缩变形实验对含Nb微合金钢静态软化行为进行了研究。结果表明：含Nb微合金钢静态再结晶临界温度随应变量增大而降低;随原始奥氏体晶粒尺寸增加而升高。温度高于静态再结晶临界温度时,含Nb微合金钢的静态再结晶激活能为常数(170589 kJ/mol);温度低于静态再结晶临界温度时,由于Nb的碳氮化物应变诱导析出,含Nb微合金钢的静态再结晶激活能为温度的函数,静态再结晶临界温度可通过再结晶激活能与温度倒数的关系曲线来确定。     

高强低合金钢Q390静态再结晶研究

通过双道次压缩试验,研究了高强低合金钢Q390在奥氏体区的软化行为,分析了变形温度与间隔时间对静态软化行为的影响,采用应力补偿法计算了静态再结晶百分数,确定了Q390钢的静态再结晶激活能,并建立了静态再结晶动力学模型。     

WNQ570桥梁钢的静态再结晶行为

 为了研究轧制工艺对WNQ570桥梁钢再结晶行为的影响,采用Gleeble-3500热模拟试验机模拟了其双道次热变形过程,测试了试验钢的应力-应变曲线,建立了静态再结晶晶粒体积分数随变形温度和道次间隔时间变化的关系模型,分析了应变诱导析出抑制对静态软化行为的影响。研究结果表明：静态再结晶体积分数随变形温度的提高或道次间隔时间的延长而增大,应变诱导析出抑制静态再结晶的进行;静态再结晶激活能为240.47kJ/mol。研究结果为制订试验钢二阶段控轧工艺提供了依据。     

高导电性电极扁钢的再结晶规律

为了研究电极扁钢在高温变形时的静态再结晶软化行为,在Gleeble-1500热模拟试验机上对电极扁钢进行双道次热压缩试验,得到了该电极扁钢在不同工艺参数条件下的应力-应变曲线,研究了变形温度和道次间隔时间对电极扁钢静态再结晶行为的影响。根据试验数据结果,计算得到了电极扁钢的静态再结晶激活能,确立了静态再结晶动力学模型。结果表明:道次间隔时间和变形温度对电极扁钢静态再结晶行为的影响比较大,随着变形温度的升高和道次间隔时间的增加,电极扁钢的静态再结晶软化率也增加。     

Cr对低碳高铌X80管线钢静态再结晶的影响

通过Gleeble-1500D热模拟试验机研究了不同Cr含量的低碳高铌X80管线钢在相同变形工艺条件下的软化行为，采用补偿法计算了试验钢的静态再结晶百分率，分析了变形温度和道次间隔时间对静态软化行为的影响。结果表明：变形温度在900℃～980℃，Cr含量达到一定水平时，可以通过溶质拖曳作用显著降低奥氏体再结晶的进行；Cr的加入还可以增加NbC的固溶度、减小其析出驱动力而延迟其析出时间。     

V-N微合金钢Q550D静态再结晶行为

使用MMS-200热模拟实验机研究V-N微合金钢Q550D的静态再结晶行为,获得了其真应力-真应变曲线,同时分析了不同工艺参数对其静态再结晶过程的影响.结果表明：随着变形温度、道次间隔时间、应变量和应变速率的增加,实验钢静态软化率升高.根据实验结果计算得到该钢的静态再结晶激活能为389.4 kJ/mol,回归了静态再结晶动力学模型.     

IF钢热变形铁素体的静态再结晶行为研究

在Gleeb-1500热力模拟试验机上采用双道次压缩法,研究了IF钢高温铁素体区变形后道次间隔时间内的软化行为,分析了温度与间隔时间对其静态软化行为的影响,得出IF钢的铁素体静态再结晶激活能为115kJ/mol,建立了静态再结晶动力学数学模型.     

微合金钢Q420静态再结晶研究

基于双道次压缩实验,研究Q420钢在变形奥氏体区的软化行为,分析变形温度与间隔时间对静态软化行为的影响,确定了Q420轧制工艺.采用应力补偿法计算静态再结晶百分数,确定Q420钢的静态再结晶激活能,并建立了静态再结晶动力学模型.     

热连轧生产船板钢E36静态再结晶行为研究

基于热模拟双道次压缩试验,研究了热连轧生产过程中船板钢E36奥氏体变形区不同变形温度、变形间隙时间内的软化行为,分析了变形温度和轧制变形间隙时间对静态再结晶软化率的影响,结果表明：变形温度是影响再结晶的最主要因素,在达到轧制变形温度时,随着轧制间隙时间的延长,再结晶软化率呈现逐步递增的趋势。通过金相分析,得出了最佳轧制...     

07N15DR低温钢150 mm连铸板坯静态再结晶行为研究

设计了不同间隔时间的双道次压缩实验,模拟热轧条件下5%Ni低温压力容器钢07Ni5DR的变形过程,实测了实验钢的应力-应变曲线。根据应力-应变曲线计算软化率,绘制出软化率-时间曲线,确定实验钢在不同变形温度变形后不同保持时间内的静态软化率。此外,分析静态再结晶动力学过程,为制定合理的轧制工艺提供了实验和理论依据。研究表明,5%Ni低温钢的静态再结晶软化率随变形温度的升高和道次间隔时间的延长而增大,其静态再结晶激活能为233.97 kJ/mol。此外,建立了5%Ni低温钢的静态再结晶动力学方程。     

Static Recrystallization Kinetics Model After Hot Deformation of Low-Alloy Steel Q345B

The static recrystallization behavior of low-alloy steel Q345B during double-pass hot compression deformation tests was investigated in the temperature range of 900-1000 ℃,the true strain range of 0.15-0.25 and the interpass time range of 0.5-50 s on Gleeble-3500 thermo-simulation machine.The results show that static recrystallization during the interpass time is observed.As the deformation temperature and strain increase,softening caused by static recrystallization is obvious.According to the analysis and calculation of thermo-simulation data,the static recrystallization activation energy was obtained and static recrystallization kinetics model was built.Finally,the error analysis of static recrystallization kinetics model proved that the model had good accuracy.Therefore,this model provides a theoretical basis for static recrystallization(SRX)and will contribute to the development of multipass hot rolling process,in order to control the rolling process more accurately.     

胀断连杆用高钒中碳钢的动态再结晶行为

利用Gleeble 3800热模拟试验机进行单道次压缩试验,研究了1种新型胀断连杆用高钒中碳钢37MnSiVS在900~1 150℃温度区间和0.1~10s-2变形速率条件下的动态再结晶行为。结果表明:试验料的热变形特征与传统的中碳微合金钢基本一致,较高的温度和较低的应变速率有利于发生动态再结晶。试验料在变形温度低于1 000℃时开始发生再结晶的时间进一步延长。透射电镜(TEM)观察结果表明,试验料中的钒主要以固溶态的形式存在于奥氏体中,从而影响奥氏体的动态再结晶行为。所获得的试验料的热变形激活能为364.9kJ/mol,并得出了其热变形方程及动态再结晶晶粒尺寸与Zener-Hollomon参数之间的关系式。     

Static Recrystallization Behavior of Twin Roll Cast Low-Carbon Steel Strip

 The static recrystallization kinetics of low-carbon steel cast strip was investigated by means of interrupted hot tensile tests. As-cast strip was reheated and soaked and its austenite grain size was similar to the width level of the as-cast columnar structure. The tests were carried out on Gleeble-3500 thermomechanical simulator. The deformation temperature is in the range of 800 to 1200 ℃ with strain rate of 001 to 1 s-1. The prestrain is fixed at 004 to 012, and the inter-hit delay time varies from 1 to 3000 s. Effect of deformation conditions and initial microstructure on static recrystallization behavior was investigated. The activation energy (Qsrx) and Avrami exponent (n) of static recrystallization were determined to have 241 kJ/mol and 054 respectively by linear regression of the experimental results. A kinetics model was proposed to describe the static recrystallization kinetics in low-carbon steel cast strip. The predicted softening fractions are in good agreement with the experimental results, indicating that the proposed equations can give an accurate estimate of the softening behaviors for the low-carbon steel cast strip.     

5052铝合金单双道次压缩动态与静态软化行为探讨

实验采用Gleeble-1500D热模拟试验机对5052铝合金进行等温热压缩,研究了该合金动态软化特征和静态软化特征,变形温度330～480℃,应变速0.005～0.05/s。结果表明,5052铝合金在热压缩过程中发生了动态软化和静态软化,首道次压下量显著地影响了道次间的静态软化率。结合流变应力曲线和显微组织分析,揭示了动态软化机制主要为动态回复,而静态软化主要是静态再结晶的结果。     

厚壁X80热轧管线钢生产实践及热加工组织演变分析

摘要：通过Thermomastor-Z热模拟试验机双道次压缩实验,研究了X80管线钢在880～1050℃温度区间的静态再结晶行为,结果表明,实验钢在920℃及以下未发生再结晶,在960℃及以上温度,随道次间隔时间延长,静态再结晶率增加。采用不同卷取温度进行了214mm厚度X80板卷工业试制,精轧开轧温度设为920℃,卷取温度510℃的试制钢组织为准多边形铁素体+粒状贝氏体+MA,卷取温度410℃的试制钢组织为粒状贝氏体+贝氏体铁素体+弥散分布的MA的细小组织,后者的MA尺寸和贝氏体板条尺寸明显小于前者,表现出更优异的低温冲击韧性和DWTT性能。通过TEM发现试制钢中的MA是以马氏体为主的组织,并含有较多纳米级尺寸、以Nb元素为主的Nb/Ti碳氮化物复合析出相,但V的析出量则很有限,此外,高卷取温度试制钢的析出相含量也更高。     

Dynamic and Static Recrystallization Behavior of Low Carbon High Niobium Microalloyed Steel

 The recrystallization behavior of a low carbon high Nb microalloyed steel was investigated using Continuous and interrupted hot compression tests. The results showed that the onset of dynamic recrystallization (DRX) could be detected from inflection in the plot of the strain hardening rate θ against stress σ regardless of whether the stress peak appears or not. According to Zener-Hollomon parameter the activity energy of DRX (Qdef) was obtained, and a new modified expression calculating Qdef was proposed in consideration of the chemical composition of experimental steel. Applying the 2% offset method the static softening fraction was determined. The graphic representation of the softening fraction vs. interrupt time gave the information of the non-static recrystallization temperature (about 1000℃)and the relationship of precipitation-time-temperature. Static recrystallization kinetics follow Avrami’s law in high deformation temperature, and different values of the exponent n were given to illustrate the different effects of Nb element on static recrystallization at different deformation temperature.