SCALE-UP OF SPRAY DRYERS

Commercial success of a new spray dryer investment depends upon the dryer meeting its specified performance in all respects, and this puts great importance on the scale-up procedures used in the projecting of the new spray dryer. Scale-up still relies heavily on the experience of the designer. However, as the applications and specifications become more and more complex, so does the need for improved test work in pilot plants, and computational fluid dynamics simulations become more important, so that better scale-up tools are available to minimize the possibility for personal errors that may lead to the new dryer investment becoming an unsuccessful commercial venture.     

SCALE-UP OF CONTACT DRYERS

ABSTRACT

The scale-up of contact dryers is still based on experimental drying curves. In order to keep the effort to a minimum the drying curve is determined using a small laboratory or pilot dryer of similar geometry to the production dryer.

This paper introduces a new scale -up method for contact dryers. The new scale-up method is based on the assumption that heat transfer is the controlling mechanism. The scale-up method is derived from the material balance, the energy balance, the kinetic equation of heat transfer and thermodynamic equilibrium. The scale up method can be used to convert the drying time required to achieve a certain residual moisture content from the laboratory or pilot dryer to the production dryer and/or different drying conditions.

The scale-up method was verified by drying test with four different products in conical mixer dryers of 1, 60, 250, 1000 I volume. Two products were free flowing and two products were non free flowing in the wet state. The products can be considered non-hygroscopic in the moisture range investigated.     

SCALE-UP OF LAYER DRYERS: A UNIFIED APPROACH

Abstract

The concept of Specific Drying Rate is introduced for analysis of experimental drying data for layer dryers and as a convenient scale-up factor. In conjunction with data obtained from a batch laboratory simulation the method is applicable to most types of continuous layer dryers. Three illustrations of the use of this approach for scale-up are presented including a continuous convection heated rotary shelf dryer, an indirectly heated paddle dryer, and an indirectly heated plate dryer with heating zones.     

SCALE-UP OF SPRAY DRYERS WITH THE AID OF COMPUTATIONAL FLUID DYNAMICS

Abstract

The scale-up of spray dryer chambers is difficult because of the complexity of gas and spray flow patterns. The principal concerns in designing a spray drying chamber are to ensure sufficient residence time for drying and to avoid particle-wall collisions. Dimensionless groups are of limited use because it is practically impossible to achieve dynamic similarity between small and large chambers. In the past, empirical, rather than theoretically based, rules generated by experience with existing plant have been used in the design and scale-up of spray dryer chambers but these models, because of their empirical nature, are limited in their range of applicability. Computational fluid dynamics (CFD) is potentially a powerful tool to aid spray dryer design allowing much more flexibility in design but because of the difficulties of modelling such complex phenomena, especially the gas turbulence, its predictions cannot, at present, be considered absolutely reliable and experimental validation of the results is required. However, by considering the principles of similarity, it is shown that validations carried out on pilot scale equipment under the correct conditions will prove the accuracy of CFD applied to spray dryers of any size.     

HEAT TRANSFER IN A CONDUCTIVE-HEATING AGITATED DRYER

Abstract

The heat transfers between the heating plane and the granular materials in both the “Stationary heating-plane type” and the “Moving heating-plane type” of the conductive-heating agitated dryers were discussed mainly from the view point of the scale-up of the dryer. Under the condition of complete mixing in the bed of bulk materials, the heat transfer models proposed for both the two types of dryers can predict the heat transfer coefficients in any sizes of the dryers. However, the complete mixing is not usually accomplished in the large scale of dryer. Hence, an “Incomplete mixing model” was proposed to estimate the effect of the incompleteness of mixing on the heat transfer coefficient. In this model, the incompleteness of mixing can be apparently taken into consideration only by increasing the contact time.     

A SCACE-UP STUDY OF NOZZLE TOWER SPRAY DRYERS

A quasi-one dimensional model taking into account hindered drying beyond the critical tmisture content and droplet size distribution is used to scale-up nozzle tower type of a spray dryer with uniformly distributed air entry, based on pilot plant data. A pilot plant with 8 m high and 1.7 m diameter spray dryer is used to collect the drying data. Equilibrium and critical mistwe contents of the particles are also experimentally msured. The index of drying rate in the hindered drying period is calculated frun the pilot plant data. This index is used in the M e 1 to determine the drying capacity and thereby the mixinnnn particle size that can be produced ina 3.5 m dimoeter 12 m high nozzle t- type of spray dryer. Experiments are carried out in this spray dryer to verify the calculated values of the spray drying capacity. It is s h m that the model when used along with the pilot plant data is adequate for scale-up calaculations for nozzle taer type of spray dryers.     

A SCACE-UP STUDY OF NOZZLE TOWER SPRAY DRYERS

A quasi-one dimensional model taking into account hindered drying beyond the critical tmisture content and droplet size distribution is used to scale-up nozzle tower type of a spray dryer with uniformly distributed air entry, based on pilot plant data. A pilot plant with 8 m high and 1.7 m diameter spray dryer is used to collect the drying data. Equilibrium and critical mistwe contents of the particles are also experimentally msured. The index of drying rate in the hindered drying period is calculated frun the pilot plant data. This index is used in the M e 1 to determine the drying capacity and thereby the mixinnnn particle size that can be produced ina 3.5 m dimoeter 12 m high nozzle t- type of spray dryer. Experiments are carried out in this spray dryer to verify the calculated values of the spray drying capacity. It is s h m that the model when used along with the pilot plant data is adequate for scale-up calaculations for nozzle taer type of spray dryers.     

FULL CONTAINMENT SPRAY DRYING

ABSTRACT

Aspects of safety, environmental protection, and powder quality will continue to influence advances within spray dryer design and operation, and the concept of full containment spray drying offers a means to meet future industrial requirements. Process air recycle and powder containment within the drying chamber leads to no process air discharge to atmosphere, provides a more favorable operator environment around the spray dryer installation, reduces regions within the dryer layout where potential explosive powder/air mixtures can exist, improves yields, reduces powder losses, and provides easier cleaning operations with reduced wash water requirements.     

SCALE-UP OF SPRAY DRYERS WITH THE AID OF COMPUTATIONAL FLUID DYNAMICS

The scale-up of spray dryer chambers is difficult because of the complexity of gas and spray flow patterns. The principal concerns in designing a spray drying chamber are to ensure sufficient residence time for drying and to avoid particle-wall collisions. Dimensionless groups are of limited use because it is practically impossible to achieve dynamic similarity between small and large chambers. In the past, empirical, rather than theoretically based, rules generated by experience with existing plant have been used in the design and scale-up of spray dryer chambers but these models, because of their empirical nature, are limited in their range of applicability. Computational fluid dynamics (CFD) is potentially a powerful tool to aid spray dryer design allowing much more flexibility in design but because of the difficulties of modelling such complex phenomena, especially the gas turbulence, its predictions cannot, at present, be considered absolutely reliable and experimental validation of the results is required. However, by considering the principles of similarity, it is shown that validations carried out on pilot scale equipment under the correct conditions will prove the accuracy of CFD applied to spray dryers of any size.     

A Three-Dimensional Simulation of a Spray Dryer Fitted with a Rotary Atomizer

Abstract

Spray dryers fitted with rotary atomizers are commonly used in diverse industries to produce engineered powders on a large scale. Scale-up of such units is still largely empirical and based on prior experience and know-how. In the present study, a three-dimensional spray dryer with rotary atomizer is investigated numerically with a commercial CFD code. Continuous-phase, i.e., air, conservation equations are formulated in the Eulerian model while the droplet or particle equations are set up in the Lagrangian model. Two-way coupling between the continuous and dispersed phases is taken into account in the governing equations. The stochastic approach is used to predict the particle trajectories. The RNG k ? ? turbulence model was used. Typical results, viz. air velocity, temperature, humidity profiles, and particle trajectories are presented and discussed. Compared with the pressure nozzle spray dryer, more volume of drying chamber is used effectively by the rotating disc type spray dryer. It is found that evaporation and drying take place mainly in the region and in the vicinity of first contact between air and spray. A parametric study is presented and, where appropriate, comparison is made with experimental data obtained with the simulated spray dryer.     

SOME CRITERIA OF SPRAY DRYER DESIGN FOR FOOD LIQUID

Abstract

Spray drying has many applications for a wide variety of dried food powders. The quality of spray dried food is quite dependent on the atomization characteristics and the heat and mass transfer on drops inside the spray dryer. This paper deals with some design criteria of the spray dryer such as the atomizer, the drop trajectory and the heat/mass transfer between the drop and the drying air.     

SCALE-UP OF SPOUTED BED DRYERS: CRITERIA AND APPLICATIONS

Abstract

The criteria required for reliable scale-up of the aerodynamics of spouted bed dryers of grains are stated and discussed. The dryer modeling role for effective scale-up, design and analyses of such dryers will be outlined. Suggestions are made on how small scale drying and aerodynamic data may be scaled up for spouted bed dryers. Appropriate empirical and semi-empirical correlations are listed. A flowchart is provided for design and analysis of a conventional and a two-dimensional spouted bed dryers.     

Supercritical Fluid Extraction Of Lemon Verbena (Aloysia triphylla): Process Kinetics and Scale-Up,Extract Chemical Composition and Antioxidant Activity,and Economic Evaluation

The extract of lemon verbena ( Aloysia triphylla ) was obtained by supercritical fluid extraction (SFE) using laboratory and pilot scale equipments. The scale-up criterion selected (maintaining solvent to feed ratio constant) was successfully used for a 14-fold scale-up. The extract obtained in pilot scale was separated in three fractions, which were characterized as for their phytochemical profile, total flavonoids content, and antioxidant activity. The extracts obtained by SFE were compared to classical Soxhlet extraction method. Maximum yield obtained for SFE was 1.8%, and for Soxhlet, 7.1%. The chemical composition revealed different phytochemical profiles for SFE and Soxhlet extracts; the last ones presented more flavonoids, while SFE extracts were more concentrated in volatile compounds. The major compounds identified in the volatile fraction of the extracts were spathulenol, phytol and octadecatrienal. Some extracts presented pro-oxidant activity and others presented antioxidant activity. The SFE process was shown to be economically feasible for obtaining lemon verbena extracts; the minimum manufacturing cost (COM) obtained was US$ 1070.00/kg, with a payback time of 2 years.     

An Investigation of Milk Powders Produced by a Laboratory-Scale Spray Dryer

ABSTRACT

A mini spray dryer has been used to investigate morphological changes that occur to milk particles during the spray drying process. We have found that the mini spray dryer is ideal for such investigations, because phenomena such as skin and vacuole formation in particles can be analyzed without the added complication of particle agglomeration, which only occurs in much larger spray dryers where particle number concentrations are higher. We have confirmed observations made by various researchers that the bulk density of spray-dried milk powder is greatly affected by the drying temperature, due to the strong influence of the latter on the porosity of the particles. In addition, we have attempted to explain observations made by various workers that fat accumulates preferentially at the surface of a particle during drying by postulating that fluid fat is transported towards the surface, via a network of cracks and pores, by the development of a vacuole overpressure which is also responsible for the inflation of the particle. Finally, we have shown that milk powders can be spray dried a second time, by reconstitution with water, with no change to the thermodynamic characteristics of the resultant powder. Thus, milk concentrates for spray drying research can be prepared from already-spray-dried milk powders rather than using the more arduous evaporation method to concentrate unprocessed milk.     

Soda Ash Production from Trona in a Spray Dryer

Production of soda ash from Trona solution was achieved in a spray dryer reactor. Fractional conversion of NaHCO₃ reached to values close to unity in this unit within a residence time of less than a second. Results indicated that above 140°C, heat transfer limitations played a significant role on the calcination process taking place in the spray dryer. Equilibrium limitations may become important only at very low temperatures and at high CO₂ and H₂O partial pressures. Results obtained in the spray dryer and from the thermal gravimetric analysis of Trona crystals agreed well. It was also shown that the predictions of the unreacted core model are in good agreement with the kinetic data. © 1997 SCI.     

Model-based scale-up strategy for mycelial fermentation processes

With the aid of a mathematical model describing the interrelationships between mycelial morphology, mycelial growth and product formation, rheology, mass transfer, and environmental conditions, a new scale-up strategy has been developed, simulating the bioreactor performance at different agitation speeds. The simulations have shown that there is an optimum agitation speed, yielding maximum product formation that is different from the conventional scale-up results based on constant P_g/V_T, k_L a and N_I D_I. It has also been shown in the simulations that the product formation scaled up by means of conventional methods is considerably lower than the simulated maximum or is close to the maximum but requiring a higher energy consumption. This indicates that model-based scale-up could be a more accurate and efficient method for scaling up complex systems such as mycelial fermentation processes.     

AIR FLOW,TEMPERATURE AND HUMIDITY PATTERNS IN A CO-CURRENT SPRAY DRYER: MODELLING AND MEASUREMENTS

ABSTRACT

In a co-current pilot plant spray dryer measurements were done of the airflow pattern (no spray) and the temperature and humidity pattern (water spray). These patterns were simulated with a computational fluid dynamics package (FLOW3D)

The measured air velocities showed large fluctuations. The measured and predicted flow pattern showed good agreement qualitatively, but the measured profiles showed less variation than the predicted ones

The measured temperatures and humidities showed good agreement in large areas of the dryer, but the agreement in the zone near the central axis leaves room for improvement.     

FLOW VISUALISATION AND INSTANTANEOUS VELOCITY MEASUREMENTS OF SPRAY DRYER GAS AND SPRAY FLOWS USING PARTICLE IMAGE VELOCIMETRY

ABSTRACT

The technique of particle image velocimetry has been used to produce good quality instantaneous velocity maps of the gas and spray phases within a pilot plant co-current spray dryer. Good quality flow visualisation data provided by the use of the laser sheet as an intense source of illumination has indicated that the air and spray flows were characterised by an offset central jet with down flowing (right hand side) and up flowing (left hand side) wall streams. This is significantly different from what would normally be expected and it was suggested that this was possibly due to a maldistribution of the air phase on inlet to the dryer.     

FRUIT AND VEGETABLE POWDERS PRODUCTION TECHNOLOGY ON THE BASES OF SPRAY AND CONVECTIVE DRYING METHODS

ABSTRACT

The peculiarities of fruit and vegetable powders production technology based on spray & convective drying methods are shown.

The experimental data related to the drying kinetics of apple juice droplets as well as the production flow diagrams and the performance of a spray dryer intended for the treatment of hygroscopic pasty products are presented.     

A Study of the Limitations to Spray Dryer Outlet Performance

Abstract

The concept of the product moisture locus was tested in this work using a pilot-scale modified Niro spray dryer (diameter 0.8 m, height 2 m), where the residence time of the particles inside this spray dryer is lower compared with larger industrial spray dryers. The moisture contents of skim milk powder produced from spray drying skim milk (solids content 8.8% w/v) at different operating conditions, namely different swirl vane angles (0°, 25°, 30°), inlet air temperatures (170°C, 200°C, 230°C) and process fluid flowrates (1.4 kg h^?1, 1.6 kg h^?1, 1.8 kg h^?1), were compared with the predicted equilibrium moisture contents. In addition, the residence time of the particles was also increased in the spray dryer by decreasing the inlet air mass flowrate from 0.016 to 0.013 kg s^?1. The outlet moisture contents of the skim milk powder for all the 23 runs carried out in this work were within 0.4% of the equilibrium values. Thus, the skim milk powder particles were in close equilibrium with the gas inside the drying chamber. These equilibrium limitations are confirmed by other literature data (Boonyai, P. Comparative Evaluation of Soymilk Drying in a Spray Dryer and Spouted Bed of Inert Particles. M.Sc. Thesis. Asian Institute of Technology: Bangkok, Thailand, 2000; 90 pp; Harvie, D.J.E.; Langrish, T.A.G.; Fletcher, D.F. A computational fluid dynamics study of a tall-form spray dryer. Trans IChemE 2002, in press). The use of this finding to predict spray dryer performance is demonstrated by mass and energy balance calculations.