TEMPERATURE AND CONCENTRATION EFFECTS OF OSMOTIC MEDIA ON OD PROFILES OF SWEET POTATO CUBES

A study was conducted to evaluate the effects of temperature and sucrose osmotic solution concentrations on osmotic dehydration profiles of sweet potato (Ipomea batata) cubes (3.5 cm sides). Two temperatures (26 and 50°C) and three concentrations (30:100, 50:100 and 70:100 w/w) were studied for various exposition times, up to 168 hours. Main influence was observed at higher temperature (50°C) due the fact that water loss (WL) and solids gains (SG) are faster and more intense. At 26°C no appreciable change in solids concentration was observed at distances deeper than 0.5 cm from the cubes surfaces even at 168 hours. At 50°C all the layers are affected even at shorter times (8 hours).     

Optimization of Osmo-convective Dehydration Process for the Development of Honey-ginger Candy Using Response Surface Methodology

Osmotic dehydration of ginger with honey is an interesting alternative for the development of confectionary-based functional food with extended shelf life. Response surface methodology (RSM) was used to investigate the effects of process variables on solid gain, water loss, and overall acceptability of honey-ginger candy. The process variables included blanching time (6–10 min), osmotic solution temperature (30–50°C), immersion time (90–150 min), and convective drying temperature (50–70°C). The honey to ginger ratio was 4:1 (w/w) during all the experiments. Ginger cubes were blanched before osmotic dehydration to increase the permeability of the outer cellular layer of tissue. After osmotic concentration of ginger with honey, convective dehydration was done to final moisture content of 3–5% (w.b.) to make it a shelf-stable product. Finally, osmo-convectively dried ginger was coated with sucrose for candy preparation. The optimum osmo-convective process conditions for maximum solid gain, water loss, and overall acceptability of honey-ginger candy were 7.07 min blanching time, 50°C solution temperature, 150 min immersion time, and 60°C convective drying temperature.     

TEMPERATURE AND CONCENTRATION EFFECTS OF OSMOTIC MEDIA ON OD PROFILES OF SWEET POTATO CUBES

A study was conducted to evaluate the effects of temperature and sucrose osmotic solution concentrations on osmotic dehydration profiles of sweet potato (Ipomea batata) cubes (3.5 cm sides). Two temperatures (26 and 50°C) and three concentrations (30:100, 50:100 and 70:100 w/w) were studied for various exposition times, up to 168 hours. Main influence was observed at higher temperature (50°C) due the fact that water loss (WL) and solids gains (SG) are faster and more intense. At 26°C no appreciable change in solids concentration was observed at distances deeper than 0.5 cm from the cubes surfaces even at 168 hours. At 50°C all the layers are affected even at shorter times (8 hours).     

Ultrasound-Assisted Osmotic Dehydration of Strawberries: Effect of Pretreatment Time and Ultrasonic Frequency

Pretreatment of fruits prior to drying has shown success in reducing drying time and costs. In this work, ultrasound-assisted osmotic dehydration has been implemented as a method to increase water diffusivity and reduce drying time in strawberries. Strawberry halves were immersed in distilled water and in two different concentrations of sucrose solutions while pretreatment time and ultrasonic frequency levels were varied to determine their effect on drying time, water loss, and soluble solids gain. A microscopic analysis was carried out to evaluate the formation of microchannels and other changes to the fruit tissue structure. Greater sucrose concentration used in ultrasound-assisted osmotic dehydration resulted in greater water loss with greatest loss observed for the strawberry halves pretreated for 45 min in a 50% w/w sucrose solution. The pretreatment carried out for 30 min employing an osmotic solution of 50% w/w of sucrose resulted in the highest drying rate among the pretreatments. Osmotic dehydration used alone during pretreatment increased total processing time, whereas osmotic dehydration combined with ultrasonic energy during pretreatment reduced total processing time and increased effective water diffusivity. Cell distortion and breakdown were observed not only in pretreatments employing ultrasound-assisted osmotic dehydration but in conventional osmotic dehydration. Formation of microchannels through ultrasonic application and effects of osmotic pressure differential were considered to be largely responsible for reducing drying time for strawberry halves.     

Optimization of Osmotic Dehydration of Kiwifruit

Mass transfer rates were quantitatively investigated during osmotic dehydration of kiwifruit slices using response surface methodology with the sucrose concentration (20-80%, w/w), temperature of sucrose solution (15-75°C), osmotic time (60-420 min), and slice thickness (2-10 mm) as the independent process variables. Quadratic regression equations are obtained to describe the effects of independent process variables on the water loss (WL), sucrose gain (SG), and ascorbic acid loss (AAL). It was found that all factors had significant effect on the WL during osmotic dehydration of kiwifruit. Effects of temperature, time, and slice thickness were more pronounced on SG than the effect of concentration of sucrose solution. The osmotic solution temperature was the most significant factor affecting the AAL, followed by slice thickness and duration of treatment. The optimal conditions for osmotic dehydration were: 60% sucrose concentration, 30-40°C osmotic temperature, 150 min osmotic time, and 8 mm slice thickness.     

Influence of Osmotic Pretreatment on Kinetics of Convective Drying and Quality of Apples

This article examines the influence of apple osmotic dehydration (OD) on the kinetics of convective drying and the quality of the products obtained. Fresh apples (Malus domestica), variety Ligol, were used as the experimental material. Samples were first dehydrated in three osmotic agents (glucose, fructose, and sucrose), each at a concentration of 40%, for 30, 60, and 120 min, and then dried convectively. Efficiency of osmotic dewatering was assessed on the basis of water loss (WL) and solids gain (SG). The influence of OD on convective drying kinetics was analyzed by comparing the drying curves and the basic kinetic parameters (time and drying rate). Quality of products was assessed on the basis of colorimetric measurements and sensory evaluation. It was found that OD significantly improved the quality of dried products through better retention of the original color, shape, texture, aroma, and taste, but it did not remarkably affect the rate of convective drying.     

Comparison of Water Blanching and High Hydrostatic Pressure Effects on Drying Kinetics and Quality of Potato

Abstract

Drying kinetics and quality parameters of potato cubes were evaluated as affected by high pressure processing and hot water blanching. The potato cubes in 1% citric acid solution as immersion medium were pressure treated at 400 MPa for 15 min. Hot water blanching was conducted in boiling water for 3 min. Drying kinetics and quality parameters (i.e., rehydrability, texture, color and apparent density) were assessed for the high pressure–treated and water-blanched samples and for dehydrated and rehydrated samples. Drying rates were found to be higher (p < 0.05) in the initial period of drying for the pressure treated samples. The Page model was found to better fit drying data of the thermally treated samples, and the two-terms model better described the drying behavior of high pressure–treated samples. High pressure–treated samples had a similar rehydrability to thermally treated samples. It was found that pressure–treated samples had a hardness value close to that of fresh samples, whereas thermal treatment resulted in a softer texture. After rehydration, samples of both treatments returned their texture before drying. The total color difference for the thermally blanched samples was higher (p < 0.05) than for pressure–treated samples before drying and after drying. High pressure–treated and dried potato cubes had a color close to that of fresh potato cubes. High pressure–treated and air-dried samples were found to have higher (p < 0.05) apparent density than thermally treated samples.     

Osmotic Dehydration Kinetics of Pumpkin Fruits Using Ternary Solutions of Sodium Chloride and Sucrose

The objective of this work was to obtain experimental data and modeling of osmotic dehydration kinetics of pumpkin fruits (Cucurbita pepo L.) with aqueous NaCl/sucrose solutions. For this purpose, effective diffusion coefficients for water, sucrose, and NaCl were calculated by means of a simple model based on Fick's second law. Water loss achieved 80%, sucrose 13%, and NaCl 6% of the initial sample weight. Effective diffusion coefficients ranged from 0.58–1.40 × 10^?9 m²/s, 0.75–1.23 × 10^?9 m²/s, and 2.60–4.11 × 10^?9 m²/s for water, sucrose, and NaCl, respectively. The proposed model gave a good correlation of the experimental data. The quality of the operation was evaluated by analysis of the values of WL/SG ratio.     

Pulsed Electric Field Pretreatment for Osmotic Dehydration of Apple Tissue: Experimental and Mathematical Modeling Studies

The aim of this study was to analyze the influence of pulsed electric field pretreatment (PEF) on the osmotic dehydration of apple tissue. Osmotic dehydration was carried out in sucrose solution at 40°C and 100 rpm in a water-bath shaker. PEF pretreatment was performed using varying field strength of 5 and 10 kV/cm and 10 and 50 pulses. On the basis of electric conductivity measurement, the cell disintegration index was calculated. The course of osmotic dehydration was described by means of water loss, solid gain, weight reduction, and water content changes. Moreover, the course of the process was described by different mathematical models that are commonly used in the literature. PEF application before osmotic dehydration significantly increased water loss after 60 minutes of the process. In turn, no significant differences were found in the case of solid gain. The highest osmotic dehydration efficiency ratio (WL/SG) was noticed for samples treated by PEF at the electric field strength of 5 kV/cm and 10 pulses. The statistical analysis of mathematical modeling of the process showed the equations utilized generally exhibit a good fit to the experimental data.     

Comparison of two alternatives of combined drying to process blueberries (O'Neal): Evaluation of the final quality

In this work, we examined and compared two combined alternatives for the drying of blueberries (O’Neal). Pretreatments of osmotic dehydration (60°Brix sucrose solution at 40°C for 6 h) and hot air drying (HAD) (60°C, 2.5 m/s for 90 min) were performed to reach the same water content. Pretreated blueberries were then dried by microwave at different microwave output power values: 562.5, 622.5, and 750 W. The combined drying processes were also compared with HAD alone (control). The effects of the processes over blueberries were studied in terms of decrease in water content, drying rate (DR), mechanical properties (firmness and stiffness), optical properties (L*, a*, and hue angle (h)), antioxidant capacity, and rehydration capacity. The hot air–microwave drying decreased the process time and presented a high drying rate compared with the osmotic dehydration–microwave processes and the control drying. In terms of quality, the antioxidant and rehydration capacities were the most affected. The results showed that the best drying method to obtain the desired final product was the hot air–microwave drying (750 W).     

Osmotic Dehydration of Apple Cylinders: III. Continuous Medium Flow Microwave Heating Conditions

Continuous flow osmotic drying permits a better exchange of moisture and solids between the food particle and osmotic solution than the batch process. Osmotic drying has been well studied by several researchers mostly in the batch mode. Microwave heating has been traditionally recognized to provide rapid heating conditions. Its role in the finish drying of food products has also been recognized. In this study, the effects of process temperature, solution concentration on moisture loss (ML), solids gain (SG), and mass transport coefficients (k _m and k _s ) were evaluated and compared under microwave, assisted osmotic dehydration (MWOD) versus continuous flow osmotic dehydration (CFOD). Apple cylinders (2 cm diameter, 2 cm height) were subjected to continuous flow osmotic solution at different concentrations (30, 40, 50, and 60°Brix sucrose) and temperatures (40, 50, and 60°C). Similar treatments were also given with samples subjected to microwave heating. Results obtained showed that solids gain by the samples was always lower when carried out under microwave heating, while the moisture loss was increased. The greater moisture loss strongly counteracted solids gain in MWOD and thus the overall ratio of ML/SG was higher in MWOD than in CFOD.     

Optimization of Vacuum Microwave Predrying and Vacuum Frying Conditions to Produce Fried Potato Chips

The effects of vacuum microwave predrying and vacuum frying conditions on the quality of vacuum-fried potato chips were studied. Both the moisture content and oil content of potato chips decreased with increasing vacuum microwave predrying time. During vacuum frying, the moisture content of potato chips decreased with increasing frying temperature and time, while the oil content increased. Statistical analysis with response surface regression showed that the moisture content, oil content, and breaking force of potato chips were significantly (P<0.05) correlated with vacuum microwave predrying time, frying temperature, and frying time. Based on surface responses and contour plots, optimum conditions were vacuum microwave predrying time of 8–9 min, vacuum frying temperature of 108–110°C, and vacuum frying time of 20–21 min.     

Optimization of Foaming Parameters and Investigating the Effects of Drying Temperature on the Foam-Mat Drying of Shrimp (Penaeus indicus)

In this study, foaming conditions of shrimp (Penaeus indicus) were optimized using response surface methodology (RSM) and the effect of drying temperature on drying behavior was investigated. The experiments were conducted according to face-centered central composite design for three independent variables: xanthan gum concentration (0.1–0.4% w/w), whipping time (2–6 min), and water : shrimp ratio (2:1–6:1 w/w) to minimize the foam density (FD) and the drainage volume (DV) as responses. Statistical analysis of results showed that linear terms of the models were significant (p < 0.01) except the linear term of whipping time in DV. Xanthan gum concentration 0.19% (w/w), water : shrimp ratio 4.5:1 (w/w), and whipping time 5.89 min were found to be the optimum foaming conditions. The effect of different drying temperatures (45, 60, 75, and 90°C) on drying behavior of optimized foam was then evaluated. The drying air temperature had a considerable effect on drying time and drying rate. As the temperature increased from 45 to 90°C, the drying time decreased to 90 min. Drying rate curves showed that foam-mat drying of shrimp principally occurred in the constant rate period. Different mathematical models were tested with the drying behavior of shrimp foam in the dryer. According to the results, the Weibull distribution model is superior to the other models for explaining the drying behavior. Effective moisture diffusivity was calculated and was between 1.114 × 10^?8 and 3.951 × 10^?8 m²/s within the studied temperature range. An Arrhenius relation with an activation energy value of 26.89 kJ/mol expressed the effect of temperature on diffusivity.     

Three-stage hybrid osmotic–intermittent microwave–convective drying of apple at low temperature and short time

ABSTRACT

In recent years, intermittent microwave coupled with hot air-drying has been used increasingly, thanks to considerable improvements observed in drying properties. The aim of this study was to investigate the effect of process of drying apple pretreated osmotically with sucrose solution at five concentrations of 0 (control), 10, 30, 50, and 70% (w/w), using intermittent microwave at four power levels of 0 (control), 360, 600, and 900?W, four pulse ratios of 1, 2, 3, and 4, and convective hot air (40°C) on drying kinetics, effective moisture diffusion coefficient, shrinkage, bulk density, rehydration ratio, and energy consumption. Results showed that the three-stage hybrid osmotic–intermittent microwave–convective drying of apple at low temperature yielded higher drying rates (with 41.5% decrease in drying time) and improved quality of final product. The effective moisture diffusion coefficient increased with an increase in power, pulse ratio, and the concentration of osmotic solution. Furthermore, shrinkage, bulk density, and energy consumption of the samples decreased with an increase in power, pulse ratio, and the concentration of osmotic solution. In summary, the use of intermittent microwave coupled with forced convection of hot air (at low temperature) in drying of apple pretreated by sucrose osmotic solution led to products with improved properties in terms of both quality and quantity.     

Drying of Chestnuts (Castanea sativa Mill.) after Osmotic Dehydration with Sucrose and Glucose Solutions

Chestnuts were dehydrated by using a combined method of osmotic dehydration followed by air drying. Samples were osmotically pretreated with sucrose (60% w/w) and glucose (56% w/w) for 8 h, air-dried at temperatures of 45, 55, and 65°C, at a relative humidity of 30% and at a velocity of 2.7 m·s^?1 and the experimental data of the drying kinetics were obtained. Whole samples were dried with different peelings: (a) removal of endocarp and pericarp (peeled) and (b) additionally the internal rough surface (cut). In all cases, cut chestnuts show greater drying rates than peeled samples, indicating that a significant mass transfer resistance in the layer nearest to the surface takes place. Peeled samples pretreated with sucrose solutions behave in a similar way to untreated samples. For the rest of the samples, the cut samples osmotically treated with sucrose solutions and all the samples treated with the glucose solution, the drying rates decrease during drying. Drying kinetics are successfully modeled by employing a diffusional model that takes the shrinkage into account. The effective coefficient of water diffusion was evaluated and correlated with temperature. The quality of the final product was monitored by color change. In spite of the fact that the total color difference is not modified by the osmotic treatment, the L?, a?, and b? color coordinates of cut samples treated with sucrose and glucose solutions do undergo changes; the L? and a? coordinates change less than the b?.     

STRUCTURAL CHANGES AND MASS TRANSFER DURING GLUCOSE INFUSION OF APPLES AS AFFECTED BY BLANCHING AND PROCESS VARIABLES

ABSTRACT

The effect of process variables and blanching on the rate of dewatering of apple slices through immersion in glucose solutions was analyzed. The adequacy of the Hawkes and Flink's and Peleg's models for fitting the rate data was evaluated as well as the structural changes produced in the tissue subjected to osmotic process. High concentration values (33-42 % (w/w)) of the soaking solution favored significantly water loss (WL) but only slightly affected solid gain (SG). Increasing system temperature over the range 20-50 °C generally provided an increase in WL and in SG. The increase in thickness decreased significantly both mass transfer rates. The use of sucrose instead of glucose lead to a greater SG while blanched samples showed higher rates of WL and SG. Microscopic studies revealed that, when applying short treatments, cells appeared slightly shrinked and cells walls folded. After long treatments, although an extensive     

Drying of Osmosed Cantaloupe: Effect of Polyols on Drying and Water Mobility

Cantaloupe slices were sequentially immersed in 40 and 50 °Brix sucrose solutions for 24 h each. Partial replacement of the 50 °Brix sucrose solution with one of two polyhydric alcohols (sorbitol or glycerol) at 10 or 15% (w/v) was also performed along with a 0% (w/v) polyhydric alcohol treatment and a 10% (v/v) invert sugar partial replacement of the 50 °Brix solution as a control and a reference, respectively. Solids gain (SG) and water loss (WL) were determined up to 48 h later. Conversely, the treatment with 10 and 15% (w/v) sorbitol and the reference showed a significantly higher SG and a lower WL than the control (p < 0.05). The treatments with 10 and 15% (w/v) glycerol presented a significantly lower SG and higher WL than the control (p < 0.05). Increasing concentrations of polyol led to an increase in both the WL and the SG. The osmosed cantaloupe was then dried in a hot air dryer at 60°C, where the numerical drying rate was observed to be as follows: control > 10% sorbitol > 15% sorbitol > 10% glycerol > 15% glycerol > reference, but these differences at each moisture ratio were not significantly different (p > 0.05). Page's model showed a better goodness of fit with the experimental data for all treatments than did the Henderson and Pabis model. The addition of either of the two polyhydric alcohols resulted in a decreased longitudinal relaxation time (T ₁), as monitored using nuclear magnetic resonance (NMR), indicating the decreased mobility of water molecules. Among all treatments evaluated, the sensory analysis derived acceptance scores for the product treated with 10% (w/v) sorbitol were not significantly different from that of the reference (p > 0.05). This may due to the ability of invert sugar and polyols to act as a humectant.     

Ultrasound-assisted osmotic process on quality of microwave vacuum drying sweet potato

The effects of pretreatment before microwave vacuum drying (MVD) on texture, color, expansion, rehydration, drying rate, microstructure, sensory evaluation, and other properties of sweet potato were investigated in this study. The pretreatment consisted in five processing conditions, using blanching; osmotic dehydration at 35°Brix of sucrose (OD); ultrasound in distilled water (US); ultrasound in distilled water before osmotic dehydration (US?+?OD), and ultrasound-assisted osmotic dehydration (USOD). Pretreatments of sweet potato before MVD have shown success in reducing drying time with US treatment relatively more effective regarding drying time than other treatments. Compared with other treatments, US showed the highest rehydration ratio values. The osmotic group pretreatment exhibited a pronounced effect on water loss and solid gain, improved the color, aroma, and taste of dried sweet potato, whereas sucrose impregnation resulted in a hard texture observed with OD sample. USOD samples had a higher expansion ratio, lower hardness and color difference values, appeared less cell damaged, and recorded better overall quality than the other samples. There was a slight difference between USOD and US?+?OD samples. Combining osmotic dehydration with ultrasound as a pretreatment can significantly accelerate the heat transfer rate, reducing the dried time accordingly and increasing energy efficiency.     

Microwave,Vacuum, and Air Drying Characteristics of Collard Leaves

Collard leaves (Brassica oleracea L. var. acephala) with an initial moisture content of 6.65 on percentage dry basis (%db) were dried by three different drying methods: microwave, air, and vacuum. Samples of fresh leaves, 25 g each, were dried until their moisture was down to 0.1 on a dry basis. The following drying levels were used in each of the drying processes: 350, 500, 650, 750, 850, and 1000 W for microwave drying; 50, 75, 100, 125, 150, and 175°C for air drying; and 0.4, 50, and 100 mmHg at 50 and 75°C for vacuum drying, respectively. Drying times ranged between 2.5 to 7.5 min, 8 to 210 min, and 35 to 195 min for microwave, air, and vacuum drying, respectively. The data obtained compared well with a thin-layer drying model. Microwave drying at 750 W provided optimal results with respect to drying time, color, and ascorbic acid content (vitamin C).     

Effect of Blanching by Ohmic Heating on the Osmotic Dehydration Behavior of Apple Cubes

The effect of blanching by ohmic heating (OH) on the damage to apple tissues and subsequent osmotic dehydration kinetics was investigated. Apple cubes were heated ohmically to various blanching scales. Heating temperature and duration were, respectively, 60–95 ± 2°C and 0–6 min. After cooling, the treated samples were put into sucrose solutions (70 °B) for the osmotic dehydration (OD). The equilibrium state of osmotic dehydration was estimated using the Azuara model. Ohmic heating leads, even for short treatments, to significant changes in the cellular structure of apples and to the enhancement of mass transfer during osmotic dehydration.