常压吸附流化冷冻干燥技术的研究与探索

阐述了常压吸咐流化冷冻干燥与真空冷冻干燥的原理，特点，研究概况和能耗分析，提出常压吸附流化冷冻干燥可能成为一种新型冷冻干燥技术而具有较高的研究开发价值。     

Trends in Microwave-Assisted Freeze Drying of Foods

Microwave-assisted freeze drying (MFD) can be accomplished in two distinct ways: freeze drying assisted concurrently with microwave application (MFD-1) and freeze drying and assisted microwave/vacuum microwave drying in two consecutive separate drying stages (MFD-2). MFD is a rapid dehydration technique that can be applied to certain foods, particularly to seafoods, solid soup, and fruits and vegetables. MFD involves much less drying time and energy consumption than conventional freeze-drying methods. Currently, this technology has been successfully used to dry many food materials and has potential in the food industry. Increasing concerns over product quality, energy savings, and production costs have motivated researchers and the industry to adopt MFD technologies. The advantages of MFD include shorter drying time, energy savings, improved product quality, and flexibility in producing a wide variety of dried products. However, current applications are limited to small categories of foods due to high startup costs and relatively complex technology compared to conventional freeze drying. This article presents a concise review of recent progress in MFD R&D and makes recommendations for future research to bridge the gap between laboratory research and industrial applications.     

Microwave Freeze Drying of Sea Cucumber Coated with Nanoscale Silver

To develop an improved dehydration method for sea cucumber, microwave freeze drying was tested as a potential method. According to our experimental results, microwave freeze drying can reduce drying time to about half of the traditional vacuum freeze-drying process. To ensure a high degree of sterilization, a novel nanoscale silver coating technique was combined with microwave freeze drying. Microwave freeze drying combined with nanoscale silver coating treatment leads to a much lower microorganism number with no significant effect on drying efficiency and sensory quality.     

Microwave Freeze Drying of Sea Cucumber Coated with Nanoscale Silver

To develop an improved dehydration method for sea cucumber, microwave freeze drying was tested as a potential method. According to our experimental results, microwave freeze drying can reduce drying time to about half of the traditional vacuum freeze-drying process. To ensure a high degree of sterilization, a novel nanoscale silver coating technique was combined with microwave freeze drying. Microwave freeze drying combined with nanoscale silver coating treatment leads to a much lower microorganism number with no significant effect on drying efficiency and sensory quality.     

A Two-Stage Vacuum Freeze and Convective Air Drying Method for Strawberries

Strawberries were dehydrated in a two-stage combination drying consisting of vacuum freeze drying (FD) followed by hot air drying (AD), and in a two-stage hybrid method involving FD and finish AD(FAD) to obtain dehydrated strawberries of high quality at reduced cost. Energy consumption and physicochemical properties of the FAD product were compared with single-stage AD and single-stage FD. The quality parameters of the products were also analyzed. It was found that the quality of combined FAD-dried products approximated that of single-stage FD. Hence, the proposed two-stage combination drying method is recommended for dehydration of strawberries to obtain a high-quality product at lower cost when compared with vacuum freeze drying alone.     

A Two-Stage Vacuum Freeze and Convective Air Drying Method for Strawberries

Strawberries were dehydrated in a two-stage combination drying consisting of vacuum freeze drying (FD) followed by hot air drying (AD), and in a two-stage hybrid method involving FD and finish AD(FAD) to obtain dehydrated strawberries of high quality at reduced cost. Energy consumption and physicochemical properties of the FAD product were compared with single-stage AD and single-stage FD. The quality parameters of the products were also analyzed. It was found that the quality of combined FAD-dried products approximated that of single-stage FD. Hence, the proposed two-stage combination drying method is recommended for dehydration of strawberries to obtain a high-quality product at lower cost when compared with vacuum freeze drying alone.     

Atmospheric Freeze Drying—A Review

This review article focuses on the development of atmospheric freeze drying (AFD): technological aspects, product possibilities, physical properties of products, drying kinetics, modeling, and simulation. The main motivation for developing atmospheric freeze drying as a new drying technology is the desire to reduce the energy consumption compared to vacuum freeze drying while maintaining a high product quality. One technical solution of atmospheric freeze drying is a combined atmospheric freeze drying and heat pump system with new environmentally friendly refrigerants. Temperature programs make it possible to customize products with desired qualities and properties, like retained color, instant properties, aroma, and nutritional value.     

黑加仑真空冷冻干燥工艺研究

以黑加仑为原料,对其真空冷冻干燥特性和工艺进行了试验研究。结果表明：黑加仑的共晶温度为-24℃,共融温度为-21℃;其合理的工艺参数为：升华温度为50℃,保持4．5h;解吸温度为60℃,保持2h。冻干后的黑加仑含水量为5％左右,能很好保持黑加仑的品质,Vc的保留率为82．6％,花青苷的保留率为57．5％。     

Ultrasonically Enhanced Osmotic Pretreatment of Sea Cucumber Prior to Microwave Freeze Drying

A new pretreatment method involving use of ultrasound prior to microwave freeze drying of sea cucumber was examined experimentally. It was observed that ultrasound-assisted osmotic pretreatment can reduce by about 2 h the time needed for microwave freeze drying. An optimization study using response surface analysis was carried out to determine the optimal operating parameters to minimize drying time while maximizing quality.     

Spray Freeze Drying in a Fluidized Bed at Normal and Low Pressure

The aim of this study is to develop the spray freeze drying process and its hardware and to investigate its capabilities to dry thermosensible substances such as pharma-proteins at normal and low pressures. As the result, the spray freeze fluidized-bed dryer was constructed. During the study, the drying kinetic comparison between classical and spray freeze-drying technologies was done. Spray freeze drying has shown short process times and allows advanced control, product particle shape and size uniformity, and high solubility. This shows that the fluidized-bed freeze-drying process could be an alternative for classical freeze-drying processes. Identified problems are the low yield of the primary drying phase and the strong electrostatic effects during the secondary drying step. However, the innovative process has shown an excellent capability to dry and stabilize the thermosensitive substances, such as pharma-proteins.     

Microwave-Assisted Thin Layer Drying of Wheat

Drying characteristics of Canada Western Red Spring (CWRS) wheat were studied using a domestic microwave convective oven. The effects of microwave power level, grain bed thickness, and initial grain moisture on the drying kinetics were investigated. Wheat samples with initial moisture levels of 0.18 to 0.29 kg water/kg of dry matter were dried for different drying periods of 180 to 360 s. The moisture loss data were recorded at regular short intervals. Then moisture loss data were fitted to various models (Page equation, modified drying equation, and Midilli equation) to study the drying kinetics of wheat. The results showed that wheat moisture loss increased with increasing microwave power level. A mathematical model was developed by coupling mass and energy balances, resulting in a system of non-linear equations. The predicted moisture loss data from the developed model were compared by fitting to experimental microwave data that were in good agreement.     

冷冻干燥法制备层状多孔羟基磷灰石支架过程中的溶剂升华行为

采用水基羟基磷灰石(hydroxyapatite,HA)浆料,经冷冻干燥和烧结工艺(1 250℃烧结3 h)制备了层状多孔HA支架.研究了冷冻温度、干燥压力和干燥温度对水基HA浆料中溶剂升华行为的影响.结果表明:随着冷冻温度的降低,多孔HA支架的层间距逐渐减小,支架的升华时间增加;由于样品的干燥过程同时受到传热和传质的...     

瓶装物料的冷冻干燥二维模型的建立与求解

本文对瓶装物料的冻干建立了一个考虑因素较为全面的二维数学模,该模型了侧面传热、结合水解吸和水蒸气温升对冻干过程的影响。根据冻干过程和模型方程的特点,本文把二循环对称分裂格式、预测－校正格式等算法联立起来对模型进行了数值求解,这些工作比目前的“只建模,不求解”或“虽求解,但模型简单、适用范围窄”的研究进行了一步。     

Microwave-Assisted Pulse-Spouted Vacuum Drying of Apple Cubes

Microwave-assisted pulse-spouted vacuum drying (MPSVD) of apple cubes was examined in a laboratory-scale apparatus. Aside from the drying time, structural and textural properties of the dried cube were measured. Results are compared with alternative drying techniques developed earlier in our laboratory. These include microwave-spouted bed drying (MSBD), microwave vacuum drying (MVD), and conventional vacuum drying (VD). Comparison is made in terms of the key quality parameters, viz. color, texture, apparent density, rehydration property, and sensory evaluation. Over the range of operating conditions tested, MPSVD apple cubes had the best color and significantly highest sensory evaluation score.     

耐火浇注料对流与微波干燥的实验研究

进行了耐火浇注料热重分析,热风和微波干燥实验研究,得到了浇注料热风和微波干燥特性曲线。实验结果表明,与热风干燥比较,微波加热极大地降低了耐火浇注料干燥时间、提高了干燥效率和能源效率高,在耐火浇注料干燥过程中有着广阔的应用前景。     

A Combination of Freeze Drying and Microwave Vacuum Drying of Duck Egg White Protein Powders

High energy consumption during freeze drying (FD) is a major concern that limits its application on common food product manufacturing. In this research, fresh duck egg white protein (FDEWP) powder and desalted duck egg white protein (DDEWP) powder were obtained by a combined two-stage tandem drying technologies (FD and microwave–vacuum drying [MVD]) in order to reduce energy consumption while maintaining good product quality. The results showed that the drying time for the FDEWP and DDEWP powders was significantly decreased by FD + MVD compared to those obtained by the FD-only process. The FDEWP powders dried by FD + MVD had a better color (higher L* and lower b*), lower apparent density, and lower foaming stability but higher emulsifying index than those dried by FD only. The DDEWP powder dried by FD + MVD had a product quality similar to that of FDEWP powder, suggesting that the DDEWP powder could be widely used as a food ingredient.     

草菇,菠萝的冷冻干燥过程及影响因素分析

从草菇、菠萝做冷冻干燥试验所得的冻干曲线和冻干时间,用分子运动论的观点分析了温度、压力等因素对冷干燥过程的影响。     

Characteristics of Milk Powders Produced by Spray Freeze Drying

Skim and whole milk powders were manufactured at lab scale by spray freeze drying (SFD), using liquid nitrogen as the cryogen. The polydispersity of droplet/particle sizes was limited using an encapsulator nozzle to atomize the feed. Particle morphology was examined using a scanning electron microscope. Samples were compared with equivalent spray-dried powders in tests of wettability and dissolution in water. The spray freeze-dried powders were found to be highly porous, with a uniform structure of pores throughout the entire particles. When tested in water, SFD skim milk powders wetted roughly three times as fast as industrially spray-dried agglomerated skim milk powders and were observed to dissolve rapidly by breaking down into smaller particles.     

关于真空冷冻千燥机新型环保制冷剂的思考简

本文首先叙述了国际上对制冷剂的分类,然后讲述了国内生产的真空冷冻干燥机采用环保型制冷剂的工作进程,最后介绍了欧盟对环保型制冷剂的最新要求及我们的对策及思考等。     

A Comparative Study on the Effect of Chemical,Microwave, and Pulsed Electric Pretreatments on Convective Drying and Quality of Raisins

In order to discourage the use of chemicals in raisin processing, the effect of microwave and pulsed electric field (PEF) pretreatments on the drying rate and other quality parameters like color, total soluble solids, bulk density, appearance, and market quality were compared with that of chemically pretreated raisins dried at 65°C. The untreated and pretreated samples had a statistically significant difference in drying rate (P < 0.05). The drying rate of chemically pretreated raisins was the highest when compared to others. The results showed that the PEF and microwave-treated samples had a significantly high Total Soluble Solids (TSS), along with good appearance and market quality.