Characteristics of Chard Leaves during Microwave, Convective, and Combined Microwave-Convective Drying

Chard leaves (Beta vulgaris L. var. cicla), which weighs 25 g with a moisture of 9.35 (db), were dried using three different drying methods, microwave, convective, and combined microwave-convective. Drying continued until leaf moisture fell down to 0.1 (db). Drying periods lasted 5-9.5, 22-195, and 1.5-7.5 min for microwave, convective, and combined microwave-convective drying, respectively, depending on the drying level. In this study, measured values were compared with predicted values obtained from Page's semi-empirical equation. Optimum drying period, color, and energy consumption were obtained for combined microwave and convective drying. The optimum combination level was 500 W microwave applications at 75°C.     

Microwave-Assisted Thin Layer Drying of Wheat

Drying characteristics of Canada Western Red Spring (CWRS) wheat were studied using a domestic microwave convective oven. The effects of microwave power level, grain bed thickness, and initial grain moisture on the drying kinetics were investigated. Wheat samples with initial moisture levels of 0.18 to 0.29 kg water/kg of dry matter were dried for different drying periods of 180 to 360 s. The moisture loss data were recorded at regular short intervals. Then moisture loss data were fitted to various models (Page equation, modified drying equation, and Midilli equation) to study the drying kinetics of wheat. The results showed that wheat moisture loss increased with increasing microwave power level. A mathematical model was developed by coupling mass and energy balances, resulting in a system of non-linear equations. The predicted moisture loss data from the developed model were compared by fitting to experimental microwave data that were in good agreement.     

Microwave,Vacuum, and Air Drying Characteristics of Collard Leaves

Collard leaves (Brassica oleracea L. var. acephala) with an initial moisture content of 6.65 on percentage dry basis (%db) were dried by three different drying methods: microwave, air, and vacuum. Samples of fresh leaves, 25 g each, were dried until their moisture was down to 0.1 on a dry basis. The following drying levels were used in each of the drying processes: 350, 500, 650, 750, 850, and 1000 W for microwave drying; 50, 75, 100, 125, 150, and 175°C for air drying; and 0.4, 50, and 100 mmHg at 50 and 75°C for vacuum drying, respectively. Drying times ranged between 2.5 to 7.5 min, 8 to 210 min, and 35 to 195 min for microwave, air, and vacuum drying, respectively. The data obtained compared well with a thin-layer drying model. Microwave drying at 750 W provided optimal results with respect to drying time, color, and ascorbic acid content (vitamin C).     

Optimization of Microwave-Vacuum Drying Parameters of Saskatoon Berries Using Response Surface Methodology

A combined microwave and vacuum system was used to dry the Saskatoon berries (Amelanchier alnifolia). A central composite rotate design and response surface methodology were used to determine the influence of process variables (microwave power, drying time, and fruit load) and arrive at optimal processing conditions to reduce the moisture content and water activity of the berries to a safe level. It is concluded that the yield of moisture content and water activity can be reduced to 20% and 0.50, respectively, for microwave power 5.7–6 kW, drying time 51.5–55 min, and fruit load 10–9.75 kg.     

Analysis of Energy Consumption in Drying Process of Non-Hygroscopic Porous Packed Bed Using a Combined Multi-Feed Microwave-Convective Air and Continuous Belt System (CMCB)

In this study, the analysis of energy consumption during the drying of non-hygroscopic porous packed bed by combined multi-feed microwave-convective air and continuous belt system (CMCB) was investigated experimentally. By using a combined multi-feed microwave-convective air and continuous belt system drier, the microwave power was generated by means of 12 compressed air-cooled magnetrons of 800 W each that give a maximum of 9.6 kW. The power setting could be adjusted individually in 800 W steps. Hot air with the maximum working temperature of 240°C was generated using 24 units of electric heater where the total power capacity is 10.8 kW. Most importantly, this work focused on the investigation of drying phenomena under industrialized microwave processing. In this analysis, the effects of the drying time, hot air temperature, porous structure (F-Bed and C-Bed), and location of magnetrons on overall drying kinetics and energy consumption were evaluated in detail. The results showed that the overall drying and energy consumption depend upon the porous structure, hot air temperature, and location of magnetrons. Furthermore, using the continuous microwave application technique had several advantages over the conventional method, such as shorter processing times, volumetric dissipation of energy throughout a product, and less energy consumption. The results presented here provided fundamental understanding for the drying process using a combined multi-feed microwave-convective air and continuous belt system in industrial size.     

Microwave-Convective and Microwave-Vacuum Drying of Cranberries: A Comparative Study

Abstract

Two drying methods of cranberries (microwave-vacuum and microwave-convective) are reviewed, and their advantages and disadvantages regarding the quality of dried product and the process performance are presented. Mechanically and osmotically pretreated berries were subjected to drying and quality evaluation. Quality parameters are color (in Hunter L*a*b* coordinates), textural characteristics (toughness and Young's modulus), and organoleptic properties (color, texture, taste, and overall appearance). Special emphasis was given to the energy performance of the process, monitoring of the real-time temperature profile, and the total microwave power-on time. Two microwave power densities are assessed, as well as different microwave power-on/power-off cycling periods. In almost all observed parameters, microwave-vacuum drying exhibited enhanced characteristics when compared to microwave-convective drying. Drying performance results (defined as mass of evaporated water per unit of supplied energy) showed that microwave-vacuum drying is more energy-efficient than microwave-convective. Tasting panel results exhibited slight preference in all parameters for microwave-convective dried samples.     

Development of a Microwave–Vacuum-Based Dehydration Technique for Fresh and Microwave–Osmotic (MWODS) Pretreated Whole Cranberries (Vaccinium macrocarpon)

A bench scale microwave–vacuum (MWV) dryer was developed using a modified consumer-grade microwave oven. MWV dehydration was first tested as a standalone method on whole frozen–thawed berries. Subsequently, a new combination drying technique was developed employing microwave osmotic dehydration under continuous-flow medium-spray (MWODS) conditions together with MWV as a secondary drying operation. Fresh (frozen–thawed) and MWODS pretreated berries were dried under a range of MWV treatments employing continuous and decreasing microwave power settings (duty cycles). Initial microwave power density for all treatments was approximately 10.2 W/g and magnetron power-on and power-off times varied from 3 to 15 s and 27 to 15 s, respectively. Drying times to 20% (db) were recorded and energy consumption was calculated according to the total magnetron power-on time where overall it was found that drying times and energy consumption decreased with increasing MWV process intensity, where drying times for all MWV treatments were significantly shorter than those of conventional air drying. Drying kinetics were fit using two models (exponential and Page's empirical model), where Page's model better fit the experimental data. The quality of the berries was monitored visually through evidence of scorching in order to screen treatments and establish upper limits of treatment intensity for further studies.     

Water migration in clay slabs during drying: A three-dimensional numerical approach

Clay products for construction offer durability, thermal and acoustic comfort as well as low cost. Drying is an important stage of the production process of these products, and it was studied herein. Experiments on convective drying of clay slabs with initial moisture content of 0.23 (db) were performed at 50, 60, 70, 80 and 90 °C. Drying occurred in two distinct periods: constant and falling rate. In the first period, the process was described by an empirical equation and, in the second one, by the diffusion equation with boundary condition of the third kind. To eliminate some restrictions found in the literature, a three-dimensional numerical approach was used to describe the process. Equations were obtained to express the process parameters as a function of the drying air temperature and local moisture content. A simulation using the values obtained from these equations for the process parameters is coherent with the experimental data.     

Microwave Drying Kinetics of a Thin-Layer Liquorice Root

Liquorice root (LR) (Glycyrrize glabra) is known as a sweetener and medicine plant. Drying kinetics of LR with initial moisture content of 49.5% (wet basis (w.b)) were experimentally investigated in a microwave drying system. The drying experiments were carried out at different drying temperatures (40, 45, 50, and 55°C) and microwave power levels (250, 500 and 750 W). Several models from literature were selected to fit the experimental data. The fit quality of models was evaluated using the coefficient of determination (R²), sum square error (SSE), and root mean square error (RMSE). A new model has been proposed for LR drying in the microwave drying. This new model best describes the experimental data for LRs. The activation energy was calculated to be 46.807 kJ/mol and effective diffusivity ranged from 2.9 × 10^?9 to 5.41 × 10^?9 m²/s, depending on drying temperatures at constant microwave power level.     

Characterization and Process Optimization of Microwave Drying of Plaster of Paris

The changes in the characteristics of plaster of Paris (pop) during drying operation under microwave irradiation conditions, namely surface morphology, effective moisture diffusivity, and absorption of microwave, were studied. The drying characteristics and kinetics of the process during microwave drying of plaster were studied for rectangular-faced cuboids (80 × 70 × 15, L × B × H in mm) through various drying parameters like microwave power input, initial moisture content, and drying time. Further, the experimental data on moisture ratio of plaster for different operating conditions were obtained and the optimization of the microwave drying process parameters was performed with response surface methodology (RSM) by considering all the above-said independent variables. Based on the RSM analysis, the optimum values of the process variables were obtained as: initial moisture content (A) 60%; microwave power input (B) 180 W; and drying time (C) 480 S.     

Comparison of two alternatives of combined drying to process blueberries (O'Neal): Evaluation of the final quality

In this work, we examined and compared two combined alternatives for the drying of blueberries (O’Neal). Pretreatments of osmotic dehydration (60°Brix sucrose solution at 40°C for 6 h) and hot air drying (HAD) (60°C, 2.5 m/s for 90 min) were performed to reach the same water content. Pretreated blueberries were then dried by microwave at different microwave output power values: 562.5, 622.5, and 750 W. The combined drying processes were also compared with HAD alone (control). The effects of the processes over blueberries were studied in terms of decrease in water content, drying rate (DR), mechanical properties (firmness and stiffness), optical properties (L*, a*, and hue angle (h)), antioxidant capacity, and rehydration capacity. The hot air–microwave drying decreased the process time and presented a high drying rate compared with the osmotic dehydration–microwave processes and the control drying. In terms of quality, the antioxidant and rehydration capacities were the most affected. The results showed that the best drying method to obtain the desired final product was the hot air–microwave drying (750 W).     

Energy Analysis of Poly-hydroxybutirate (PHB) Drying Using a Combined Microwave/Rotating Pulsed Fluidized Bed (MW/RPFB) Dryer

The aim of this study was to investigate the drying kinetics and energy efficiency of a combined microwave/rotating pulsed fluidized bed (MW/RPFB) dryer to dry particles of poly-hydroxybutirate (PHB). In order to analyze the effects of microwaves and hot air conditions on the drying kinetics of PHB and energy efficiency, an experimental design technique was applied. Drying energy efficiencies were in the range of 12–30%, and an estimated value of 10.5% was found for pure convective drying of PHB in an RPFB with the same final moisture content.     

Analysis of Energy Consumption in Drying Process of Biomaterials Using a Combined Unsymmetrical Double-Feed Microwave and Vacuum System (CUMV)—Case Study: Tea Leaves

An energy analysis of drying of biomaterials (tea leaves) was conducted on a combined unsymmetrical double-feed microwave and vacuum system (CUMV) to optimize the operating conditions and quality of the products. Tea leaves were dried from an initial moisture content of 172 to 7% (db). An energy consumption model based on the first law of thermodynamics was developed to evaluate energy efficiency. The influences of microwave power, vacuum pressure, and microwave operation modes on energy consumption were investigated in detail. The results showed that energy consumption as well as energy efficiency were strongly dependent on vacuum pressure and microwave power. Energy consumption and color parameters of the tea leaves were compared at different drying conditions. In particular, the experiments were carried out at different microwave powers (800 and 1,600 W) at a frequency of 2,450 MHz and different vacuum pressures (535 and 385 torr) to investigate the effects of these factors on the microwave–vacuum drying.     

Effect of Convective Air Attributes with Microwave Drying of Soybean: Model Prediction and Experimental Validation

The heat and mass transfer that occurred during drying of soybeans by a combined process using microwave (MW) and convective hot air was studied. A coupled mathematical model was developed to simulate this phenomenon. The soybean samples were re-wetted to 20% wet basis, the selected level of initial moisture content (IMC), and then dried in a domestic microwave oven under various MW power levels from 300 to 390 W, using inlet air with relative humidity of 35, 55, 75, and 95%. The simulated moisture loss profiles obtained from the coupled model compared well with those obtained in the experiments. Results showed that the drying rate decreased from 6.235 × 10^?5 to 6.192 × 10^?5 kg water/(kg wb s) as the inlet air temperature increased from 30 to 60°C. Furthermore, the drying rate was observed to increase from 6.192 × 10^?5 to 6.211 × 10^?5 kg water/(kg wb s) as the relative humidity (RH) increased from 35 to 95%.     

Effective Diffusivity Determination Considering Shrinkage by Means of Explicit Finite Difference Method

Drying data of salted shark (Carcharhinus limbatus) muscle pieces samples, dried in a convective dryer, by using three different air conditions and two different air velocities, were treated by Fick's second law. The shrinkage during drying process was considered as a linear function of sample moisture. The Fick's second law equation was numerically solved by the explicit finite difference method to obtain effective diffusivity, considering shrinkage and with and without simplification of moisture content profile. The experimental data fitted very well independently of the simplification introduced on the moisture content profile. The best fit was obtained by considering volumetric average of sample moisture content. The effective diffusivity values calculated considering the shrinkage varied from 0.72 to 2.20 × 10^?10 m²/s with the mean relative deviation modulus from 1.02 to 6.51%. The activation energy expressed in function of air temperature varied from 3.42 to 19.23 kJ/mol.     

Microwave Drying Kinetics of Okra

In this work, the effects of power level and sample mass on moisture content, moisture ratio, drying rate, and drying time of Turkey okra (Hibiscus esculenta L.) were investigated using microwave drying technique. Various microwave power levels ranging from to 180 to 900 W were used for drying of 100 g of okra. To investigate the effect of sample mass on drying, the samples in the range of 25 to 100 g were dried at microwave power level of 360 W. To determine the kinetic parameters, the drying data were fitted to various models based on the ratios of the differences between the initial and final moisture contents and equilibrium moisture content. Among of the models proposed, Page's model gave a better fit for all drying conditions used. The activation energy for microwave drying of okra was calculated using an exponential expression based on Arrhenius equation and was found to be 5.54 W/g.     

Quality Evaluation of Microwave-Dried Packham's Triumph Pear

Abstract

The objectives of this work were to carry out the microwave and microwave-convective drying of pear, in order to preserve the quality by reducing the drying time of the fruit; to compare the kinetic with convective drying mode data and to fit the comparative data to models from literature. The effect of osmotic dehydration and the variation in the microwave power were analyzed at constant values of air temperature and velocity. The experimental data fit well the proposed kinetic model. The processed pear was evaluated with respect to water content, quantity of calcium, phosphorus and potassium, water activity and apparent density. The best results were found for the samples osmotically dehydrated and dried in the microwave-convective dryer. The osmotic dehydration and the short drying times were important to maintain sample characteristics.     

Estimation of Effective Moisture Diffusivity of Okra for Microwave Drying

The effect of microwave output power and sample amount on effective moisture diffusivity were investigated using microwave drying technique on round okra (Hibiscus esculentus L.). The various microwave output powers ranging from 180 to 900 W were used for the determination of effective moisture diffusivity for constant sample amount of 100 g okra. To examine the effect of sample amount on effective moisture diffusivity, the samples in the range of 25–100 g were dried at constant microwave output power of 360 W. By increasing the microwave output powers and decreasing the sample amounts, the effective moisture diffusivity values ranged from 20.52 × 10^?10 to 86.17 × 10^?10 and 34.87 × 10^?10 to 11.91 × 10^?9 m²/s^?1, respectively. The modeling studies were performed to illustrate the relationship between the ratio of the microwave output power to sample amount and effective moisture diffusivity. The relationship between drying constant and effective moisture diffusivity was also estimated.     

Microwave Heat Treatment of Spinach: Drying Kinetics and Effective Moisture Diffusivity

The effect of microwave drying technique on moisture content, moisture ratio, drying rate, drying time, effective moisture diffusivity, and porosity of spinach (Spinacia oleracea L.) were investigated. By increasing the microwave output powers (180–900 W) and the sample amounts (25–100 g), the drying time decreased from 18 to 3.5 min and increased from 7.7 to 25 min, respectively. To determine the kinetic parameters, the drying data were fitted to various models based on the ratios of the differences between the initial and final moisture contents and equilibrium moisture content versus drying time. Among of the models proposed, Page's model gave a better fit for all drying conditions applied. The activation energy was calculated using an exponential expression based on Arrhenius equation. The relationship between the drying rate constant and effective moisture diffusivity was also estimated and gave a linear relationship.     

Effect of Microwave Energy on Vacuum Drying Kinetics of Alginate-Starch Gel

Microwave energy drying under vacuum was investigated for alginate-starch hydrogel. Drying was conducted using 2450 MHz microwave energy at 25 mm Hg absolute pressure and different power levels; e.g., 300, 500, 700, 900, and 1100 watts. Drying was continued until final moisture content of the sample reached less than 1% wet basis. Moisture loss during drying was measured at 3-min intervals. Drying kinetics were used to describe both macroscopic and microscopic mechanisms of heat and mass transfer. Experimental drying kinetic data were fitted to a mathematical model. Experimental drying data points were fitted to an empirical model equation.