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Swapna Rabha Markus Schubert Michael Wagner Dirk Lucas Uwe Hampel 《American Institute of Chemical Engineers》2013,59(5):1709-1722
Gas hold‐up and bubble size distribution in a slurry bubble column (SBC) were measured using the advanced noninvasive ultrafast electron beam X‐ray tomography technique. Experiments have been performed in a cylindrical column (DT = 0.07 m) with air and water as the gas and liquid phase and spherical glass particles (dP = 100 μm) as solids. The effects of solid concentration (0 ≤ Cs ≤ 0.36) and superficial gas velocity (0.02 ≤ UG ≤ 0.05 m/s) on the flow structure, radial gas hold‐up profile and approximate bubble size distribution at different column heights in a SBC were studied. Bubble coalescence regime was observed with addition of solid particles; however, at higher solid concentrations, larger bubble slugs were found to break‐up. The approximate bubble size distribution and radial gas hold‐up was found to be dependent on UG and Cs. The average bubble diameter calculated from the approximate bubble size distribution was increasing with increase of UG. The average gas hold‐up was calculated as a function of UG and agrees satisfactorily with previously published findings. The average gas hold‐up was also predicted as a function of Cs and agrees well for low Cs and disagrees for high Cs with findings of previous literature. © 2012 American Institute of Chemical Engineers AIChE J, 59: 1709–1722, 2013 相似文献
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Huahai Zhang Zhongshan Guo Yuelin Wang Xiankun Shen Tiefeng Wang 《American Institute of Chemical Engineers》2023,69(3):e17843
The effects of particle concentration and size on hydrodynamics and mass transport in an air–water slurry bubble column were experimentally studied. When the particle concentration αs increased from 0% to 20%, the averaged gas holdup decreased by ~30%, gas holdup of small bubbles and gas–liquid volumetric mass transfer coefficient decreased by up to 50%, while the gas holdup of large bubbles increased slightly. The overall effect of particle size was insignificant. A liquid turbulence attenuation model which could quantitatively describe the effects of particle concentration and size was first proposed. Semi-empirical correlations were obtained based on extensive experimental data in a wide range of operating conditions and corrected liquid properties. The gas holdup and mass transfer coefficient calculated by the correlations agreed with the experimental data from both two-phase and three-phase bubble columns, with a maximum error <25%. 相似文献
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Air-holdup and heat transfer coefficient data are reported for the air-water and air-water-sand system as a function of air velocity in the temperature range 297-343 K as measured in a 0.305 m diameter bubble column operating in semi-batch mode and equipped with either a five- or seven-tube bundle. A 65 μm average size sand powder is used at concentrations of 5 and 10 mass percent in the slurry. Available correlations of gas holdup and heat transfer coefficients are examined on the basis of these data. These are found inappropriate and inadequate for representing these experimental data. Gas holdup data are well represented by an approach based on Nicklin's (1962) work, and heat transfer data are adequately represented by a simple semi-empirical expression. Accurate experimental data on additional systems are needed to develop a reliable heat transfer theory particularly for process representation at temperatures higher than ambient. 相似文献
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很多废水处理装置涉及非牛顿型流体中的多相流动和传质问题,研究其中的气液传质过程有助于实现装置的优化设计和高效节能运行。以鼓泡反应器内清水和不同质量分数的羧甲基纤维素钠(CMC)水溶液为实验对象,分别研究气相表观气速和液相流变特性对气泡尺寸分布、全局气含率和体积氧传质系数的影响。实验结果表明,液相的流变特性对其传质特性参数均有较大影响。与清水相比,CMC水溶液中气泡平均直径和分布范围更大;清水和CMC水溶液的全局气含率均随表观气速的增加而增大;CMC水溶液的体积氧传质系数随CMC水溶液质量分数的增加而减小。基于实验研究,得出修正的体积氧传质系数公式和适用于幂律型非牛顿流体流动体系氧传递过程的无量纲关联式,可很好地实现非牛顿流体流动的废水处理装置中气液传质参数的计算。 相似文献
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Gaku Okuma Daiki Kadowaki Tsuyoshi Hondo Akihiro Sato Satoshi Tanaka Fumihiro Wakai 《Journal of the American Ceramic Society》2017,100(3):867-875
Sintering stress and bulk viscosity were derived as functions of relative density from microtomographic images in viscous sintering of glass particles. Three methods were proposed to estimate the sintering stress from relative density, specific surface area, and average of curvature on pore surface, which were directly measured by X‐ray microtomography. The surface energy method gave valid value in the final stage of sintering, while the mixed method gave better estimation in the intermediate stage. For the initial stage of sintering, the sintering stress was calculated from the average contact radius and the average coordination number observed by X‐ray microtomography. The sintering stress at the final stage increased in free sintering, but it decreased in constrained sintering due to pore coarsening. The bulk viscosity was calculated from the shrinkage rate and the sintering stress. 相似文献
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Gas holdup and surface‐liquid mass transfer rate in a bubble column have been experimentally investigated. De‐mineralized water, 0.5 and 1.0% aqueous solutions of carboxy methyl cellulose (CMC), and 60% aqueous propylene glycol have been used as the test liquids. Effects of column diameter, liquid height to column diameter ratio, superficial gas velocity and liquid phase viscosity on gas holdup and mass transfer rate are studied. Generalized correlations for the average gas holdup and wall to liquid heat and mass transfer coefficients are proposed. These are valid for both Newtonian and pseudoplastic non‐Newtonian fluids. 相似文献
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An experimental and modeling study was carried out to understand the relationship between the viscosity of a multimodal latex and its particle‐size distribution (PSD) and polymer concentration. This study illustrates the inadequacy of existing models in predicting the viscosity of complex latices. It is shown that the latex viscosity at a fixed shear rate is very sensitive to the polymer concentration at high solids content and to the PSD. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 84: 1878–1896, 2002; DOI 10.1002/app.10511 相似文献
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了解离心泵内微气泡的发生特性,对于优化现有基于旋转流场的微气泡发生装置的性能、提高工业废水废气的污染物去除率至关重要。在考虑气泡破碎合并的前提下,通过将双流体模型(TFM)与群体平衡模型(PBM)进行耦合,求解离心泵内气液两相旋转流场,研究了入口体积气含率(IGVF)、入口气泡尺寸对泵内气泡沿程尺寸变化、出口气泡尺寸分布的影响,并结合Luo等的破碎合并模型分析成因。结果表明,随IGVF增加,叶轮内气体聚集引起局部气含率陡升,气泡由破碎主导转变为合并主导,而后在蜗壳内气含率恢复正常,气泡又变为破碎主导,总体上出口气泡尺寸逐渐增大。另外,入口气泡尺寸对出口气泡尺寸的影响对IGVF敏感,当IGVF较低时,随入口气泡尺寸增大,出口气泡尺寸先增大后减小;而当IGVF较高时,由于泵内气体聚集,入口气泡尺寸的影响并不明显。 相似文献
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R. F. Mudde 《American Institute of Chemical Engineers》2011,57(10):2684-2690
We present experiments on a bubble train in a 23‐cm‐diameter fluidized bed of a Geldart B powder. The bubbles are injected via a single capillary inserted in the bed. We use our double X‐ray tomographic scanner to measure the solids distribution in two parallel cross sections of the bed. We report data for four different heights of the measuring planes above the capillary outlet. The velocity of individual bubbles is found from the time of flight from the lower to the upper plane. We have done separate calibration experiments for the velocity. In this article, we present data for the size and velocity of individual bubbles. From the bubble velocity, we could obtain the vertical dimension of the bubbles. This makes it possible to measure the volume of each bubble. The results show that our scanner is capable of measuring properties of bubbles with a size of 2.5 cm and above. © 2010 American Institute of Chemical Engineers AIChE J, 2011 相似文献
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A comparative study of the effect of clay and titanium dioxide on the mechanical properties and permeability of nanocoated cotton fabrics 下载免费PDF全文
This paper explores a comparison of mechanical properties of nanocoated cotton fabric for coatings synthesized with two different additives: Tunisian natural clay and titanium dioxide. The natural raw clay is a mixture of various other simple clays (kaolinite, calcite, illite, and quartz) requires preparation. TiO2 and Tunisian clay were added to two different resins, polyacrylate and polyurethane, widely used for numerous textile improvements such as impermeability and brightness effects. The additives used offer the advantage of being nontoxic and widely available. First, we check the constitution of the nanocoatings via X‐ray diffraction. Then, a defined amount of the resulting solution is applied on a cotton fabric. Finally, we check the mechanical properties and barrier effects on the modified fabric. The results show that when a small amount of clay or TiO2 particles are added to resin, the tear, tensile, bursting, and abrasion strength and water and air barrier properties of the coated fabric are globally enhanced. However, the use of natural clay in the coating gives better results than TiO2. In fact, in terms of mechanical performance, it is two to nine times more efficient than the titanium dioxide coating, except for the barrier effect, which is exactly two times more efficient. © 2017 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2018 , 135, 45642. 相似文献
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Xiao Xu Xiao‐Ling Ge Yun‐Dong Qian Hua‐Lin Wang Qiang Yang 《American Institute of Chemical Engineers》2018,64(7):2689-2701
A planar cyclone is designed for visualizing bubbles in the cross‐section of a degassing hydrocyclone. The pressure distribution is studied through a series of experiments and Reynolds stress model simulations. The velocity distribution of the planar cyclone mostly exhibits the quasi‐forced vortex zone and boundary layer zone. The bubble dynamics are simulated using both Euler‐Euler and Euler‐Lagrange approaches, and the output is compared with the imaging results. The Euler‐Euler simulation provides more accurate predictions of the bubble trajectory. The histograms of residence time and traveling distance given by the Euler‐Lagrange approach exhibit a reasonably regular pattern. With higher values of the inlet Reynolds number, stronger forces acting on the bubbles lead to a decreased but more uniform residence time. © 2018 American Institute of Chemical Engineers AIChE J, 64: 2689–2701, 2018 相似文献
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Power consumption, gas holdup and oxygen mass transfer in agitated gas-liquid columns have been studied for an air-water system. Measurements have been carried out in a reciprocating plate reactor using five different types of perforated plates and in a stirred tank reactor with one, two and three Rushton turbines, a helical ribbon impeller with and without surface baffles. Each mixing vessel had an identical geometry with a working volume of 17 L. For reciprocating plate stacks, the gas holdup is a complex function of the perforation diameter, the frequency of agitation and the gas superficial velocity. For radial-type mixing devices, the gas holdup increases more rapidly with the speed of rotation for the helical ribbon. The power imparted to the fluid by the mixing device is independent of the gas superficial velocity for the plate stacks and the helical ribbon impeller for a given frequency or speed of agitation whereas it decreases for Rushton turbines. The correlation of the power consumption obtained for all mixing devices plotted against the reciprocating frequency or speed of rotation to the third power shows a linear fit. KLa values were correlated very well with the power input per unit volume and superficial gas velocity for all mixing devices. At lower power input per unit volume, KLa is a function of only the gas superficial velocity. At higher input power per unit volume, KLa increases rapidly with an increase in the intensity of agitation. Reciprocating plates with larger diameter perforations led to higher KLa values whereas the lowest KLa were obtained with the helical ribbon impeller. Correlations for one and three Rushton impeller assemblies were almost identical whereas measured KLa were much higher for the two-impeller assembly due to the presence of a highly mixed zone in the vicinity of the dissolved oxygen probe. 相似文献
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Rotor–stator reactor (RSR), an efficient mass transfer enhancer, has been applied in many fields. However, the hydrodynamic characteristics of liquid flow in RSR are still a mystery despite they are fundamental for the mass transfer performance and processing capacity. In view of the above, this paper studies the liquid–liquid flow and liquid holdup in RSR under various conditions with a high-speed camera. The paper firstly demonstrates two flow patterns and liquid holdup patterns that we obtained from our experiment and then presents in succession a flow pattern and a liquid holdup criterion for the transition of film flow to filament flow and complete filling to incomplete filling. It is found that experimental parameters, including rotor–stator distance, rotational speed and volume flow rate exert great influence on the average droplet diameter and size distribution. Besides, by comparison and contrast, we also find that the experimental values match well with our previous predicted calculations of the average diameter, and the relation between the average diameter and the mean energy dissipation rate. 相似文献
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Haruki Kobayashi Masatoshi Shioya Tomoya Tanaka Toshihira Irisawa Shinichi Sakurai Katsuhiro Yamamoto 《应用聚合物科学杂志》2007,106(1):152-160
Fracture behavior of amorphous poly(ethylene terephthalate) (PET) films added multiwalled carbon nanotube (MWCNT) has been compared with that of the PET films added with carbon black (CB) to elucidate the effects of the large aspect ratio of MWCNT. Fracture toughness has been evaluated using the essential work of fracture tests. Evolution of the crazes has been analyzed by conducting time‐resolved small‐angle X‐ray scattering measurements during tensile deformation of the films at room temperature using synchrotron radiation. CB and MWCNT increased the fracture toughness of the PET film by increasing the plastic work of fracture. This resulted from the effects of the fillers to prevent the localization of deformation upon the crazes formed at earlier stages of tensile deformation and to retard the growth of the fibrils in the crazes to a critical length. The CB particles provided a number of sites where the crazes were preferably formed due to stress concentration. In the case of MWCNT, on the other hand, the widening of the crazes formed at earlier stages was suppressed due to the bridging effect arising from the large aspect ratio of MWCNT. © 2007 Wiley Periodicals, Inc. J Appl Polym Sci 2007 相似文献
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Miriam Petitti Andrea Nasuti Daniele L. Marchisio Marco Vanni Giancarlo Baldi Nicola Mancini Fabrizio Podenzani 《American Institute of Chemical Engineers》2010,56(1):36-53
Local gas hold‐up and bubbles size distributions have been modeled and validated against experimental data in a stirred gas–liquid reactor, considering two different spargers. An Eulerian multifluid approach coupled with a population balance model (PBM) has been employed to describe the evolution of the bubble size distribution due to break‐up and coalescence. The PBM has been solved by resorting to the quadrature method of moments, implemented through user defined functions in the commercial computational fluid dynamics code Fluent v. 6.2. To overcome divergence issues caused by moments corruption, due to numerical problems, a correction scheme for the moments has been implemented; simulation results prove that it plays a crucial role for the stability and the accuracy of the overall approach. Very good agreements between experimental data and simulations predictions are obtained, for a unique set of break‐up and coalescence kinetic constants, in a wide range of operating conditions. © 2009 American Institute of Chemical Engineers AIChE J, 2010 相似文献