V部分替代Nb对含Co FINEMET型合金磁性的影响

研究了含Co的Finemet型（Fe.．5Co0．5）73．5Nb3Si13．5B9Cu1和（Fe0.5Co0．5）73．5Nb2V1Si13．5B9Cu1合金在不同温度纳米晶化后的磁性．结果表明,用V部分替代Nb对淬态（Fe0.5Co0．5）73．5Nb2V1Si13.5B9Cu1非晶合金的居里温度没有明显的影响,但是形成（Fe0．5Co0．5）7a．5Nb2V1Si13．589Cu1纳米晶合金使剩余非晶中Co的含量降低,导致初始磁导率在高温下快速衰减;用V部分替代Nb使（Fe0．5Co0.5）73．5Nb2ViSi13．5B9Cu1纳米晶合金中的晶体相含有更多的Co,增大了材料的饱和磁感应强度B8并显著提高了初始磁导率．     

FeCuNbSiB／丁基橡胶复合薄膜压磁性能的研究

利用模压成型法制备了Fe73.5Cu1Nb3Si13.5B9非晶粉体/丁基橡胶和Fe73.5Cu1Nb3Si13.5 B9纳米晶粉体/丁基橡胶复合薄膜,采用4284A阻抗分析仪在20～50℃测试温度范围内研究了复合薄膜的压磁性能.结果表明,复合薄膜在＜0.09MPa微应力、低于200kHz测试频率下压磁性能最好;升高测试温度使复合薄膜的压磁性能增加,非晶粉体/丁基橡胶复合薄膜在40℃时压磁性能最好,纳米晶粉体/丁基橡胶复合薄膜在50℃时压磁性能最好;在相同条件下,非晶粉体/丁基橡胶复合薄膜的压磁性能优于纳米晶粉体/丁基橡胶复合薄膜.     

FeCuNbSiBV非晶纳米晶合金带材压磁特性研究

研究了Fe71.5Cu1Nb3Si13.5B9V2非晶带材经不同退火工艺处理后的压磁特性,并对不同成分带材的压磁特性进行了对比分析。研究表明,在测试频率f=1 kHz、压应力σ≤0.2 MPa条件下,Fe71.5Cu1Nb3Si13.5B9V2非晶带材闭合回路的电感值随压应力的增大而增大,带材具有良好的压磁稳定性,当退火温度为550℃时,带材的压磁特性稳定性最好,电感值与加载时间、SI(%)与压应力均具有良好的线性关系;热处理工艺对Fe71.5Cu1Nb3Si13.5B9V2带材的压磁性能具有显著影响,退火工艺为300℃×30 min时SI(%)达到最大值0.183;带材的压磁效应与其成分有关,相同测试条件下,Fe73.5Cu1Nb3Si13.5B9带材具有最大的压磁效应,Fe78Si9B13带材次之,Fe71.5Cu1Nb3Si13.5B9V2带材压磁效应最小。     

薄带宽度对(Fe_(0.9)Co_(0.1))_(76.9)Cu_(0.6)Nb_(2.5)Si_(11)B_9非晶合金阻抗效应的影响

研究了薄带宽度对(Fe0.9Co0.1)76.9Cu0.6Nb2.5Si11B9非晶合金薄带阻抗效应的影响。样品长度为40mm,宽度分别为8和4.4mm。淬态下4.4mm宽的样品在f=3.75MHz的条件下达到最大值28%,而8mm宽的样品在f=4.34MHz的条件下达到最大值17%;各频率下4.4mm宽的样品的阻抗效应均8mm宽的样品。(Fe0.9Co0.1)76.9Cu0.6Nb2.5Si11B9非晶合金薄带阻抗效应远大于Co68Fe5Si12B15非晶合金阻抗效应。     

连续压应力下Fe基非晶合金带材的压磁效应

通过对Fe基非晶合金带材连续施加压力,测试其附近闭合回路电感变化,研究了Fe基非晶合金带材的电感式压磁效应。结果表明,通过测试Fe基非晶合金带材附近闭合回路电感变化可用来测试和表征Fe基非晶合金带材的压磁性能;在f=1kHz时,Fe基非晶合金带材压磁性能稳定性好,随着压力的增大带材压磁性能升高,在同一压力情况下,Fe73.5Cu1Nb3Si13.5B9带材压磁性能优于Fe78Si9B13带材;在f=100kHz时,Fe73.5Cu1Nb3Si13.5B9带材压磁性能稳定性优于Fe78Si9B13带材,并且Fe73.5Cu1Nb3-Si13.5B9带材在f=1kHz、压应力为0.69MPa时具有最佳的压磁性能;在压应力<0.1MPa条件下,随着压应力增大,线圈电感值Ls有一个剧增的上升趋势,铁基非晶带材压磁性能对微小应力更加敏感。     

硅橡胶表面状态的非晶带材压磁性能的研究

采用4284A阻抗分析仪,在0～1MHz频率范围内,研究了不同测试温度和退火条件下硅橡胶表面状态的非晶Fe73.5Cu1Nb3Si13.5B9带材的压磁性能.结果表明,非晶带材的阻抗变化|ΔZ|随着压应力和频率的增加而增加,对0.1MPa以下的微应力变化非常敏感;在13～37℃测试温度范围内,随着温度的升高,非晶带材压磁灵敏度增加,37℃时压磁性能最好;退火温度低于300℃时,非晶带材经300℃×0.5h退火处理后,其压磁性能最好.     

硅橡胶压磁复合材料力学性能纳米压痕实验研究

通过纳米压痕测试技术对非晶Fe73.5Cu1Nb3Si13.5B9/硅橡胶压磁复合材料薄膜的力学性能进行了研究,讨论了加载速率、保载时间、峰值载荷等试验参数对模量和硬度测试结果的影响.进一步分析了纳米压痕实验表征非晶Fe73.5Cu1Nb3Si13.5B9/硅橡胶压磁复合材料薄膜蠕变行为的可行性,通过合理确定压痕蠕变实验参数,获得该材料的蠕变应力指数.结果表明:相对峰值载荷,加载速率对测试结果影响更为显著,而保载时间对硬度和模量测试结果几乎没有影响.     

纳米晶FeCuNbSiB多层膜的巨磁阻抗效应研究

研究了纳米晶态下Fe73.5Cu1Nb3Si13.5 B9多层膜的巨磁阻抗(GMI)效应。研究结果表明纵向巨磁阻抗(LMI)效应在3MHz时取得最大值为44％,横向巨磁阻抗(TMI)效应在6MHz时取得最大值为46％。LMI与TMI随外磁场有不同的变化行为,TMI曲线具有阁值行为,超过阈值磁场后出现明显的磁阻抗效应。晶化后出现最大值阻抗效应所对应的频率下降,由非晶态下的13MHz下降为晶化后的3MHz。薄膜样品的磁阻抗效应与样品中磁矩的空间分布密切相关．磁矩垂直面向分布时。磁阻抗效应下降为5％     

一种新型压磁薄膜

在硅橡胶基体中复合非晶Fe73.5Cu1Nb3Si13.5B9粉体,制得一种具有压磁特性的复合薄膜,并对一些影响因素进行了初步探讨.实验表明,该复合薄膜具有灵敏的压磁特性,尤其在＜120kPa微应力,测试频率低于400kHz时,压磁效应最好.在相同测试频率下,压应力与应力阻抗值成正比关系;薄膜中非晶粉体越细、粉体含量越高,薄膜越薄,其压磁效应越大.     

FeCuNbCrSiB非晶合金的晶化及磁导率与温度的关系

对Fe6 8Cu1 Nb3Cr8Si1 0 B1 0 非晶合金在 40 0～ 5 40℃等温退火 1h后的晶化行为及初始磁导率 μi 与温度的关系进行了研究。结果表明 :用Cr取代部分Fe和Si的Fe6 8Cu1 Nb3Cr8Si1 0 B1 0 非晶合金经适当温度退火后可获得具有bcc结构的α Fe(Si)纳米晶 ,合金的居里温度 (Tc <15 0℃ )远低于Finemet合金的Tc(约为 3 40℃ ) ;合金在淬态和 40 0℃退火后的 μi T曲线上出现Hop kinson峰 ,经 5 0 0℃和 5 40℃退火后其 μi T曲线上Hopkinson峰消失 ,曲线具有明显的长尾特征。     

Influence of mould design on the solidification of heavy forging ingots of low alloy steels by numerical simulation

Ingot casting of a 6-ton, heat-treatable Cr–Mo low alloy steel was simulated using finite element method in three dimensions. Effects of casting parameters including bottom pouring rate, mould slenderness ratio, mould slope, and height and shape of the hot top isolate on solidification behaviour and crack susceptibility during subsequent hot forging of the ingot were investigated. The simulation model was validated against experimental data of two different ingot mould designs. Influences of the casting parameters on the riser efficiency and possible crack formation in the intersection of hot top and ingot body during subsequent open-die forging of the cast steel ingots were discussed. Results showed that pouring the melt under a constant rate, reducing the mould slenderness ratio, and using a proper design for the hot top isolate would all improve the riser efficiency and thereby possibly reduce crack susceptibility during subsequent hot forging.     

Study of the interface behaviour between MABS/TPU bi-layer structures obtained through over moulding

The strength of adhesion between two over-moulded polymers, methylmethacrylate–butadiene–styrene copolymer (MABS) and thermoplastic polyurethane (TPU) that constitute a bi-component laminar system has been the subject of study. Results showed that at the bi-layer interface the adhesive fracture toughness increases as temperature and surface roughness are increased. Roughness has been demonstrated to be the most important parameter defining adhesion strength and failure. With the increase of roughness the failure was observed to change from adhesive towards cohesive type. An increase in either the temperature or the pressure applied to the samples caused a rise in adhesion energy. However, pressure seemed to have a minor effect in comparison to temperature. Significant increments in adhesion were obtained after applying the corona discharge treatment (CDT) to the attaching surfaces resulting in adhesion strengths almost double those of non-treated systems.     

Thermal design and performance of the SCUBA-2 instrument 1-K and mK systems

Various research fields require large and complex instruments containing detectors operating at millikelvin temperatures. The materials and techniques traditionally used in cryogenics are often unsuitable for the demanding requirements of such instruments. We describe the thermal design and performance of the 1-K and millikelvin systems of the SCUBA-2 instrument. This is an astronomical “camera” operating at wavelengths of 450 and 850 μm. It is the largest and most complex instrument ever built for sub-mm astronomy, and the first to use a cryogen-free dilution refrigerator. The design consists of a mix of traditional techniques (but used in demanding situations) as well as novel elements. The thermal performance has been stable and very successful, and we hope that the details described here will be useful to the designers of future large instruments.     

非晶Sm5Fe74.3Nb1.5Si11.7B4.5C2.5Cu0.5合金经预退火后的晶化动力学的DTA研究

研究了非晶Sm5Fe74.3Nb1.5Si11.7B4.5C2.5Cu0.5合金经400℃，保温10min预退火后的晶化动力学。结果表明；该合金的晶化相为α-Fe固溶体和Sm2Fe17Cx金属间化合物，两相的晶化表观激活能分别为557KJ/mol和514KJ/mol，当晶化体积分数为60%时，α-Fe相的晶化激活能达极大值；Sm2Fe17Cx相晶化激活能则随其晶化体积分数的增加而逐渐减小。     

PMMA单分子膜成膜特性研究

研究了ＰＭＭＡ单分子膜的成膜特性及其结构．结果表明，ＰＭＭＡ能够在较大的表面压范围内形成稳定的单分子膜，并且具有不可重复压缩性、表面压力的各向异性和松驰特性．ＴＥＭ照片显示，ＰＭＭＡ分子链在单分子膜中是有序平行排列的     

共沉淀法合成La_(0.9)Sr_(0.1)Ga_(0.8)Mg_(0.2)O_(3-δ)及其性质的研究

采用共沉淀法合成了具有钙钛矿结构的中温固体电解质La_(0.9)Sr_(0.1)Ga_(0.8)Mg_(0.2)O_(3-δ)(LSGM),并用DTA-TGA和X射线衍射仪分析了LSGM材料中钙钛矿相的形成过程,采用SEM、交流阻抗谱等检测技术对LSGM电解质的结构及性能进行了表征.XRD分析结果表明,1200℃烧结后,粉体开始形成钙钛矿结构,随温度的升高粉体中杂相含量越来越少,于1450℃时形成了单一的钙钛矿相结构.     

HDDR工艺条件及均匀化处理对Nd12.6Fe69.3Co11.6 B6.0 Al0.5合金磁性能的影响

研究了HDDR工艺条件(包括HD温度、HD时间、DR温度、DR时间)对Nd12.6Fe69．3Co11.6B6．0Al0．5合金磁性能的影响；比较了均匀化处理和未均匀化处理的合金经HDDR工艺后磁性能的差异；通过对两种舍金原始态的XRD谱线分析，找出存在差异的原因。     

Fabrication of NiCr alloy parts by selective laser melting: Columnar microstructure and anisotropic mechanical behavior

NiCr alloy, because of its wide applications in electrical elements and dental field was widely studied in the past. In this work, NiCr cubes and tensile specimens were fabricated by using a new processing technique-selective laser melting (SLM). Microstructural and mechanical behavior characterization of SLM-processed NiCr components was performed. An unusual columnar microstructural architecture composed of 〈1 0 0〉 texture (corresponding to (2 0 0) plane) oriented the building direction was observed. Moreover, it was found that the columnar grain growth across the melt pools occurred during the SLM process and the growth trend became stronger with the decrease of the laser scanning speed. Associated with the microstructural characteristic, an anisotropic mechanical behavior at different reference planes (i.e., at the horizontal and vertical surfaces) was demonstrated for the samples fabricated using different processing parameters. The results showed that with increasing the laser scanning speed, the microhardness at the horizontal surface decreased, while at the vertical surface it increased; an increase of the yield strength (YS) and the ultimate tensile strength (UTS) was observed.     

Thermal Stability of Amorphous Hydride Mg_(50)Ni_(50)H_(54) and Mg_(30)Ni_(70)H_(45)

The thermal stability of amorphous ternary hydrides Mg_(50)Ni_(50)H_(54) and Mg_(30)Ni_(70)H_(45) and their corre-sponding amorphous binary alloys Mg_(50)Ni_(50) and Mg_(30)Ni_(70) were studied with X-ray diffraction(XRD) and differential scanning calorimetry(DSC). Samples of the amorphous alloys were preparedby mechanical alloying and the amorphous hydrides were obtained by charging the alloys with gas-eous hydrogen at 3.0 MPa and 423 K. It was found that the amorphous hydrides released most oftheir hydrogen before the crystallization of the essentially hydrogen depleted amorphous alloy. Thecrystallization temperature of amorphous Mg_(50)Ni_(50)H_(54) elevated and that of amorphousMg_(30)Ni_(70)H_(45) did not change in relation to the original binary amorphous alloy. This is very excep-tional for amorphous hydrides. The reason for the effects of hydrogen absorption/desorption on thecrystallization of amorphous alloys was discussed.