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1.
叶黄素是一种重要的抗氧剂,对视力有很好的保护作用。万寿菊花瓣中的叶黄素含量很高,是叶黄素提取的理想原料。超声波的空化效应可以破坏植物细胞而使溶剂渗透入植物细胞,加速细胞内物质的释放以达到缩短提取时间和提高提取效率的目的。本实验主要考察超声时间,超声功率,提取温度和料液比等因素对叶黄素提取效率的影响。 相似文献
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采用表面活性剂辅助-微波法提取金盏花的叶黄素。研究了表面活性剂种类及浓度、微波提取时间、温度、料液比对叶黄素提取率的影响。利用单因素法和响应曲面分析法研究表面活性剂辅助-微波法提取金盏花叶黄素的最佳条件为:浓度42mg·mL~(-1)的月桂酰肌氨酸钠(OLI-4208),料液比为1︰20 mg/mL,微波提取温度68℃,微波提取时间5 min,金盏花叶黄素的提取率可达70.35%。 相似文献
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微波-表面活性剂协同提取万寿菊叶黄素工艺研究 总被引:4,自引:0,他引:4
以提高万寿菊叶黄素的提取率为目的,采用单因数实验结合正交实验的方法.研究了微波-表面活性剂协同提取万寿菊花中叶黄素的丁艺.结果表明:万寿菊叶黄素的微波-表面活性剂协同提取最优工艺为:以乙酸乙酯为提取剂,表面活性剂Tween-20为最佳助萃取剂(质量分数为0.03%),提取固液比1∶60(g/mL),微波功率400 W,微波提取温度为60℃,提取时间2 min.在此工艺下,万寿菊叶黄素的提取量为3.209 mg/g. 相似文献
5.
叶黄素提取方法研究概况 总被引:2,自引:0,他引:2
叶黄素是一种天然的食品色素,又是一种很好的食品营养剂.近年来研究发现,其具有保护视力、预防动脉硬化、抗氧化、抗癌等作用,极具商业开发价值.本文介绍了叶黄素的性质,并详细阐述了叶黄素的提取方法,同时对其发展前景进行了展望. 相似文献
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从虾壳中提取虾青素工艺及其生物活性应用研究进展 总被引:8,自引:0,他引:8
虾青素是自然界中分布很广泛的一种叶黄素,具有很强的抗氧化作用和独特的生理功能,存在巨大的商业价值.从甲壳类动物加工下脚料中提取回收虾青索是虾青素生产的重要途径之一.简述了虾青素的结构、生物活性及应用的一些最新研究成果,探讨了从虾壳中提取虾青素的方法,介绍了碱提法、油溶法、有机溶剂法和超临界CO2萃取法. 相似文献
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叶黄素的提取及应用研究进展 总被引:11,自引:0,他引:11
叶黄素是一种天然的、具有双重功效(增色和营养)的食品、医药添加荆。综述了近年来国内外叶黄素的提取及应用研究进展,并提出了实现工业化需要深入研究的几个方面内容。 相似文献
11.
Seed roasting is practiced in the mustard oil industry in some areas of the world, and can affect the physicochemical properties
of the oil for further applications. This research studied the differences in oxidative stability, tocopherols, and carotenoids
during heating at 160 °C between oil extracted from roasted mustard seeds and that from unroasted seeds. The content of free
fatty acids, polar compounds (PC), and lutein were not significantly different between the roasted and unroasted seed oils
before heating. The fatty acid compositions of both oils were also similar, with high amounts of erucic, linoleic, and oleic
acids, moderate amounts of linolenic and eicosenoic acids, and low amounts of palmitic and stearic acids. However, the levels
of tocopherols and conjugated dienoic acids (CDA) were higher in the roasted seed oil. Heating increased the content of CDA
and PC in both oils, but decreased tocopherols and lutein. The rates of increase in CDA and PC and the degradation rates of
tocopherols and lutein during heating were lower in the roasted than in the unroasted seed oil. Overall, the increased thermo-oxidative
stability of the mustard oil by roasting the seeds before oil extraction was highly correlated with improved heat stabilities
for both tocopherols and lutein. 相似文献
12.
Andrew Proctor Sevugan Palaniappan 《Journal of the American Oil Chemists' Society》1991,68(7):493-495
The effectiveness of sequential isopropanol/hexane washes of increasing polarity for desorbing soy oil pigment (lutein) from
alkaline and acid rice hull ash was studied. Increasing the polarity promoted desorption of pigment. However, the amount of
pigment desorbed with each extraction decreased after washing with 2% isopropanol. More lutein was desorbed as the amount
of adsorbed lutein increased. Desorption from acid ash was greater than that from alkaline ash, which may be due to the absence
of potassium from acid ash. The data suggest that the adsorption sites, occupied by lutein, are not all equally accessible
to isopropanol, probably because of the irregular structure of the ash. 相似文献
13.
This paper established a viable process for the simultaneous reaction, extraction, and primary purification of lutein in marigold flower by the isopropanol–KOH aqueous two-phase system (ATPS). In this process, the liposoluble lutein esters were translated into water-soluble lutein by saponification reaction in ATPS and distributed to the top phase. Meanwhile, the water-soluble flavonoids in marigold were also extracted and distributed to the bottom phase. The concentrations of phase-forming isopropanol and KOH, the added mass of marigold flower powder, temperature, and time were investigated to evaluate their effects on the extraction and partition behaviour of lutein and flavoniods in ATPS. Under the optimal conditions (38% isopropanol, 18% KOH, 0.05 g of marigold flower powder, 500°C and 1.5 h extraction time), the leaching efficiency, extraction efficiency, and partition coefficient of lutein were 84.64%, 86.73%, and 5.115, respectively, and at this point, the saponification rate of lutein reached 93.98%. Meanwhile, the leaching efficiency, extraction efficiency, and partition coefficient of flavoniods were 96.68%, 78.31%, and 0.2167, respectively. This method shows the superiority to the conventional one for it can not only efficiently extract lutein in marigold flower, but also achieve a high saponification rate of lutein esters and simultaneously separate two major pigments. 相似文献
14.
Effects on lutein adsorption of adding polar solvents to silicic acid or to soy oil/hexane miscellas
Polar solvents limit adsorption of lutein from a soy oil miscella on silicic acid by competitive adsorption. Water and selected
alcohols were added to miscella and adsorbent to observe if the mode of adding solvent affected lutein adsorption. No differences
were produced by the method of addition. However, different mechanisms of limiting lutein adsorption were observed. Isopropanol
limited lutein adsorption by competitive adsorption. Water was less competitive because it was less soluble in the miscella
and was more thermodynamically stable as free water. Propanediol, a polyol, totally inhibited lutein adsorption by binding
silica particles together. This study may have implications for silicic acid adsorption of oil components from hydrolyzed
oils in which glycerides and free glycerol are present. 相似文献
15.
The chlorophyll and carotenoid pigment composition in 12 mono-variety virgin olive oils was examined every 30 d during 1 yr
of storage at 15°C in darkness. The oil authenticity parameters, as defined by the ratio of chlorophylls/carotenoids and the
ratio of minor carotenoids/lutein, remained stable throughout storage, irrespective of the variety and degree of ripeness
of the source fruit. The percent of violaxanthin, percent of lutein, and total pigment content, the classifying variables
chosen as the best possible discriminators among olive varieties, also remained stable during storage. The prediction model
for olive variety, which was based on a discriminant multivariate analysis of the observed values of these variables, gave
a correct classification in 99.6% of the oils analyzed. The discriminant criterion established remained valid after 1 yr of
oil storage. The detection of chlorophyll derivatives other than those associated with the physical extraction process was
seen as a quality index, as small, analytically detectable transformations in the structure of pigments were indicative of
oil storage. 相似文献
16.
Harold E. Pattee Albert E. Purcell 《Journal of the American Oil Chemists' Society》1967,44(5):328-330
A method for analysis of carotenoid pigments in peanut oil is described. The major carotenoid pigments found in peanut oil
were beta-carotene and lutein. A sample of oil from immature peanuts contained 60 μg of beta-carotene and 138 μg of lutein
per liter of oil. The total carotenoid concentration in oil from mature peanuts appears to be less than 1 μg per liter of
oil.
Contribution from the Departments of Botany and Food Science, North Carolina State Experiment Station, Raleigh, N. C., in
cooperation with the US Department of Agriculture, ARS, Market Quality Research Division, and SURDD. Paper No. 2273 of the
Journal Series.
MQRD, ARS, USDA.
SURDD, ARS, USDA. 相似文献
17.
Lutein and zeaxanthin are selectively accumulated in the macula of the retina, yet their bioavailability is influenced by
various dietary factors. Insights regarding the effects of dietary lipids on lutein micellization that is available for absorption
are limited. This study investigated the influence of vegetable oils on the relative efficiency of lutein micellization using
in vitro digestion procedure. Lutein dispersed in either olive oil (OO), corn oil (CO), soybean oil (SBO), sunflower oil (SFO),
groundnut oil (GNO), rice bran oil (RBO) or palm oil (PO) was subjected to simulated gastric and small intestinal digestion.
Results showed that the efficiency of micellization of lutein dispersed in olive oil exceeds the other vegetable oils. The
percent lutein micellization was in the order of OO > GNO > RBO > SFO > CO > SBO > PO. In comparison, the values for OO were
higher than GNO (11%), RBO (18.3%), SFO (19%), CO (21.7%), SBO (30.5%) and PO (35.2%), respectively. These results suggest
that OO rich in oleic acid may favor the incorporation of lutein into micelles at the intestinal level. To conclude, the type
of vegetable oil in which carotenoids are dispersed is important to achieve an enhanced bioavailable lutein. The correlation
between the micellizable lutein and fatty acid composition of vegetable oils are discussed. 相似文献
18.
Ana G. Pérez Carmen Romero Khaled Yousfi José M. García 《Journal of the American Oil Chemists' Society》2008,85(7):685-691
The use of four concentrations of common salt (NaCl) used as coadjuvant for the extraction of virgin olive oil has been tested
on a laboratory scale and the quality attributes of the oils obtained were compared to those obtained with talc as coadjuvant.
The oils extracted from Picual fruits after NaCl addition were not significantly affected in terms of the physicochemical
requirements established for extra virgin olive oil, the best level of quality of this produce. Addition of NaCl during the
extraction process was positively correlated with the presence of o-diphenol compounds and the stability of the oils obtained. Moreover the use of NaCl resulted in a significant increase in
contents of pigments (β-carotene, lutein and chlorophylls a and b) and volatile compounds in the oils. 相似文献
19.
A pretreatment process using alcohol for the removal of chlorophyll a, b and β‐carotene from Chlorella vulgaris was developed to improve the yield and selectivity of lutein in the extract obtained by supercritical carbon dioxide extraction. Supercritical carbon dioxide extraction was carried out after pretreatment in the pressure range of 20 to 40 MPa and the temperature range of 40 to 80 °C. Ethanol and methanol were selected as elution solvents, of which ethanol was found most suitable for the elution, or pretreatment, process. The amounts of lutein and other compounds were analyzed by HPLC with the mixture of methanol and THF as the mobile phase. The amount of lutein in the extract increased with pressure, but decreased with extraction temperature. The highest recovery percentage and the selectivity of lutein were around 52.9 ± 0.02 % and 43.1 ± 0.02 %, respectively, obtained from supercritical carbon dioxide extraction with pretreatment and ethanol entrainer at 40 MPa and 40 °C. 相似文献
20.
The amounts of the different carotenoids (lutein, lutein monoesters and diesters) in soybean and rapeseed oil were determined
through a combination of column chromatography and UV spectrometry. The lutein diesters in the oils have been isolated by
a combination of column and thin layer chromatography. Identification and determination of the amount of the various fatty
acids of the lutein diesters have been carried out by means of gas chromatography after transesterification of the fatty acids
to their methyl esters. Comparison of the fatty acids of the lutein diesters with those of the triglycerides of the oils revealed
a striking difference. First, the fatty acids of the lutein diesters have shorter chains than the triglycerides acids. Secondly,
the lutein fatty acids are more saturated than the fatty acids of the triglycerides of the corresponding oils. However the
amount of linoleic acid in the case of the fatty acids of the lutein diesters in rapeseed oil is greater than that in the
fatty acids of the triglycerides in rapeseed oil.
Deceased, October 26, 1971. 相似文献