FROM SINGLE PARTICLE TO FLUID BED DRYING KINETICS

The concept of a normalized single particle drying curve has been integrated into a generic, heterogeneous fluid bed model in order to describe batch fluid bed drying. Drying curves have been measured for both single particles and fluid beds. Two different coarse-grained materials, aluminum silicate and a technical product, have been used. In general, fluid bed drying curves appear to be predictible on the basis of single particle data and with the help of the model. Dificulties may arise mainly with particles of low sphericity and a large initial moisture content. Model parameters are in the range indicated by general fluidization literature. However, Sherwood numbers for particle-to-fluid mass transfer in the- fluid bed are significantly lower than the values for single particles. This can hardly be attributed to bubbling and bypassing, since these effects have been explicitly accounted for in the model.     

OSMO-CONVECTIVE DRYING OF GRAPES

In order to reduce browning of grapes during drying, a special drying method was developed and evaluated using a laboratory scale fluidized bed dryer. Fresh Thompson seedless grapes were initially dried by immersion in a fluidized bed of sugar. The mass ratio of grapes to sugar was 1:1. The flow rate of hot air (at 45 and 60^°C) was sufficient to fluidize the sugar bed, while grapes placed on the screen, 3 cm above the drying air distributor, remained generally stationary.

Due to the simultaneous osmotic and convection drying effects, the drying time was reduced by factor ∼1.5 as compared to drying under the similar conditions without added sugar. A special pre-treatment of dipping of grapes in ethyl oleate (2% solution in 0.5% sodium hydroxide) at 80†deg; C for 30 s further reduced the drying time by factor 2 in both cases. The color of osmo-convective dried grapes were comparable to that of sulfur dioxide treated grapes. The texture of osmo-convective dried grapes was more pliable (softer) than convective dried samples. The major problem associated with die osmo-convective drying of grapes on a sugar bed was the stickiness, caused by sugar, on the fruit surface. This was reduced by partially substituting sugar with semolina (maintaining a 1:1 ratio) to create fluidized bed.     

OSMO-CONVECTIVE DRYING OF GRAPES

ABSTRACT

In order to reduce browning of grapes during drying, a special drying method was developed and evaluated using a laboratory scale fluidized bed dryer. Fresh Thompson seedless grapes were initially dried by immersion in a fluidized bed of sugar. The mass ratio of grapes to sugar was 1:1. The flow rate of hot air (at 45 and 60^°C) was sufficient to fluidize the sugar bed, while grapes placed on the screen, 3 cm above the drying air distributor, remained generally stationary.

Due to the simultaneous osmotic and convection drying effects, the drying time was reduced by factor ～1.5 as compared to drying under the similar conditions without added sugar. A special pre-treatment of dipping of grapes in ethyl oleate (2% solution in 0.5% sodium hydroxide) at 80?deg; C for 30 s further reduced the drying time by factor 2 in both cases. The color of osmo-convective dried grapes were comparable to that of sulfur dioxide treated grapes. The texture of osmo-convective dried grapes was more pliable (softer) than convective dried samples. The major problem associated with die osmo-convective drying of grapes on a sugar bed was the stickiness, caused by sugar, on the fruit surface. This was reduced by partially substituting sugar with semolina (maintaining a 1:1 ratio) to create fluidized bed.     

Analysis of Fluidized Bed Drying Kinetics on the Basis of Interphase Mass Transfer Coefficient

A particular way to define fluidized bed drying kinetics on the basis of interphase mass transfer coefficient and the conception of general kinetic curve has been described. The presented method, which allows for minimization of laboratory tests, has been checked experimentally. The method for calculating of mass transfer interphase coefficient in the constant rate period of fluidized bed drying based on Kunii and Levenspiel bubbling bed model is shown.     

Analysis of Fluidized Bed Drying Kinetics on the Basis of Interphase Mass Transfer Coefficient

A particular way to define fluidized bed drying kinetics on the basis of interphase mass transfer coefficient and the conception of general kinetic curve has been described. The presented method, which allows for minimization of laboratory tests, has been checked experimentally. The method for calculating of mass transfer interphase coefficient in the constant rate period of fluidized bed drying based on Kunii and Levenspiel bubbling bed model is shown.     

SIMULATION OF DRYING SUSPENSIONS IN SPOUT-FLUID BEDS OF INERT PARTICLES

In spouted and spout fluid bed dryers, the suspension is spread into the bed of inert particles, covering these particles with a thin layer. As the inert particles circulate, this suspension layer is dried and must become brittle enough to break off by the particle attrition. The powder produced is then carried out by air. Problems with the spout stability, particle agglomeration and powder deposits inside the column should be overcome by controlling the drying operation. The present work is aimed at modeling and simulating the drying of suspensions, such as organic and biological pastes, in conical spout-fluid beds of inert particles. A computer program has been developed combining the air flow and particle circulation models with the mass and energy balances and the drying kinetic equations in order to describe this drying process. The effect of cohesive forces is also incorporated to the fluid flow model. Simulation results are analyzed and compared with experimental data reported in the literature. Implication of these results in drying suspensions is also discussed.     

KINETICS OF THE CLAY ROOFING TILE CONVECTION DRYING

Kinetics of the convection drying process of flat tile has been investigated experimentally in an industrial tunnel dryer. Several velocities of wet tile movement through the dryer were tested to obtain maximum allowable drying rate curve. As there are various models to describe the kinetics of convection drying, finding a model that would fairly well approximate the kinetics of the whole drying process was part of the research. Especially the polynomial and exponential models were tested.

It was found that exponential model of the type: B(t) = (a-B_e. EXP(-bt²) +B_et (-dB(t)/dt) = 2bt(B(t)-B_e significantly correlates the kinetics of the whole tile drying process.

Applying the maximum allowable drying rate curve obtained for flat tile in the first period of drying, a grapho-analytic model for the optimal conducting of the process has been developed.     

DRYING OF TOBACCO PARTICLES IN A MOBILISED BED

ABSTRACT

The drying performance of a novel device capable of mobilising a bed of fibrous materials is evaluated. The drying kinetic of the vegetable product used for this work, cut lamina tobacco particles, was determined from fixed bed experiments. A falling-rate period was observed for the entire drying curve. The results showed that the drying rate is controlled by internal mass transfer mechanism for gas superficial velocities above 0.8 m/ s. The proposed model is based on an effective liquid diffusion coefficient that varies with solids temperature according to an Arrhenius-type relationship. Batch drying experiments were carried out in the mobilised bed apparatus under various conditions of inlet air temperature, humidity and flowrate. Assuming perfect mixing and no internal resistance to heat transfer for the solids, the performance of the mobile bed can be predicted using the proposed internal liquid diffusion model     

Modeling and Simulation of Industrial PVC Drying in Fluidized Beds with Internal Heat Source

An engineering application case study on a two‐fluid flow model for the control of industrial drying operations is reported. The mathematical model of this process was numerically solved by a computer code developed in FORTRAN language and was validated through data taken from PVC drying performed in an industrial continuous fluidized‐bed dryer. The predicted steady‐state outlet temperature and PVC moisture content values agree with the real data observed on the industrial plant. This model was also used to predict the temperature and concentration profiles inside the dryer as a function of time as a response to the disturbances and variations on the PVC water content at the dryer inlet.     

A Quasi-stationary Approach to Drying Kinetics of Fluidized Particulate Materials

A modified quasi-stationary method has been proposed to describe drying kinetics of particulate materials dried in convective dryers with active hydrodynamic regimes. Both our own results and literature data were used. These include sliced celery, cranberry, diced carrot, wheat and polystyrene granules dried in four types of dryers: pulsed fluid bed dryer, fluid bed dryer with a mixer, spouted bed dryer with a draft tube, and vortex dryer. The method was validated by comparing experimental data with results of modeling in terms of a reduced moisture content and material temperature. A new form of the generalized drying curve has been proposed with the reduced time and the index of hydrodynamic intensity as parameters. The equations developed can be used to calculate the total drying time and determine the temporal variation of the moisture content and material temperature.     

DRYING OF TOBACCO PARTICLES IN A MOBILISED BED

The drying performance of a novel device capable of mobilising a bed of fibrous materials is evaluated. The drying kinetic of the vegetable product used for this work, cut lamina tobacco particles, was determined from fixed bed experiments. A falling-rate period was observed for the entire drying curve. The results showed that the drying rate is controlled by internal mass transfer mechanism for gas superficial velocities above 0.8 m/ s. The proposed model is based on an effective liquid diffusion coefficient that varies with solids temperature according to an Arrhenius-type relationship. Batch drying experiments were carried out in the mobilised bed apparatus under various conditions of inlet air temperature, humidity and flowrate. Assuming perfect mixing and no internal resistance to heat transfer for the solids, the performance of the mobile bed can be predicted using the proposed internal liquid diffusion model     

Batch Drying Kinetics in a Two-Zone Bubbling Fluidized Bed

This article deals with investigation and modeling of batch drying process of solids in fluidized bed apparatus. There has been used model of fluidized bed drying, which consists two zones: emulsion zone and bubbling zone with taking into consideration the presence of solid particles in the bubbles. The results of theoretical expectations that arise from simulation calculations have been verified with experimental data obtained with the use of fluidized bed dryer 0.225 m in diameter. A drying process of silica gel, sand, and ammonium sulfate has been tested. To verify the model, the concept of a generalized drying curve has also been employed.     

DRYING CHARACTERISTICS OF OSMOTICALLY PRETREATED CRANBERRIES—ENERGY AND QUALITY ASPECTS*

ABSTRACT

This study reports on finish drying of osmotically pretreated (dehydrated and sugar-infused) cranberries. The halved fresh berries pretreated in a standard osmotic solution (67.5 Brix at 50°C for 5 h) were then freeze-dried, vacuum-dried and air-dried in various dryers (cabinet-air-through, fluid bed, pulsed fluid bed, and vibrated fluid bed dryers) in order to identify the best drying technology. Energy consumption and product quality were chosen as the comparison criteria. The best product quality, quantified by the anthocyanins content, rehydration ratio, color and taste, was noted for freeze-dried berries. As all other drying methods gave similar, albeit slightly lower quality products than freeze-drying, the selection of a drying method could be based on the unit heat consumption. The vibrated fluid bed and the pulsed fluid bed should be favored because of the highest energy efficiency. Even though sugar infused into cranberries during osmotic pretreatment reduces drying rates during the second drying period as compared to untreated berries, osmotic dehydration reduces the total energy consumption on top of the preferential sensory characteristics of the final product.

     

Calculation of the Effective Diffusion Coefficients by Applying A Quasi-Stationary Equation for Drying Kinetics

A modified quasi-stationary equation for drying kinetics has been used to develop a method allowing calculation of the effective diffusion coefficient and tracing its variation with drying time. The method has been validated with experimental drying kinetics for wheat dried in a two-dimensional spouted bed, and with literature data on drying of tobacco lamina in a fixed bed, and on sliced celery in a pulsed fluid bed.     

HEAT AND MASS TRANSFER DURING DRYING OF A LIQUID FILM FROM THE SURFACE OF A SINGLE INERT PARTICLE

ABSTRACT

This paper presents the results of theoretical and experimental studies on drying of aqueous suspensions of finely dispersed solids sprayed over the surface of an inert ceramic sphere. The effects of temperature and air velocity on kinetics of heat and mass transfer as well as peeling off the layer of a dry material from the sphere surface are described. The mathematical model of a drying process based on simplified ?gradientless? approach to transfer phenomena is proposed. The adequacy of the model developed for drying of the wet coat from a single sphere to the real drying process taking place in a bed of particulate carrier is confirmed by results of drying of several organic dyestuffs in an industrial spouted bed dryer with inert particles.     

KINETICS OF THE CLAY ROOFING TILE CONVECTION DRYING

ABSTRACT

Kinetics of the convection drying process of flat tile has been investigated experimentally in an industrial tunnel dryer. Several velocities of wet tile movement through the dryer were tested to obtain maximum allowable drying rate curve. As there are various models to describe the kinetics of convection drying, finding a model that would fairly well approximate the kinetics of the whole drying process was part of the research. Especially the polynomial and exponential models were tested.

It was found that exponential model of the type: B(t) = (a-B_e. EXP(?bt²) +B_et (?dB(t)/dt) = 2bt(B(t)?B_e significantly correlates the kinetics of the whole tile drying process.

Applying the maximum allowable drying rate curve obtained for flat tile in the first period of drying, a grapho–analytic model for the optimal conducting of the process has been developed.     

PREDICTING THE ENERGY CONSUMPTION OF CONTINUOUS WELL-MIXED FLUIDIZED BED DRYERS FROM DRYING KINETIC DATA

ABSTRACT

Previous work has shown that it is possible to predict the size of a continuous welt-mixed fluidized bed dryer from batch drying curve measurements. This approach has been extended in the present study to include energy consumption calculations. A computer code was written to simulate the performance of the dryer and to determine its specific energy consumption E_s. Starting in this case with an isothermal bed batch drying curve, the program first calculates the mean solids residence time required under specified operating conditions. Mass and energy balances are then used to calculate the heat duty and E_s. The bed temperature was found to have a significant effect on specific energy consumption in all cases. However, the influences of air flowrate and humidity, and of solids loading, were shown to depend on the solids drying characteristics.     

A Learning Process Simulator for Fluidized Bed Dryers Application to Bentonite Drying

A fluid bed dryer simulator was developed under Excel 5 wlth Visual Basic for Applications environment The simulator iS based on a mathematical model describing heat and mass transfer in the dryer. The total model incorporates empirical models for the Drying Constant and the Residence Time. These empirical models are crucial in the total model efficiency. Thus a procedure for updating the parameters of the empirical models is provided. This procedure constitutes the 'learnhg' property of the simulator. Two databases are Supplied. The first contains laboratory drying data and it is used for tuning the Drying Constant empirical model. The second contains industrial drying data from the real operation of the dryer, and it is used for tuning the Residence Time empirical model. The experience from the industrial application of the simulator proved that the simulator is a powerful tool for flexible operation of an industrial dryer. This paper is presents the total mathematical model of the dryer, the learning concept, and the databases, including useful information concerning the drying kinetics of bentonite. A simulator outline is presented and typical capabilities and uses are briefly described. A case study for flexible operation of an industrial dryer is discussed.     

From hygroscopic single particle to batch fluidized bed drying kinetics

A new normalization concept for convective drying of hygroscopic particulates is introduced. Both, intraparticle drying kinetics and sorption equilibrium are considered separately, and integrated into a new heterogeneous fluid bed model for coupled heat and mass transfer. Experiments were carried out using spherical γ-Al₂O₃ particles. Sorption isotherms, as well as drying curves, for single particles and fluidized beds have been measured. Batch fluid bed drying curves appear to be predictable on the basis of single particle and material equilibrium data and with the help of the model. All model parameters are directly taken, or estimated from fluidization literature, without any fitting.