共查询到18条相似文献,搜索用时 141 毫秒
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综述了近10多年来常规光度法、催化动力学光度法、化学光度法、紫外光度法、流动注射光度法和荧光光度法测定铈的研究结果.指出在常规光度法中,碱性染料类二安替比林甲烷类显色剂灵敏度最高,但受高价离子干扰严重;化学发光光度法、流动注射光度法和催化动力学光度法测定铈的应用较少,应加强研究. 相似文献
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铌的光度分析试剂及其在光度分析中的应用 总被引:1,自引:0,他引:1
铌的分析测定对于航天、电子、通讯、能源等行业的发展都具有重大意义。近年来各种新试剂、新方法的不断涌现,使铌的光度分析有了新的进展。通过对铌的光度分析试剂予以综述,重点介绍了各类显色剂及其显色反应体系、相应光度分析方法的最大吸收波长、摩尔吸光系数、检测限、干扰情况及其应用。 相似文献
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Spraque-Dawley(SD)big rats with weaning weight of (195±15) g were randomly divided into 4 groups with 8 males and 8 females each group. One group drank de-ionized water served as control and also used for analysis with the background. The other three groups were cultured for five months by drinking de-ionized water with 3.0, 4.5 and 6.0 mg·L-1 Sm (NO3)3, respectively. Compared with the rats in control, it is found that the organs of the treated rats are apparently pathologically changed, such as liver swell, lung intumescence, peritoneum conglutination and hardness. Especially, in the high Sm group, the pathological percentage in liver and lung is up to 30%. The pathological changes in liver and lung show that rare earth Sm does hazard biological effects to animals. With increasing Sm concentration, the weight rate of organ/body has a tendency of increasing; the activity of superoxide dismutase (SOD) in liver and kidney decreases, but the maglonydiadehyde (MDA) concentration increases, indicating the abilities of anti-oxidation and the lipid per-oxidation inhibition degenerate, which leads to hard pathological changes in organs. Moreover, the relative weight rate of organ/body, the activity of SOD and the MDA concentration are remarkably lager in liver than in kidney and other organs, suggesting that the biological effect of Sm on liver is the greatest and Sm has a high affinity for liver. 相似文献
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Sixty-four Spraque-Dawley(SD)big rats with weaning weight of (195±15) g were randomly divided into 4 groups with 8 males and 8 females each group. One group drunk with de-ionized water served as control and was also used for analysis of the background. The other three groups rats were raised by de-ionized water containing low, middle and high concentrations of Sm for four months, then learning and memory tests were carried out in Y-electric maze. Compared with the control rats, the learning and memory of rats in low and middle groups shows a deterioration trend, exhibiting the function degradation of rats' brain. It may results from the rare earth elements through blood-brain barrier affecting the normal physiological functions of rats' brain. In addition, the activity of superoxide dismutase (SOD) in rats' brain decreases, while the content of malondialdehyde (MDA) concentration increases. The decreased SOD activity and the increased MDA mean the degeneration the ability of anti-oxidation in rats' brain, which are accordance with the degradation of learning and memory function of rats in low and middle Sm groups. 相似文献
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镧热还原氧化钐过程冶金动力学分析 总被引:3,自引:2,他引:3
讨论了镧热还原氧化钐过程的动力学环节,分析了还原过程镧—钐合金存在的可能性,采用反证法确定了制备金属钐温度下的动力学控速环节。依据确定的控速环节,很好地解释了相关文献工艺条件实验的结果。 相似文献
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Luminescent Properties of Samarium Ion in Calcium Molybdate 总被引:4,自引:0,他引:4
Trivalent samarium ion (Sm^3 ) activated calcium molybdate (CaMoO4) phosphor was prepared by solid-state reaction in air. The XRD pattern of the powder CaMoO4: Sm shows that the CaMoO4: Sm single phase is developed fully through our preparation procedure. The excitation spectrum of CaMoO4: Sm is composed of a broad absorption of host and some sharp lines of the f-f transition absorption of Sm^3 . Illustrated in photoluminescence spectrum, CaMoO4 doped with Sm^3 displays orange red emission that is ascribed to the inner 4f^5 electron transitions ^6H7/2(orange)and ^6H9/2(red)of Sm^3 . Different from the sites of Sm^3 in CdWO4, the Sm^3 ions substitute for the Ca^2 and form only one type emission center in the CaMoO4 crystal lattice. 相似文献