An Inexpensive Raman,Spectroscopy Setup for Raman,Polarized Raman,and Surface Enhanced Raman,Spectroscopy

Instruments and Experimental Techniques - We present a simple and inexpensive lab-built Raman spectroscopy setup. In the setup a low-cost laser diode is used as an excitation source, the dichroic...     

Torque detected broad band electron spin resonance

We present a novel technique to measure high frequency electron spin resonance spectra in a broad frequency range (30-1440 GHz) with high sensitivity. We use a quasioptical setup with tunable frequency sources to induce magnetic resonance transitions. These transitions are detected by measuring the change in the magnetic torque signal by means of cantilever torque magnetometry. The setup allows tuning of the frequency, magnetic field, polarization, and the angle between the sample and the external magnetic field. We demonstrate the capabilities of this technique by showing preliminary results obtained on a single crystal of an Fe(4) molecular nanomagnet.     

Four point bending setup for characterization of semiconductor piezoresistance

We present a four point bending setup suitable for high precision characterization of piezoresistance in semiconductors. The compact setup has a total size of 635 cm(3). Thermal stability is ensured by an aluminum housing wherein the actual four point bending fixture is located. The four point bending fixture is manufactured in polyetheretherketon and a dedicated silicon chip with embedded piezoresistors fits in the fixture. The fixture is actuated by a microstepper actuator and a high sensitivity force sensor measures the applied force on the fixture and chip. The setup includes heaters embedded in the housing and controlled by a thermocouple feedback loop to ensure characterization at different temperature settings. We present three-dimensional finite element modeling simulations of the fixture and discuss the possible contributions to the uncertainty of the piezoresistance characterization. As a proof of concept, we show measurements of the piezocoefficient pi(44) in p-type silicon at three different doping concentrations in the temperature range from T=30 degrees C to T=80 degrees C. The extracted piezocoefficients are determined with an uncertainty of 1.8%.     

Tunable eletro-optical modulators based on a split-ring resonator

We present a novel design of an electro-optical modulator setup, consisting of a mechanically tunable cavity which allows the modulation frequency to be varied over a broad range. The design is based on the frequently used geometry of a split-ring resonator which allows for high-efficiency sideband generation. Normally such a configuration has the limitation of a narrow excitation band width ( approximately 20 MHz). Our adjustable setup offers broad-range tunability over several hundred megahertz while still keeping the modulation efficiency. Such a widely tunable modulator may find applications in a variety of experiments in atomic physics.     

High pressure rheometer for in situ formation and characterization of methane hydrates

We present a novel setup for a high pressure rheometer operating with concentric cylinders geometry for in situ studies of hydrate formation and rheological characterization. The apparatus uses an external high pressure mixing cell to saturate water-in-oil emulsions with methane gas. The capability of mixing combined with a true rheometer design make this apparatus unique in terms of setup and sample formation. We have used the apparatus to form gas hydrates in situ from water-in-oil emulsions and characterize suspension rheological properties such as yield stress and shear-thinning behavior.     

An efficient setup for femtosecond stimulated Raman spectroscopy

We present an efficient and robust setup for femtosecond stimulated Raman (FSR) spectroscopy with 60 fs and 10 cm(-1) resolution. Raman pulses of 0.5-5 ps are tunable between 450-750 nm with energies 1-10 μJ. Experimental features of the setup, signal processing, and data treatment are discussed in detail to be readily reproduced in other labs. The setup is tested by measuring FSR spectra of stilbene in solution.     

A simple and accurate method for calibrating the oscillation amplitude of tuning-fork based AFM sensors

We have developed a simple and accurate method for calibrating the amplitude of vibration of quartz tuning fork sensors commonly used in atomic force- and near field optical-microscopy. Unlike interferometric methods, which require a complex optical setup, the method we present requires only a simple measurement of the electro-mechanical properties of the tuning-fork oscillator and can be performed in a matter of minutes without disturbing the experimental setup. Comparison with interferometric methods shows that an accuracy of better than few percent can be routinely achieved.     

Normalization schemes for ultrafast x-ray diffraction using a table-top laser-driven plasma source

We present an experimental setup of a laser-driven x-ray plasma source for femtosecond x-ray diffraction. Different normalization schemes accounting for x-ray source intensity fluctuations are discussed in detail. We apply these schemes to measure the temporal evolution of Bragg peak intensities of perovskite superlattices after ultrafast laser excitation.     

Grouping PCBs with Minimum Feeder Changes

In printed circuit board (PCB) assembly, the majority of electronic components are inserted by high-speed placement machines. Although the efficient utilization of the machinery is important for a manufacturer, it is hard to fully realize in high-mix low-volume production environments. On the machine level, the component setup strategy adopted by the manufacturer has a significant impact on the overall production efficiency. Usually, the setup strategy is formulated as a part type grouping problem or a minimum setup problem. In this article, we consider a hybridization of these two problems for the single machine case: The object function to be minimized includes a weighted sum of the number of part type groups (giving the number of setup occasions) and the number of feeder changeovers. We present algorithms for the problem and compare their efficiency.     

Piezoelectric and optical setup to measure an electrical field: application to the longitudinal near-field generated by a tapered coax

We propose a new setup to measure an electrical field in one direction. This setup is made of a piezoelectric sintered lead zinconate titanate film and an optical interferometric probe. We used this setup to investigate how the shape of the extremity of a coaxial cable influences the longitudinal electrical near-field generated by it. For this application, we designed our setup to have a spatial resolution of 100 microm in the direction of the electrical field. Simulations and experiments are presented.     

Note: Detection of a single cobalt microparticle with a microfabricated atomic magnetometer

We present magnetic detection of a single, 2 μm diameter cobalt microparticle using an atomic magnetometer based on a microfabricated vapor cell. These results represent an improvement by a factor of 10(5) in terms of the detected magnetic moment over previous work using atomic magnetometers to detect magnetic microparticles. The improved sensitivity is due largely to the use of small vapor cells. In an optimized setup, we predict detection limits of 0.17 μm(3).     

A versatile low-temperature setup for the electrical characterization of single-molecule junctions

We present a modular high-vacuum setup for the electrical characterization of single molecules down to liquid helium temperatures. The experimental design is based on microfabricated mechanically controllable break junctions, which offer control over the distance of two electrodes via the bending of a flexible substrate. The actuator part of the setup is divided into two stages. The slow stage is based on a differential screw drive with a large bending range. An amplified piezoceramic actuator forms the fast stage of the setup, which can operate at bending speeds of up to 800 μm/s. In our microfabricated break junctions this is translated into breaking speeds of several 10 nm/s, sufficient for the fast acquisition of large statistical datasets. The bandwidth of the measurement electronics has been optimized to enable fast dI/dV spectroscopy on molecular junctions with resistances up to 100 MΩ. The performance of the setup is demonstrated for a π-conjugated oligo(phenylene-ethynylene)-dithiol molecule.     

Simultaneous surface plasmon resonance and x-ray absorption spectroscopy

We present an experimental setup for the simultaneous measurement of surface plasmon resonance (SPR) and x-ray absorption spectroscopy (XAS) on metallic thin films at a synchrotron beamline. The system allows measuring in situ and in real time the effect of x-ray irradiation on the SPR curves to explore the interaction of x-rays with matter. It is also possible to record XAS spectra while exciting SPR in order to study changes in the films induced by the excitation of surface plasmons. Combined experiments recording simultaneously SPR and XAS curves while scanning different parameters can be also carried out. The relative variations in the SPR and XAS spectra that can be detected with this setup range from 10(-3) to 10(-5), depending on the particular experiment.     

High resolution 3D gas-jet characterization

We present a tomographic characterization of gas jets employed for high-intensity laser-plasma interaction experiments where the shape can be non-symmetrically. With a Mach-Zehnder interferometer we measured the phase shift for different directions through the neutral density distribution of the gas jet. From the recorded interferograms it is possible to retrieve 3-dimensional neutral density distributions by tomographic reconstruction based on the filtered back projections. We report on criteria for the smallest number of recorded interferograms as well as a comparison with the widely used phase retrieval based on an Abel inversion. As an example for the performance of our approach, we present the characterization of nozzles with rectangular openings or gas jets with shock waves. With our setup we obtained a spatial resolution of less than 60?μm for an Argon density as low as 2 × 10(17) cm(-3).     

A high sensitivity ultralow temperature RF conductance and noise measurement setup

We report on the realization of a high sensitivity RF noise measurement scheme to study small current fluctuations of mesoscopic systems at milli-Kelvin temperatures. The setup relies on the combination of an interferometric amplification scheme and a quarter-wave impedance transformer, allowing the measurement of noise power spectral densities with gigahertz bandwidth up to five orders of magnitude below the amplifier noise floor. We simultaneously measure the high frequency conductance of the sample by derivating a portion of the signal to a microwave homodyne detection. We describe the principle of the setup, as well as its implementation and calibration. Finally, we show that our setup allows to fully characterize a subnanosecond on-demand single electron source. More generally, its sensitivity and bandwidth make it suitable for applications manipulating single charges at GHz frequencies.     

Characterization of JEOL 2100F Lorentz-TEM for low-magnification electron holography and magnetic imaging

We present results that characterize the performance and capabilities of the JEOL 2100F-LM electron microscope to carry out holography and quantitative magnetic imaging. We find the microscope is well-suited for studies of magnetic materials, or for semi-conductor dopant profiling, where a large hologram width ( approximately 1 microm) and fine fringe spacing ( approximately 1.5 nm) are obtained with good contrast ( approximately 20%). We present, as well, measurements of the spherical aberration coefficient Cs=(108.7+/-9.6)mm and minimum achievable focal step delta f=(87.6+/-1.4)nm for the specially designed long-focal-length objective lens of this microscope. Further, we detail experiments to accurately measure the optical parameters of the imaging system typical of conventional holography setup in a transmission electron microscope. The role played by astigmatic illumination in the hologram formation is also assessed with a wave-optical model, which we present and discuss. The measurements obtained for our microscope are used to simulate realistic holograms, which we compare directly to experimental holograms finding good agreement. These results indicate the usefulness of measuring these optical parameters to guide the optimization of the experimental setup for a given microscope, and to provide an additional degree of practical experimental possibility.     

Note: Investigation of atom transfer using a red-detuned push beam in a double magneto-optical trap setup

We present our results on transfer of cold (87)Rb atoms from a vapor cell magneto-optical trap to ultrahigh vacuum magneto-optical trap (UHV-MOT) using a red-detuned continuous wave push beam in a double-magneto-optical trap setup. We find that use of retro-reflected red-detuned push laser beam results in higher number in UHV-MOT than the number obtained without retro-reflection of push beam.     

Portable chamber for the study of UHV prepared electrochemical interfaces by hard x-ray diffraction

We report on a new electrochemical cell setup, combined with a portable UHV chamber, for in situ x-ray diffraction using synchrotron radiation. In contrast to more traditional electrochemical sample preparation schemes, atomically clean and well-ordered surfaces are routinely prepared by UHV methods, even in the case of reactive elements or alloys. Samples can be transferred from larger UHV systems into the portable chamber without exposure to ambient air. They can then be studied successively in UHV, in controlled gas atmospheres, and in contact with electrolyte solutions under applied electrochemical potential. The electrochemical setup employs a droplet geometry, which guarantees good electrochemical conditions during in situ x-ray measurements combined with voltammetry. We present first experimental results of Cu deposition on GaAs(001) and on freshly produced nanometric Pd(001) islands on Cu(0.83)Pd(0.17)(001), respectively.     

An integrated fixture planning system for minimum tolerances

Fixture planning is an important aspect of process planning. The steps involved in automatic fixture planning are manufacturing feature recognition, setup planning and fixture configuration planning. In the present work, an integrated setup and fixture planning system is developed for minimum tolerances at critical regions using a data exchanged part model as an input. A platform-independent STEP-based automatic feature recognition system that can recognize both design and manufacturing features, including intersecting features is implemented. An automatic setup planning module is developed for generating setup plans for complete machining of a given component. A fixture planning module is developed applying the criteria of uniqueness, stability, accessibility and tolerance minimization. A case study is presented to demonstrate the capabilities and integration between the various modules of the system.     

Velocity-map imaging at low extraction fields

We present a velocity-map imaging (VMI) setup for photoelectron imaging that utilizes low electric extraction fields. This avoids any complications that could arise from electrostatic interactions between the extraction field and the molecular properties that are probed and has a minimal effect on the trajectory of ions in ion beam experiments. By using an attractive potential supplied to the detector, and keeping the electrodes at ground (zero) potential, we show that fringe fields between the VMI arrangement and the vacuum chamber can be eliminated, which is important in experiments on ions.