Forming regularity and relation between composition and property of B_2O_3-BaO-ZnO glass

1INTRODUCTION Colorplasmadisplaypanel(PDP)isakindofeligibleapparatusforlargearea,hang on wallhighdefinitiontelevisions,computermonitorsandvari ousdisplaypanelsforcivilianandmilitaryapplica tion[13].Comparedwithotherflatdisplaypanels,themarketperspectiveforPDPisrapidlygrowingbecauseoftheiradvantagessuchasthinthickness,lowdensity,largeareaandlargevisualangle[4,5].TheglasssubstratesandthedisplayelectrodesinPDParethemainpartsandplayaveryimportantroleinhighperformancePDP[6].Inordertopro t…     

Enzymatic Cell Isolation and Explant Cultures of Rat Calvarial Osteoblast Cells

1Introduction Osteoblastcellsplayakeyroleintheformation,se cretionandmineralizationoftheextracellularmatrixof bonetissues[1,2].Thesecellssynthesizeandreleasebone matrixandglucoprotein,andhelpthematrixcalcifiedto formbones[3].Osteoblastcellculturetechnique…     

Preparation and Characterization of Starch-g-PVA/Nano-hydroxyapatite Complex Hydrogel

1Introduction Biodegradablehydrogelshadattractedmuchattentioninrecentyearsduetotheiruniquecombinationofproper ties,suchasbiocompatibility,permeability,hydrophilici ty,andlowcoefficientoffriction[1].Poly(vinylalcohol)(PVA)waswater solubleanddegradable[2].I…     

Zinc Oxide Nanorods and Their Photoluminescence Property

1　IntroductionOne dimensional(1D)nanostructures,suchasnano tubes,nanowires,nanorodsandnanoribbons,haveattractedextraordinaryattentionfortheirpotentialapplicationsindeviceandinterconnectintegrationinnanoelectronicsandmolecularelectronics[1- 4].Thesemiconductingmetalox ideZnOisawideband gap (3.37eV)compoundsemi conductorthatissuitableforblueoptoelectronicapplica tions ,withultravioletlasingactionbeingreportedindisor deredparticlesandthinfilms[5 ].One dimensionalZnOnanostructureshavebeensynthe…     

Synthesis of Ni-Zn ferrite and its microstructure and magnetic properties

1 INTRODUCTION Ni-Zn ferrite with spinel structure is a versatile technological material due to their high-resistivity and low-eddy current losses, particularly suitable for high-frequency applications. Ni-Zn ferrites have been commercially used in recording heads, antennas rods, loading coils, microwave devices and telecommunication applications fields, and so on[1?2]. Ni-Zn ferrites are usually prepared by the conventional ceramic method[3] and the wet-chemical method[4?16]. The cerami…     

Ultrastructure Changes and Mechanism of Cancer Cells Induced by Inorganic Crystal Nanoparticles

1Introduction Itwasreportedthatnanoparticlescankillcancer cell[1],andTiO2nanoparticlescaninhibittheproliferation oftumorcells[2,3].Hydroxyapatite(HAP)nanoparticles wasreportedthatcouldinducethedeathofhepatoma cells[4,5].Buthowthecancercelldiedisnotstillun…     

Relationship between interfacial structure and property of steel-mushy Al-28Pb bonding-pate

1INTRODUCTION SteelAl28Pbbondingplateismadeupof steelplateandAl28Pballoylayer[13].Steelplate hasahigherstrength,andAl28Pballoylayerhasexcellentheatconductivityandperfectlubricating property.Thusthisbondingplateisanidealmate rialofneotypebearingwhichiswidelyneededinmachineryandautomobilefields[46].Forthis bondingplate,theinterfacialmechanicalproperty thatdeterminesthesafetyofproductisveryim portant.Thehighertheinterfacialmechanicalproperty,thesafertheproduct.Interfacialmechanicalpropert…     

Design and Fabrication of Drug Delivery Devices with Complex Architectures Based on Three-dimensional Printing Technique

1Introduction Drugdeliverydevices(DDD)playanimportantrole incontrollingthedrugreleaseinadesignedmanner[1].AsanimportantkindofDDD,theimplantableDDDmay beusedtotreatsomedeceases,suchasdiabetes,antibi oticadministration,immunization,andtheboneinfectio ns[2].…     

Measurement of Solubilities of o-Phenylphenol in Petroleum Ether and DDP in Acetone ＋ Water Solution

[(6oxide6H dibenze(c,e)(1,2)oxaphosphorin6yl)methyl]butanedioicacid(DDP,Fig.1a)isa flameretardantforco polymerizationtoformflame retardingpolymers[1].Theobtainedfireretardant poly(ethyleneterephthalate)(FR PET)demonstrat edsomefavorablepropertiesintermsofthermalsta bility,intrinsicviscosity,theresidualcharandlimit ingoxygenindex(LOI)value[1].AnFR PETfiber containingthephosphoruslinkingpendentgroupswill givenotonlysufficientflameretardancybutalsoex cellenthydrolysisresistance[2].Forthesy…     

钢丝增强AZ91复合材料的力学性能

为了提高AZ91镁合金的力学性能,采用浸入铸造法制备了体积分数为3.3%的不锈钢纤维增强AZ91复合材料,并在相同条件下对AZ91及其复合材料进行了热挤压处理.采用扫描电镜（SEM）和力学性能试验机分别对铸态和挤压态材料的显微组织、断口和拉伸性能进行了研究.结果表明：铸态AZ91及其复合材料的抗拉强度分别为250和240MPa.然而经过挤压后,钢丝增强AZ91镁合金的屈服强度和抗拉强度分别达到了375和428.6MPa,与挤压态AZ91和铸态AZ91复合材料相比,分别提高了50%、20%和57.6%、78.6%.同时挤压态复合材料的塑性变形量也显著提高.     

Microstructure and RRA treatment of LFEC 7075 aluminum alloy extruded bars

The microstructures after casting and extruding, the mechanical properties and electrical conductivity after RRA treatment of conventional DC casting and low frequency electromagnetic casting (LFEC) 7075 aluminum alloy were investigated. The results showed that finer grains which distributed more homogeneously was obtained in LFEC ingots compared with those conventional DC ingots. The extruded bars of LFEC alloy kept its fine grain features of original as-cast structure. In the RRA treatment, with the extension of second aging time, the tensile strength and hardness of alloy decreased, but the electrical conductivity increased. Meanwhile, as the second aging temperature raised, the phase change rate in precipitation also increased. Under the same conditions, extruded bars of LFEC alloy had better performance than that of conventional DC cast alloy. The optimum RRA heat treatment process was 120 ℃/24 h+180 ℃/30 min+120 ℃/24 h. The LFEC extruded bars acquired tensile strength 676.64 MPa, hardness 198.18, and electrical conductivity 35.7% IACS respectively, which were higher than that in the T6 temper, indicating that a notable RRA response takes place in LFEC extruded bars, whose second-step retrogression time was 30 min, and it was suitable for mass production.     

Microstructure and mechanical property of 2024／3003 gradient aluminum alloy

2024/3003 gradient aluminum alloy was prepared by semi-continuous casting using double-stream-pou-ring technique. The microstructures of the as-cast, pressed and heat-treated alloys were analyzed by scanning elec-tron microscope and transmission electron microscope. And the mechanical properties of the alloy in pressed and heat-treated states were studied. The results show that the ingots with diameter of 65 mm and external thickness about 5.5 mm are obtained when the temperatures of the melt in the internal and external ladles are 1 023 and 1 003 K, respectively, and the nozzle diameter is 2.0 mm. The microstructures of the as-cast alloy consist of α(AI) θ(CuAl2)q S(Al2CuMg) in the internal region and α(Al) MnAl6 in the external region. The phases found in the internal and external layers coexist in the transition zone. The transition layer is maintained after plastic deformation and heat treatment of the alloy. The tensile strength, yield strength and elongation of the alloy are 300 MPa,132 MPa and 16.0%, respectively, after T6 treatment. The tensile and yield strength are increased by 150.0% and 94.1%, respectively, compared with that of 3003 aluminum alloy. The maximum hardness in the internal region of 2024/3003 gradient aluminum alloy can be increased from HRF 55 in the pressed state to HRF 70 in the heat-treated state.     

挤压温度对固相再生ZM6镁合金组织和性能的影响

利用固相再生方法在挤压比为25：1的条件下,将ZM6镁合金屑分别在350℃、400℃、450℃和500℃温度下制备成试样,进行微观组织观察和力学性能测试。结果表明：当挤压温度为400℃时,ZM6耐热镁合金没有发生再结晶,合金中金属化合物在挤压过程中被打碎,均匀分布在基体中;当挤压温度为450℃和500℃时,ZM6镁合金发生部分动态再结晶;随着挤压温度的提高,合金的抗拉强度和延伸率提高;在挤压温度为500℃,合金的抗拉强度、屈服强度和延伸率分别为300．2MPa、142．9MPa和30％。合金室温拉伸断口主要表现为穿晶韧窝断裂。     

热处理工艺对Ti55531钛合金组织及性能的影响

为了进一步扩大Ti5551钛合金的应用与研究范围,采用β退火和固溶强化两种典型的热处理工艺,通过力学性能检测、显微组织分析和断口扫描分析,系统研究了不同热处理工艺对Ti5551钛合金棒材组织和性能的影响．实验结果表明：β退火态的组织满足强度和塑性匹配,断裂韧性KE值可达97．6MPa·m^-1/2,冲击AK值可以达到35J;固溶强化热处理后,强度达到1360MPa,塑性和断裂韧性相对较低．     

Al-5Fe-1.2Si-1Mg-0.6Cu-0.5Mn合金轧制变形行为及组织性能

为了细化Al-5%Fe基合金中粗大的脆性针状或针片状富铁相,采用电磁搅拌及固态挤压技术制备Al-5%Fe-1.2%Si-1%Mg-0.6%Cu-0.5%Mn合金轧制坯锭,研究Al-5%Fe基合金的轧制变形能力及合金的组织性能,并用热压缩实验模拟了铝铁合金在783~693K、变形速率为0.01~10s^-1条件下的热变形行为.结果表明：该合金高温变形时存在明显的稳态流变特征,流动应力对应变速率和温度敏感.板材力学性能较挤压态有大幅度提升,其室温下的抗拉强度和伸长率最高达到354.5MPa和7.6%,比挤压态分别提高了105.6%和184.6%.轧制对铝铁合金中富铁相的破碎作用十分明显.     

Effects of annealing on microstructure, mechanical and electrical properties of AlCrCuFeMnTi high entropy alloy

The multi-component A1CrCuFeMnTi high entropy alloy was prepared using a vacuum arc melting process. Serial annealing processes were subsequently performed at 590 ℃, 750 ℃, 955 ℃ and 1 100 ℃ respectively with a holding time of 4 h at each temperature. The effects of annealing on microstructure, mechanical and electrical properties of as-cast alloy were investigated by using differential thermal analysis （DTA）, X-ray diffraction （XRD）, scanning electron microscopy （SEM） and transmission electron microscopy （TEM）. The experimental results show that two C14 hexagonal structures remain unchanged after annealing the as-cast A1CrCuFeMnTi alloy specimens being heated to 1 100℃. Both annealed and as-cast microstructures show typical cast-dendrite morphology and similar elemental segregation. The hardness of alloys declines as the annealing temperature increases while the strength of as-cast alloy improves obviously by the annealing treatment. The electrical conductivities of annealed and as-cast alloys are influenced by the distribution of interdendrite re~ions which is rich in Cu element.     

Microstructures and mechanical properties of Mg-Ce-Zn-Zr wrought alloy

Microstructures and mechanical properties of Mg-2.0 ?-0.7 % Zn-0.7% Zr alloy were studied. The results of scanning electron microscopy show that Mg12 Ce phase mainly distributes at the grain boundaries. The fine Mg12 Ce phase can apparently elevate recrystallization temperature by preventing the grain boundary migration. No dynamic recrystallization occurs during the hot-extrusion. The mechanical properties of as extruded specimens are σb=278.5MPa, δ=12.0%, while those of the specimens annealed at 250℃ for 100 h are σb=272.6 MPa, δ=11.3%, which indicate that the alloy has good mechanical properties at room temperature.     

Microstructural characterizations and mechanical properties of Mg-8Sn-1Al-1Zn-xCu alloys

Microstructural characterization and mechanical properties of as-cast Mg-8Sn-1Al-1Zn-xCu（x=0wt%, 1wt%, 1.5wt% and 2.0wt%） alloys were studied by OM, Pandat software, XRD, SEM, DSC and a standard universal testing machine. The experimental results indicate that adding Cu to TAZ811 alloy leads to the formation of the AlMgCu and Cu3 Sn phases. Tensile tests indicate that yield strength increases fi rstly and then decreases with increasing Cu content. The alloy with the addition of 1.5wt% Cu exhibits optimal mechanical properties among the studied alloys. The improved mechanical properties can be ascribed to the second phase strengthening and fi ne-grain strengthening mechanisms resulting from the more dispersed second phases and smaller grain size, respectively. The decrease in ultimate tensile strength and elongation of TAZ811-2.0wt% Cu alloy at room temperature is ascribed to the formation of continuous AlMgCu and coarse Mg2 Sn phases in the liquid state.     

Effects of cerium on microstructure and mechanical properties of ZK60 alloy

ZK60-xcerium alloys were studied,where x mass fraction is 0, 0.52%, 0.94%, 1.51% and 1.98%, respectively. Influence of Ce contents and heat-treatment on microstructure and tensile properties was analyzed. The results show that cast ZK60 alloy containing no Ce has coarse crystal grains, and lots of segregation aggregates around the grain-boundary. However, the alloys containing Ce have refined grains, and grain-boundaries are purified at the same time. Obvious dynamic recrystallization occurs in tested alloys after hot-extrusion. Tensile strength heightens with the increase of Ce content, and grows higher after aging at 150℃ for 0 -24 h （T5 treatment）. Comparing tensile properties of investigated alloys in different states, it can be concluded that synthetical properties of the alloy with 1.51% Ce addition is the best of all. In extruded state, σb and δ of this alloy are 318.6 MPa and 14.4%, respectively. After aging for 24 h ,σb is 338.6 MPa and δ is 15.6%.