Micromagnetic Structure of Co-Rich Amorphous Microwires

1. IntroductionSince the discovery of amorphous materials theirmagnetic prOPerties have been eXtensively studieddue to a great deal of laterest for fundamental investigations and their enormous potelltial in technological applications (in sensors, transducers, magnetic screens). Co-rich amorphous wires are promising candidates for a variety of sensor applications.It is knownlll thst some importal magnetic characteristics for technical applications (for example,low field magnetoresistance, mag…     

铁基非晶及纳米晶合金纤维的研制

通过自主开发的熔融快淬炉制备出了铁基非晶合金纤维,研究了制备工艺参数对纤维几何尺寸、微观形貌的影响,结果表明:转轮线速度、线圈功率(熔体温度)及气氛等对其微观形貌和几何尺寸的影响较大,通过调整优化工艺参数可稳定地制备直径为10～40μm可调的非晶磁性纤维.通过适当热处理可得到双相纳米晶磁性合金纤维.     

不同直径玻璃包覆非晶微丝的制备及其磁性能

采用熔融拉丝法制备了直径范围分别在6.1～28.0μm和14.0～35.2μm之间的玻璃包覆非晶Fe基和Co基合金微丝, 测试了不同合金直径和不同玻璃包覆层厚度的玻璃包覆合金微丝样品的静磁性能. 结果表明: 轴向矫顽力和轴向剩磁比随着微丝直径的增大而降低, 随着玻璃包覆层的增大而升高; 径向剩磁比的变化趋势则相反. 微丝合金直径和玻璃包覆层厚度改变, 静磁性能变化的主要原因是作用在合金芯上的内应力的变化, 导致了具有不同磁畴结构的合金内芯区和合金外壳区体积比的改变.     

玻璃包覆Co68Fe4.5Si13.5B14非晶微丝的力学性能

以玻璃包覆Co68Fe4.5Si13.5B14非晶微丝为研究对象,对经氢氟酸溶液腐蚀不同时间的微丝和不同直径的原丝进行了力学性能评价和断口形貌分析。结果表明,玻璃包覆非晶微丝的断裂过程是弹性变形。外径为28μm、内径为8.8μm的微丝经氢氟酸溶液腐蚀,刚去掉玻璃包覆层时裸丝的抗拉强度最大,可达到3545MPa,应变量为1.96%;若微丝经酸液腐蚀仍存在玻璃层,当腐蚀时间为40s时,抗拉强度和延伸率达到该阶段的最大值,分别为724MPa和1.3%;同时玻璃包覆Co68Fe4.5Si13.5B14非晶微丝具有尺寸效应,微丝的抗拉强度随直径的减小而增大。     

An Overview of Hydrogen Interaction with Amorphous Alloys

Theories, experimental results and applications associated with hydrogen behavior in amorphous metals and alloys are reviewed. An emphasis is made on the potential use of these advanced materials for hydrogen storage technology. Therefore, several properties that are especially relevant for such applications are assessed. These include structural models for hydrogen occupancy, sorption characteristics, solubility, diffusion behavior and thermal stabilities. Hydrogen effects on the mechanical properties and fracture modes of glassy metals are also presented, and possible mechanisms of hydrogen embrittlement are discussed. Similarities and differences between hydrogen behavior in amorphous and crystalline metals and alloys are discussed in detail.     

Effect of Nuclear Quadrupole Interaction on the Relaxation in Amorphous Solids

Recently it has been experimentally demonstrated that certain glasses display an unexpected magnetic field dependence of the dielectric constant. In particular, the echo technique experiments have shown that the echo amplitude depends on the magnetic field. The analysis of these experiments results in the conclusion that the effect seems to be related to the nuclear degrees of freedom of tunneling systems. The interactions of a nuclear quadrupole electrical moment with the crystal field and of a nuclear magnetic moment with magnetic field transform the two-level tunneling systems inherent in amorphous dielectrics into many-level tunneling systems. The fact that these features show up at temperatures T<100 mK, where the properties of amorphous materials are governed by the long-range R⁻³ interaction between tunneling systems, suggests that this interaction is responsible for the magnetic field dependent relaxation. We have developed a theory of many-body relaxation in an ensemble of interacting many-level tunneling systems and show that the relaxation rate is controlled by the magnetic field. The results obtained correlate with the available experimental data. Our approach strongly supports the idea that the nuclear quadrupole interaction is just the key for understanding the unusual behavior of glasses in a magnetic field.     

浅析音速喷嘴装置中喷嘴间的相互影响

目前采用音速喷嘴作为传递标准的气体流量标准装置被国内外检测机构广泛使用。在使用时,将根据需要的流量使用单个或多个喷嘴组合。与国外音速喷嘴的实际应用相比较,国内装置在喷嘴的安装方式、结构排列和上游设计方面多有不同。在对装置进行不确定度评定时,需要考虑喷嘴间相互影响(包括数量和位置等)对流量不确定度的影响。本文基于国内两套音速喷嘴法气体流量标准装置,利用单个、多个喷嘴的组合,测得两组相近流量点下涡轮流量计仪表系数,计算出不同组合的仪表系数偏差。本文考虑了实验时各组实际体积流量差值的影响,利用曲线拟合的方法,拟合出涡轮流量计仪表系数特性曲线,给出拟合方程式。将流量不同带来的影响剔除,最终给出喷嘴间相互影响带来的偏差,两套装置得出由此影响带来的不确定度为0.02%和0.07%。因此,在对音速喷嘴装置进行不确定度分析时应考虑这一分量。此外,通过相近流量不同喷嘴的组合对流量计进行检测,可以发现和找出喷嘴的问题,也是一种装置期间核查的好办法。     

纳米阳离子微球与HPAM的相互作用

采用微乳聚合法制备一系列不同阳离子度的微球与HPAM复合形成一种新型调剖剂,通过透射扫描电镜及激光粒度分析测定出合成微球的初始粒径在50—100nm,水中膨胀后的粒径为l-3μm;使用微电泳仪分析了微球的表面电势,在阳离子度30％时达到最大;由于静电作用,阳离子微球和HPAM浓度在0．02％即发生絮凝反应;通过不同剪切下的粘度测定,发现静电作用可以大幅度提高体系的粘度;增~HPAM的水解度可以将体系粘度再提高约20％。岩心驱替实验表明,复合体系具有较好的调剖性能。     

玻璃包覆铁基微丝的微波电磁特性

本文研究了玻璃包覆非晶微丝FeCoMnSiB在微波频段的电磁特性用x射线衍射技术分析了退火前微丝和不同温度退火后微丝的组织结构分析结果表明，铁基微丝在退火前的组织是由纳米晶和非晶混合组成的，经过465～550℃等温退火1h后，微丝内部组织和电磁特性都发生了改变．把退火前和经过不同温度退火处理过的微丝按一定配比分别散乱混合在石蜡基体里制成同轴样品，采用矢量网络分析仪测试微丝在2GHz到18GHz频段的复介电常数和复磁导率，同时模拟计算不同厚度单层吸波涂层的反射吸收率．由退火前微丝填充组成的涂层中，最小反射率可达一30dB；当微丝经过490℃等温退火后，不同厚度涂层的反射率曲线出现了不止一个吸收峰，而且有的曲线上的吸收峰同时都小于-10dB，吸波的频率范围变宽．结果表明，玻璃包覆铁基微丝可作为电磁损耗材料，具有良好的微波吸收特性．     

Dipolar Magnetic Envelope Solitons

The possibility of existence of envelope solitons in dipolar coupled systems (particularly magnetic soliton in nuclear spin-system with dipole-dipole interaction) is proved. The expressions for the width, group velocity and shift of frequency of the soliton are obtained in both short and large wavelength limits. It is shown that large-wavelength envelope soliton's width depends only on its amplitude.     

ACIS与HOOPS图形平台的交互

介绍了ACIS与HOOPS图形平台各自的数据结构与特点,剖析了两者之间的交互,以开发的Dcam凸轮设计系统为例,进一步阐明了两者的沟通与协调过程,为基于ACIS与HOOPS双重平台的图形系统开发提供了方法.     

Magnetic Properties and MCE in Heusler-Type Glass-Coated Microwires

We prepared Heusler-type Ni–Mn–Ga glass-coated microwires with total diameters, D, from 16 until 65 μm consisted of a metallic nucleus with diameters, d, between 10 and 31 μm and surrounded by the glass coating by the Taylor–Ulitovsky technique and measured the magnetocaloric effect, MCE, by the recently introduced precise method allowing the detection of a change in the temperature, ΔT, with an accuracy of below 10^?3 K. As-prepared microwires did not show ferromagnetic ordering at least near room temperature. Annealing above 773 K even for few minutes results in drastic change of magnetic properties: annealed sample show magnetization versus temperature dependence typical for ferromagnetic behavior with the Curie temperature about 315 K. Analysis of the X-ray diffraction allows us to identify presence of cubic phase in as-prepared state with the space group Fm3m and some amount of the tetragonal phase with space group I4/mmm. We measured directly the MCE, ΔT, in annealed samples. Before glass removal, we observed ΔT≈0.06 K for sample 1 and 0.08 K for sample 2. After glass removal of sample 1, ΔT increased until 0.22 K. Observed MCE is associated with magnetic (paramagnetic–ferromagnetic) and probably structural (austenite–martensite) phase transitions. Temperatures of the peak values of MCE were found to be of ～318 K and ～309 K, respectively Use of the glass-coating fabrication technique allows fabrication of composite thin wires from the brittle Ni–Mn–Ga alloy that cannot be cold-drawn to create fibers by conventional methods.     

Fe-Si-B-P-C薄带和块体非晶态合金磁性能的比较研究

对Fe76 P5 (B0.5Si0.3C0.2)19非晶薄带和块体非晶态合金试样的磁性进行了对比研究.通过磁力显微镜对试样的磁畴结构进行了观察,结果显示非晶薄带和块体非晶态合金具有完全不同的磁畴结构.非晶薄带自由面的磁畴结构为带状,磁畴宽度较大,约为5μm;而块体非晶态合金的纵剖面磁畴结构密集,呈枝状分布,磁畴宽度较小.而磁畴结构上的差异解释了非晶薄带和块体非晶态合金在矫顽力及居里温度上的差别.     

玻璃包覆金属微丝的快速凝固制备及应用

玻璃包覆金属微丝具有耐蚀、耐高温、抗辐照及高绝缘性等特点,作为精密电子元器件用电磁线,具有重要的应用前景.综述了玻璃包覆金属微丝制备技术的发展现状、基本工艺原理、主要工艺参数以及玻璃包覆金属微丝材料的种类、微丝的形状尺寸与组织,介绍了玻璃包覆金属微丝在电气、电子工业以及复合材料制备等领域的用途.     

Interaction Between Domain Walls in Chiral p-Wave Superfluids

We calculate microscopically the interaction energy of domain walls separating degenerate ground states in a chiral p-wave fermionic superfluid. The interaction is mediated by the quasiparticles experiencing Andreev scattering at the domain walls. As a by-product, we derive a useful general expression for the free energy of an arbitrary nonuniform texture of the order parameter in terms of the quasiparticle scattering matrix.