快速凝固铝合金粉末透射电镜试样制备

本文通过对镀镍法实验装置的改进和工艺参数的优化,较成功地实现了快速凝固铝合金粉末透射电镜样品的制备。     

快速凝固耐热铝合金的现状和发展

采用快速凝固/粉末冶金技术可制备出含有大量过渡族元素的铝合金,这种铝合金具有优良的高温力学性能和热稳定性,并已发展成为一系列耐热铝合金。简要评述了耐热铝合金的研究现状、发展趋势及应用前景。     

快速凝固7000系超高强铝合金的研究现状

在对传统7000系高强铝合金分析的基础上,着重阐述了快速凝固超高强铝合金的发展过程、存在问题和研究现状.快速凝固技术可有效细化组织、提高合金元素的极限固溶度、抑制宏观和微观偏析,并提高超高强铝合金的综合性能,最后提出了快凝超高强铝合金的应用和发展前景.     

快速凝固/粉末冶金(RS/PM)高硅铝合金材料的研究

采用冷压 +热挤压工艺制备快速凝固高硅铝合金材料 ,并探讨了挤压温度、保温时间、挤压比等工艺参数对材料组织及性能的影响 .研究结果表明 ,与高硅铝合金铸造材料相比 ,本研究所制的材料硅相尺寸得到了显著细化 ,且分布更为均匀 ,材料的抗拉强度和延伸率有明显的提高 .采用光学金相显微镜、SEM、XRD等手段对快速凝固高硅铝合金粉末及大块材料的微观结构及相组织进行了深入研究 .     

快速凝固/粉末冶金高硅铝合金微观组织及拉伸性能

采用快速凝固／粉末冶金法制备Al-17Si-6Fe-4.5Cu-0.5Mg合金,并进行T6处理。利用现代测试手段对挤压态及T6处理态合金微观组织及拉伸性能进行研究。结果表明：采用这种工艺可使合金组织中第二相得到显著细化,经T6处理后第二相有粗化趋势,同时也有新相沉淀析出;合金拉伸性能主要表现在高温、低塑性及良好耐热性。     

快速凝固耐热铝合金焊接技术的研究现状

阐述了快速凝固耐热铝合金焊接研究现状,分析了快速凝固耐热铝合金的焊接性,讨论了钨极氩弧焊、电容放电焊、电子束焊、激光焊、摩擦焊以及钎焊在快速凝固耐热铝合金材料连接中的应用和存在的问题,指出具有高能量密度、低能量输入的电子束焊、激光焊以及摩擦焊适于快速凝固耐热铝合金的焊接.     

快速凝固锌铝合金微观形貌研究

利用单辊急冷法制备了一种锌铝合金，通过XRD分析表明，合金相组成主要为过饱和相α’和富锌相η，以及微量的介稳定相ε-CuZn4。ESEM及TEM观察结果发现，快速凝固所得合金晶粒为等轴晶，并且极其细化，甚至达到纳米级别，其中Si元素以特殊圆薄片状单质存在，较高含量的Si元素未出现偏析，均匀分散在基体中。     

喷射沉积快速凝固材料的研究及应用概况

喷射沉积是一种新型的快速凝固技术，近年来广泛应用于研究和开发多种高性能愉速凝固材料。简要介绍了喷射沉积技术的基本原理和特点，对其在快速凝固材料中的应用进行了综述。     

Potential New Matrix Alloys for production of PM Aluminium Foams

The powder compact melting technique for aluminium foam production as practised today accepts a certain mismatch between foaming agent decomposition and matrix alloy melting temperatures. This mismatch is believed to influence the pore structure in an unfavourable way. Adjustment of TiH₂ decomposition as well as liquidus and solidus temperatures of matrix alloys can be used to counteract it. Effects of TiH₂ thermal treatments are investigated using thermal analysis. TiH₂ variants gained via annealing treatments were used to produce aluminium foam precursor materials. As matrix for these specimens, aluminium based alloys with low liquidus and solidus temperatures were selected. Alloy systems considered include established combinations of aluminium with Cu, Mg, Si and Zn as well as special quaternary mixtures of these elements. First examinations presented include thermal analysis of alloys as well as studies on expansion vs. time and temperature relationships of precursor material based on new alloys and foaming agent variants.     

Microstructural Evolution of Rapidly Solidified Co-Mo and Ni-Mo Eutectic Alloys

Droplets of Co-37.6 wt pct Mo and Ni-47.7 wt pct Mo eutectic alloys were rapidly solidified during containerless processing in a 3 m drop tube. A kind of anomalous eutectic appears in these two eutectic alloys when undercooling is beyond 56 and 61 K, respectively. The two eutectic phases in anomalous eutectic were observed to grow in dendrite manner. The formation of anomalous eutectic is ascribed to the cooperative dendrite growth of the two independently nucleated eutectic phases. Current dendrite and eutectic growth theories are applied to describe the observed processes.     

雾化沉积Al—Cu—Mg合金的显微组织

本文采用雾化沉积技术制备了大块Ａ１—Ｃｕ—Ｍｇ合金快速凝固材料，对沉积态和经挤压及热处理后的材料组织进行了观察和分析。结果表明基体呈全部等轴晶并存在少量显微孔洞是沉积态组织的主要特征。过饱和固溶体、时效析出相以及变形和热处理过程中形成的弥散相构成了材料的主要强化相。     

粉末冶金泡沫铝的研究进展

泡沫铝是一种新型的超轻多功能材料。粉末冶金发泡法因能制备异型泡沫铝和泡沫铝芯三明治复合结构．可满足汽车、航天、航空和军工等领域的需求，已成为当前泡沫铝研究的热点方向.本文介绍了国内外粉末冶金泡沫铝方面的研究现状，指出了现存问题。并展望了今后的发展趋势。     

快速凝固镁合金的研究现状

简述了快速凝固镁合金的制备方法、组织结构及性能特征,介绍了国内外各合金系快速凝固镁合金的研究现状,并指出了当前研究存在的问题及发展动向.     

快速凝固铝硅合金材料及其在汽车中的应用

本文介绍了快速凝固技术的特点及在高硅铝合金中的应用潜力,综述了快速凝固高硅铝合金的制取方法及研究现状,扼要总结了快速凝固高硅铝合金在汽车工业中的应用,最后提出这一研究领域中存在的问题及发展前景。     

快速凝固Ni-Mo-Cr-B合金粉末的显微组织

运用 X 光,金相和透射电镜等显微分析技术观察分析了快速凝固 Ni-Mo-Cr-B 台金粉未的凝固组织,研究结果表明,粉未尺寸由大到小,其组织经历了共晶、枝晶,胞晶和非晶等一系列演变,高硼含量有助于非晶形成。     

Preparation and Structural Characterization of Rapidly Solidified AI-Cu Alloys

Rapidly solidified Al_(100-x)—Cu_x alloys(x = 5,10,1 5,25,35 wt%) were prepared and analyzed.High cooling rate increased the Cu solubility in 9.-AI matrix.The influence of the cooling rate on Cu solubility extension in Al was experimentally simulated.Thus the pouring was performed in metallic die and by melt spinning-low pressure(MSLP) technique.Melt processing by liquid quenching was performed using a self-designed melt spinning set-up which combined the cooling technology of a melt jet on the spinning disc with the principle of the mold feeding from low pressure casting technology.The thickness of the melt-spun ribbons was in the range of30—70 μm.The cooling rate provided by MS-LP was within 10~5—10~6 K/s after the device calibration.The obtained alloys were characterized from structural,thermal and mechanical point of view.Optical microscopy and scanning electron microscopy were employed for the microstructural characterization which was followed by X-ray analysis.The thermal properties were evaluated by dilatometric and differential scanning calorimetric measurements.Vickers microhardness measurements were performed in the study.In the case of the hypereutectic alloy with 35 wt%Cu obtained by MS-LP method,the microhardness value increased by 45%compared to the same alloy obtained by gravity casting method.This was due to the extended solubility of the alloying element in the α-AI solid solution.     

Microstructures and Mechanical Properties of Rapidly Solidified Mg-Al-Zn-MM Alloys

Mg-Al-Zn-M M （misch metal） alloy powders were manufactured by inert gas atomization and the characteristics of alloy powders were investigated.In spite of the low fluidity and easy oxidation of the magnesium melt,the spherical powder was made successfully with the improved three piece nozzle systems of gas atomization unit. It was found that most of the solidified powders with particles size of less than 50μm in diameter were single crystal and the solidification structure of rapidly solidified powders showed a typical dendritic morphology because of supercooling prior to nucleation.The spacing of secondary denrite arms was deceasing as the size of powders was decreasing.The rapidly solidified powders were consolidated by vacuum hot extrusion and the effects of misch metal addition to AZ91 on mechanical properties of extruded bars were also examined.During extrusion of the rapidly solidified powders,their dendritic structure was broken into fragments and remained as grains of about 3μm in size.The Mg-Al-Ce intermetallic compounds formed in the interdendritic regions of powders were finely broken,too.The tensile strength and ductility obtained in as-extruded Mg-9 wt pct Al-1 wt pct Zn-3 wt pct MM alloy wereσ-（T.S.） =383 MPa andε=10.6%,respectively.All of these improvements on mechanical properties were resulted from the refined microstructure and second-phase dispersions.