共查询到20条相似文献,搜索用时 9 毫秒
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二(β-丁氧甲酰乙基)锡二氯化物的合成新工艺 总被引:1,自引:0,他引:1
在水体系中用锡粉、丙烯酸丁酯等原料,直接合成二(β-丁氧甲酰乙基)锡二氯化物。对反应温度、溶剂、组分摩尔比、催化剂选择及催化剂用量进行了系统规律性试验。 相似文献
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周理 《中国化学工程学报》1986,1(1):107-119
A new strategy of finding the best set of tear streams is proposed in this paper.It includes lining upall the nodes of the net in the declining order of node weights,and then adjusting the node positions in thesequence such that the total weights of the counter streams minimilcd.The finally formed node sequenceindicates the computation order of the nodes,and the still existing counter streams constitute the tear set.Neither loop identification nor excessive matrix operations are needed in this procedure;therefore,it hasbeen the simplest reliable method of net decomposition to data,and this is demonstrated by seven well-knownexamples. 相似文献
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The separation of Pd(II) from Pt(II), Ir(III) and Rh(III) with trioctylphosphine oxide (TOPO) in heptane using centrifugal partition chromatography (CPC) has been investigated for the first time. The extraction of Pd(II) has been studied by CPC and batch solvent extraction. The distribution ratios for Pd(II) determined by both methods agree well. In low HCl concentrations (<0.1 M), the extracted species was PdCl2.(TOPO)2, irrespective of the chloride concentration, while at acid concentrations above 0.1 M, the Pd was extracted as the ion pair, 2(TOPO.H+).PdCl4 2-. Base line separation of Pd(II) and Pt(II) in CPC was obtained under a variety of chloride and HCl concentration with the average number of theoretical plates being 390 ± 40 at a flow rate of 0.47 ± 0.05 mL/min. 相似文献
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新法合成1,4 二羟基 2 萘甲酸,操作简便,溶剂消耗少,反应时间短,收率高。探索了影响反应产率的几种因素。 相似文献
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研究了 Ti和 Sb催化下不同的间苯含量的共聚酯 (PEIT)的酯化、缩聚反应。结果表明 :随着间苯含量的增加 ,PEIT的酯化反应诱导期缩短 ,酯化温度降低 ,缩聚反应诱导期增长。Ti催化的 PEIT酯化反应速率高于 Sb,而且缩聚反应诱导期比 Sb明显缩短。 相似文献
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阻燃剂型氢氧化镁生产新工艺研究 总被引:16,自引:0,他引:16
介绍了以白云石为原料制备阻燃剂用氢氢氧化镁的试验原理及工艺流程,讨论了试验条件对氢氧化镁性能的影响,与卤水,烧碱法比较,该方法具有原料来源方便,生产成本较低等特点。 相似文献