Short fatigue cracks in austempered ductile cast iron (ADI)

The growth of short fatigue cracks was investigated in an austempered ductile cast iron (wt% 3.6C, 2.5Si, 0.6Mn, 0.15Mo, 0.3Cu), austenitized at 870 °C and then austempered at 375 °C for 2 h. At stress amplitudes close to the fatigue limit endurance limit of 10⁷ cycles, subcritical crack nuclei initiated at graphite nodules. The crack nucleus decelerated and arrested after propagating a short distance. The position of an arrested crack tip was characterized using an electron backscatter diffraction technique, demonstrating that short fatigue cracks in austempered ductile cast iron (ADI) can be arrested by boundaries such as those between ausferrite sheaves or packets and prior austenite grains. Refinement of the prior austenite grain size decreased the size of subcritical crack nuclei. It is proposed that the arrest and retardation of short crack nuclei are controlled by the austenite grain size and graphite nodule size. This determines the fatigue endurance limit.     

On the fatigue damage micromechanisms in Si‐solution–strengthened spheroidal graphite cast iron

Graphite nodules in spheroidal graphite cast iron (SGI) play a vital role in fatigue crack initiation and propagation. Graphite nodules growth morphology can go through transitions to form degenerated graphite elements other than spheroidal graphite nodules in SGI microstructure. These graphite particles significantly influence damage micromechanisms in SGI and could act differently than spheroidal graphite nodules. Most of the damage mechanism studies on SGI focused on the role of spheroidal graphite nodules on the stable crack propagation region. The role of degenerated graphite elements on SGI damage mechanisms has not been frequently studied. In this work, fatigue crack initiation and propagation tests were conducted on EN‐GJS‐500‐14 and observed under scanning electron microscope to understand the damage mechanisms for different graphite shapes. Crack initiation tests showed a dominant influence of degenerated graphite elements where early cracks initiated in the microstructure. Most of the spheroidal graphite nodules were unaffected at the early crack initiation stage, but few of them showed decohesion from the ferrite matrix and internal cracking. In the crack propagation region, graphite/ferrite matrix decohesion was the frequent damage mechanism observed with noticeable crack branching around graphite nodules and the crack passing through degenerated graphite elements. Finally, graphite nodules after decohesion acted like voids which grew and coalesced to form microcracks eventually causing rapid fracture of the remaining section.     

Relation between microstructural heterogeneities and damage mechanisms of a ferritic spheroidal graphite cast iron during tensile loading

In this work, the influence of the metallic matrix heterogeneities and the spheroidal graphite nodules distribution on both crack initiation and propagation and damage evolution during tensile loading of ferritic spheroidal graphite cast iron is examined. The experimental methodology involves specialized metallographic techniques, step by step tensile loading, microscopic observation by using optical and scanning electron microscopy and three‐dimensional (3D) reconstruction of the graphite nodules distribution. The results show that the graphite nodules are the major heterogeneities responsible for inducing the development of cracks in the metallic matrix. Crack initiation is preferentially located at the irregular contour of graphite nodule cavities, ferritic grain boundaries and internodular areas highly strained. The final fracture involves cracks mainly propagating through the internodular ligaments of matrix‐nodule debonded areas belonging to the first‐to‐freeze zones resulting from the solidification process.     

Effect of intermetallic particles and grain boundaries on short fatigue crack growth behaviour in a cast Al–4Cu–3Ni–0.7Si piston alloy

The short fatigue crack growth behaviour in a model cast aluminium piston alloy has been investigated. This has been achieved using a combination of fatigue crack replication methods at various intervals during fatigue testing and post‐mortem analysis of crack profiles. Crack–microstructure interactions have been clearly delineated using a combination of optical microscopy, scanning electron microscopy and electron backscatter diffraction. Results show that intermetallic particles play a significant role in determining the crack path and growth rate of short fatigue cracks. It is observed that the growth of short cracks is often retarded or even arrested at intermetallic particles and grain boundaries. Crack deflection at intermetallics and grain boundaries is also frequently observed. These results have been compared with the long crack growth behaviour of the alloy.     

Influence of bulk damage on crack initiation in low‐cycle fatigue of 316 stainless steel

To investigate the effect of bulk damage on fatigue crack initiation, crack initiations due to low‐cycle fatigue of Type 316 stainless steel were observed by electron backscatter diffraction (EBSD) and scanning electron microscopy. The EBSD observations showed that local misorientation developed inhomogeneously due to the cyclic strain, and many cracks were initiated from the slip steps and grain boundaries where the local misorientation was relatively large. The crack initiations could be categorized into two types: enhancement of the driving force by geometrical discontinuity (slip steps and notches), and reduction of material resistance against crack initiation caused by accumulated bulk damage at grain boundaries. In particular, more than half of the cracks were initiated from grain boundaries. However, in spite of the significant bulk damage, the fatigue life was extended by removing the surface cracks under strain of 1 and 2% amplitude. The stress state at the microstructural level was changed by the surface removal, and the damaged portion did not suffer further damage. It was concluded that although bulk damage surely exists, the fatigue life can be restored to that of the untested specimen by removing the surface cracks.     

Effect of beta flecks on mechanical properties of Ti–10V–2Fe–3Al alloy

The effects of beta flecks on tensile properties and low-cycle fatigue life were investigated at room temperature for Ti–10V–2Fe–3Al alloy. It was found that beta flecks had a significant influence on tensile ductility and low-cycle fatigue life. The greater the volume fraction of beta flecks (P_A) or maximum area of beta flecks (S_max), the lower the tensile ductility and low-cycle fatigue life. Extensive scanning electron microscopy (SEM) and light microscopy (LM) observation showed that under tensile load, cracks preferentially nucleated at β grain boundaries of beta flecks, then grew, connected and propagated along grain boundaries to form characteristics of intergranular fracture and quasi-cleavage fracture. While under an alternating load, beta flecks acted as sites for low-cycle fatigue crack nucleation due to inhomogeneous alternating strains between soft GB and aged beta matrix. The presence of beta flecks accelerates both the crack nucleation and early crack propagation.     

Cyclic behaviour of 12% Cr ferritic‐martensitic steel upon long‐term on‐site service in power plants

The strain‐controlled and stress‐controlled low‐cycle fatigue behaviour of served 12% Cr ferritic–martensitic steel is conducted at room temperature. Continuous softening is observed at both control modes, and the fitting results show that the fatigue properties of 12% Cr steel are not reduced significantly after 230 000 h service at 550 °C/13.7 MPa. Scanning electron microscopy has been employed to investigate the microstructure evolution after long‐term service. It is proved that the decomposition of martensite laths structure and the coarsening of carbides at grain/lath boundaries are the main reasons why the pipe bursts after 180 000 h service at 550 °C/17.1 MPa. The fracture under both control modes has been observed by using scanning electron microscopy, and it indicates coarse carbides along grain/lath boundaries are favourable sites for micro‐crack nucleation and the secondary cracks along the fatigue striations are formed by the connection of micro‐cracks nucleated during fatigue behaviour.     

Damage propagation mechanism in low-cycle creep fatigue of Cu–Cr–Zr alloy

This paper describes a characteristic damage propagation mechanism in low-cycle creep–fatigue of Cu–0.7Cr–0.09Zr (mass%), as investigated by creep–fatigue tests including strain controlled fatigue and stress-holding type creep, and following microstructural observations by scanning electron microscopy (SEM). The total stress-holding time until rupture in the creep–fatigue test was shorter than one-tenth of the rupture life in the simple creep test, and the rupture life of the specimen in the creep–fatigue test was shorter than half of that in the simple fatigue test. The SEM images suggest that the connection between fatigue crack propagating along grain boundaries and intergranular creep voids rapidly accelerates crack propagation.     

Growth of short cracks during low and high cycle fatigue in a duplex stainless steel

Damage evolution during low- and high-cycle fatigue in an embrittled duplex stainless steel is characterized in this paper. Moreover, scanning electron microscopy observations (SEM) in combination with electron backscattered diffraction (EBSD) measurements and transmission electron microscopy (TEM) were employed in order to analyze microcracks formation and propagation. During low-cycle fatigue, microcracks initiate the ferrite phase either along slip planes with the highest Schmid factor (SF) inside the grains or at the α/α grain boundary. Then, microcracks propagation take place in ferrite or austenite grains with the highest SF. An analysis of the dislocation structure in the near-surface and in ferritic grains in the bulk of the specimen has shown that dislocation microbands are associated with microcrack initiation.In the high-cycle fatigue regime, damage generally initiates in the austenite by slip band formation followed by crack initiation either at an α–α boundary or at an α–γ boundary in the intersection of slip bands in the austenite. The microstructure in the austenite consists of a low density of dislocation pile-ups while the ferrite is practically inactive or develops only micro-yielding at boundaries.Despite the differences in both fatigue regimes, phase boundaries are an effective barrier against crack propagation because they delay the advance of the crack tip.     

Evolution of surface deformation during fatigue of PH 13-8 Mo stainless steel using atomic force microscopy

The relationship between microstructure and nucleation of fatigue cracks in PH 13‐8 Mo stainless steel was explored with the use of atomic force microscopy (AFM) that allowed an accurate quantitative characterization of the surface features. Fully reversed strain‐ controlled fatigue tests were performed at 0.4 and 0.6% strain amplitudes, and the evolution of the surface deformation was observed at various fractions of life. At 0.4% strain amplitude, fatigue surface damage occurred first in the shape of streaks about 4 nm deep that formed at the interface between martensite laths and at prior austenite grain boundaries, and eventually coalesced to form crack nuclei. The increase in strain amplitude to 0.6% led to the formation of large extrusions, on average between 2 and 5 μm long with heights between 10 and 200 nm, which were the preferred crack nucleation sites.     

High-temperature low cycle fatigue behavior of a gray cast iron

The strain controlled low cycle fatigue properties of the studied gray cast iron for engine cylinder blocks were investigated. At the same total strain amplitude, the low cycle fatigue life of the studied material at 523 K was higher than that at 423 K. The fatigue behavior of the studied material was characterized as cyclic softening at any given total strain amplitude (0.12%–0.24%), which was attributed to fatigue crack initiation and propagation. Moreover, this material exhibited asymmetric hysteresis loops due to the presence of the graphite lamellas. Transmission electron microscopy analysis suggested that cyclic softening was also caused by the interactions of dislocations at 423 K, such as cell structure in ferrite, whereas cyclic softening was related to subgrain boundaries and dislocation climbing at 523 K. Micro-analysis of specimen fracture appearance was conducted in order to obtain the fracture characteristics and crack paths for different strain amplitudes. It showed that the higher the temperature, the rougher the crack face of the examined gray cast iron at the same total strain amplitude. Additionally, the microcracks were readily blunted during growth inside the pearlite matrix at 423 K, whereas the microcracks could easily pass through pearlite matrix along with deflection at 523 K. The results of fatigue experiments consistently showed that fatigue damage for the studied material at 423 K was lower than that at 523 K under any given total strain amplitude.     

The structural-phase state changes under the pulse current influence on the fatigue loaded steel

Structure and phase transformations in Fe-0.6C-1Mn-2Si steel subjected to multicyclic fatigue tests under normal conditions and with intermediate electrostimulation are investigated by the methods of metallography of etched microsections and scanning and transmission electron diffraction microscopy of thin foils and carbon replica. It is demonstrated that fatigue failure under normal loading is preceded by complete dissolution of initial cementite particles with carbon localized on structural defects (dislocations, subboundaries, and boundaries), micropores, and microcracks. Electrostimulation, promoting the relaxation of stress concentrators through dissolution of particles localized on the grain boundaries and the state change of the interphase boundaries between the matrix and second-phase particle, causes the mean and maximum subcritical crack length to increase together with the thickness of the sample layer involved in the strain of the material and the zone of fatigue crack growth. This is accompanied by a significant increase in the operating lifetime of the material.     

Influence of microstructure on high-cycle fatigue behavior of austempered ductile cast iron

An investigation was carried out to examine the influence of austempering heat treatments and the resultant microstructure of austempered ductile cast iron, on the fatigue crack growth rate, fatigue threshold, and high-cycle fatigue strength of the material. Two different approaches were used to study the fatigue behavior of this relatively new material, that is, a traditional S-N curve approach for determination of fatigue strength and a fracture mechanics-based approach for determination of the fatigue threshold. Compact tension and cylindrical specimens prepared from alloyed nodular ductile cast iron were given three different austempering heat treatments to produce three different microstructures. The fatigue threshold and high-cycle fatigue behavior of these specimens were studied in room temperature ambient atmosphere. The results of the present investigation demonstrate that the fatigue threshold of the material increases with increase in volume fraction of carbon-saturated austenite. The fatigue strength of the material, on the other hand, was found to increase with decrease in austenitic grain size. The crack growth process in the material was a combination of ductile striations and microvoid coalescence, and crack propagation by connecting the graphite nodules along its path.     

Ductile cast irons: Microstructure influence on the fatigue initiation mechanisms

In the last decades, the combination of high mechanical performances and low production costs increased the industrial interest on ductile cast irons. These grades are often used for applications where the fatigue resistance can be a critical issue (eg, machine frames for the wind‐power industry or crankshaft used in trucks) and the investigation of the main damaging mechanisms during both the crack initiation and the crack propagation stage could offer new perspectives about these alloys. Ductile cast irons can be considered as a natural composite, being characterized by graphite elements (nodules) embedded in a more or less ductile matrix (ranging from fully ferritic to pearlitic, from martensitic to austempered). In this work, the fatigue crack initiation mechanisms were investigated considering different matrix microstructure and the presence of a mechanical properties gradient in the graphite nodules.     

Effect of microcracking on the micromechanics of fatigue crack growth in austempered ductile iron

The effect of microcracking on the mechanics of fatigue crack growth in austempered ductile iron is studied in this paper. The mechanism of fatigue crack growth is modelled using the boundary element method, customized for the accurate evaluation of the interaction effects between cracks and microcracks emanating from graphite nodules. The effects of nodule size and distribution and crack closure are considered, with deviation bounds of computed results estimated through weight-function analyses. A continuum approach is employed as a means of quantifying the shielding effect of microcracking on the dominant propagating crack, due to the reduction of stiffness of the material in the neighbourhood of the crack tip. Although the results obtained may not yield actual numbers for real cases, they are in accordance with experimental observations and demonstrate how the main factors affect the crack growth of the macrocrack.     

Experimental characterization of short crack nucleation and growth during cycling in lean duplex stainless steels

Considering that many applications of Lean Duplex Stainless Steels (LDSSs) involve cyclic loading, the aim of this paper is to study short crack initiation and growth during low (LCF) and high cycle fatigue (HCF) in AL 2003 (UNS S32003). Electron Backscattered Diffraction (EBSD) analysis of plastically active grains allows to determinate the slip systems and their associated Schmid factor (SF). Additionally, the dislocation structure developed during cycling is observed by transmission electron microscopy (TEM). Whereas in HCF cracks nucleate at grains boundaries, during LCF cracks nucleate along intrusion/extrusions in ferritic grains and as they reach austenitic grains grow along active slip systems or by double slip system. Moreover, phase boundaries and grain boundaries act as effective barrier against crack propagation.     

Bruchzähigkeit und Ermüdungs-Rißwachstum von Gußeisen

Fracture Toughness and Fatigue Crack Growth of Cast Irons Fracture toughness, elastic moduli and fatigue crack growth rates in air and in vacuum were measured for 17 different cast irons. The graphite shape in the cast irons varied from flakes to nodules, the matrix varied from ferrite to pearlite to martensite. In the fatigue crack growth rate tests, using fracture mechanics methods, it was observed that the fatigue crack growth rate increases significantly as the cyclic stress intensity range approaches the critical value for stable crack growth. This phenomenon was used to determine the fracture toughness of the cast irons. Such toughness data agree well with literature data on the fracture toughness of cast irons. An extensive review of the effects of strength on the fracture toughness of commercial cast irons is presented. In cast irons with flake graphite, cyclic loading results in a reduced modulus of elasticity. This is attributed to the rupture of the graphite flakes under cyclic loading.     

蠕化率对蠕墨铸铁组织及热疲劳性能的影响

采用自约束热疲劳试验机,对不同蠕化率下的蠕墨铸铁进行热疲劳性能试验并观察其组织变化。结果表明,试样的抗热疲劳性能随着蠕化率的升高呈现先上升后下降的趋势。当蠕化率为70%~80%时,蠕墨铸铁的热疲劳性能最好。蠕虫状石墨占基体比重有一个最佳值,蠕化率过低时,由于球状石墨数量较多分布较密集,导致热疲劳性能较差;蠕化率过高时,由于蠕虫状石墨过于粗大使裂纹扩展速度加快,导致热疲劳性能较差。在裂纹扩展后期,主裂纹变粗大导致其向前扩展所需驱动力不足以及主裂纹上形成分叉裂纹及二次裂纹,进而导致裂纹扩展呈现先快后慢、阶段性扩展的特点。     

Einfluß der Wärmebehandlung auf die Schwingfestigkeitseigenschaften der Legierung AlMgSi 0,7

Influence of Heat Treatment on the Fatigue Behaviour of 6005A Aluminium Alloy The influence of industrial heat treatment on the fatigue behaviour of 6005A Aluminium alloy has been investigated. By variation of the cooling rate from solution temperature and holding time at room temperature the size of precipitates improving strength and the width of precipitation free zones at grain boundaries may be altered independently from each other. Increasing the size of precipitates and the width of the precipitation free zones will decrease the tensile properties. In the high cycle fatigue region minor fatigue properties result from a significant broadening of the precipitation free zones, which enhance deformation and crack initiation at the grain boundaries. Coarsening the precipitates has no influence on fatigue behaviour, before crack initiation has taken place, but reduces fatigue crack propagation rate and by this improves the total lifetime.     

Investigation on the Static Fatigue Mechanism and Effect of Specimen Thickness on the Static Fatigue Lifetime in WC–Co Cemented Carbides

The static fatigue mechanism and effect of specimen thickness on static fatigue lifetime for four WC–Co cemented carbides were studied with different binder contents and carbide grain sizes. Static fatigue tests under three-point bend loading were conducted on different sized specimens. The fracture surfaces of rupture specimens were examined by scanning electron microscopy to investigate the static fatigue micromechanisms. Experimental results show that microcracks nucleate from defects or inhomogeneities and the connection of microcracks produces a main crack. The main crack propagates rapidly, resulting in the fracture of specimens. The extension of static fatigue lifetime with the increase of specimen thickness is due to the decrease of plastic zone size near the crack tip and relevant energy change during the crack growth. The effect of specimen thickness on static fatigue lifetime is much greater for cemented carbides with larger WC grain size or higher cobalt content, which is attributed to operative toughening mechanisms.