Microstructure and mechanical properties of friction stir welded 7136–T76 aluminium alloy

Abstract

The microstructure of the weld was examined by light and electron microscopy (scanning and transmission). The various regions, i.e. thermomechanically affected zone, heat affected zone and unaffected base material, were studied in detail to better understand the microstructural evolution during friction stir welding and its impact on basic mechanical properties. The change in morphology of the strengthening phases reflected the relative temperature profile and the amount of deformation across the welded joint during the stir welding process. The centre of the weld was composed of fine grains and coarse particles identified mainly as MgZn₂. In the thermomechanically and heat affected zones, the grain size was not uniform, and the strengthening phases filled the grain interiors, while grain boundaries were surrounded by precipitation free zones. The size of the strengthening phase decreased towards the base material. The hardness profile of the friction stir weld displayed the lowest hardness on the retreating side. Tensile properties of the weld itself were superior to those for material containing weld.     

Effect of welding parameters on mechanical and microstructural properties of dissimilar AA6082–AA2024 joints produced by friction stir welding

The effect of processing parameters on the mechanical and microstructural properties of dissimilar AA6082–AA2024 joints produced by friction stir welding was analysed in this study. Different samples were produced by varying the advancing speeds of the tool as 80 and 115 mm/min and by varying the alloy positioned on the advancing side of the tool. In all the experiments the rotating speed is fixed at 1600 RPM. All the welds were produced perpendicularly to the rolling direction for both the alloys. Microhardness (HV) and tensile tests performed at room temperature were used to evaluate the mechanical properties of the joints. The mechanical tests were performed on the joints previously subjected to annealing at 250 °C for 1 h. For the fatigue tests, a resonant electromechanical testing machine was employed under constant loading control up to 250 Hz sine wave loading. The fatigue tests were conducted in the axial total stress–amplitude control mode, with R = σ_min/σ_max = 0.1. In order to analyse the microstructural evolution of the material, the welds’ cross-sections were observed optically and SEM observations were made of the fracture surfaces.     

The microstructure and mechanical properties of friction stir welded Al–Zn–Mg alloy in as welded and heat treated conditions

High strength aluminium alloys generally present low weldability because of the poor solidification microstructure, porosity in the fusion zone and loss in mechanical properties when welded by fusion welding processes which otherwise can be welded successfully by comparatively newly developed process called friction stir welding (FSW). This paper presents the effect of post weld heat treatment (T₆) on the microstructure and mechanical properties of friction stir welded 7039 aluminium alloy. It was observed that the thermo-mechanically affected zone (TMAZ) showed coarser grains than that of nugget zone but lower than that of heat affected zone (HAZ). The decrease in yield strength of welds is more serious than decrease in ultimate tensile strength. As welded joint has highest joint efficiency (92.1%). Post weld heat treatment lowers yield strength, ultimate tensile strength but improves percentage elongation.     

Effects of friction stir welding on microstructure and mechanical properties of extruded secondary aluminum 6061 alloy

Experiments were carried out to determine the effects of friction stir welding on microstructure and properties of recycled Aluminum 6061 alloy, whose alloy content varied from that of primary alloy. The alloy was processed at tool speed and feed ranges of 530 rev/min–1320 rev/min and 40 mm/min–100 mm/min respectively. Microstructure examination; tensile test and Vickers microhardness evaluation were carried out. Microstructure of the alloy was in four zones including: base metal, heat affected zone, thermo-mechanically affected zone and stirred zone. Average grain size of unprocessed material was 93 μm. Processing the alloy at 530 rev/min and 100 mm/min resulted in grains of average size 93 μm, 183 μm and 7 μm; in base metal, heat affected zone and stirred zone respectively. Tensile failure occurred in heat affected zone; that was exposed to high heat. The alloy hardness decreased to a minimum in heat affected zone, followed by a brief rise in thermo-mechanically affected zone, to another maximum in stirred zone. Processed zone hardness was inversely proportional to tool speed and directly proportional to feed rate. Increase in the speed and decrease in feed, increased heat which deteriorated the properties.     

Microstructural characteristics and mechanical properties of friction stir welded joints of Ti–6Al–4V titanium alloy

The α + β titanium alloy, Ti–6Al–4V, was friction stir welded at a constant tool rotation speed of 400 rpm. Defect-free welds were successfully obtained with welding speeds ranging from 25 to 100 mm/min. The base material was mill annealed with an initial microstructure composed of elongated primary α and transformed β. A bimodal microstructure was developed in the stir zone during friction stir welding, while microstructure in the heat affected zone was almost not changed compared with that in the base material. An increase in welding speed increased the size of primary α in the stir zone. The weld exhibited lower hardness than the base material and the lowest hardness was found in the stir zone. Results of transverse tensile test indicated that all the joints had lower strength and elongation than the base material, and all the joints were fractured in the stir zone.     

Microstructural characterization and mechanical properties of high power ultrasonic spot welded aluminum alloy AA6111–TiAl6V4 dissimilar joints

Aluminum alloy AA6111 and TiAl6V4 dissimilar alloys were successfully welded by high power ultrasonic spot welding. No visible intermetallic reaction layer was detected in as-welded AA6111/TiAl6V4 welds, even when transmission electron microscopy was used. The effects of welding time and natural aging on peak load and fracture energy were investigated. The peak load and fracture energy of welds increased with an increase in welding time and then reached a plateau. The lap shear strength (peak load) can reach the same level as that of similar Al–Al joints. After natural aging, the fracture mode of welds transferred from ductile fracture of the softened aluminum to interfacial failure due to the strength recovery of AA6111.     

Evaluating the microstructure and mechanical properties of friction stir processed Al–Si alloy

In this study, mechanical behaviour and microstructural evolution in friction stir processing (FSP) of casting hypereutectic A390 aluminium alloy have been investigated. The mechanical behaviour of FSP samples was investigated by measuring the strain rate sensitivity using shear punch testing. The room-temperature shear punch tests were conducted at shear strain rates in the range of 10^?4–10^?1?s^?1. The results indicate that the strain rate sensitivity index increases from about 0.015 to 0.120 for as-cast A390 after third FSP pass and then experiences a further growth in FSP passes. The increase in the grain size and CuAl₂ intermetallic particle size result in a reduction in strain sensitivity index as well as shear strength after third FSP pass.     

Microstructural characteristics and mechanical properties of non-combustive Mg–9Al–Zn–Ca magnesium alloy friction stir welded joints

Non-combustive Mg–9Al–Zn–Ca magnesium alloy was friction stir welded with rotation speeds ranging from 500 to 1250 rpm at a constant welding speed of 200 mm/min. Defect-free joints were successfully produced at rotation speeds of 750 and 1000 rpm. The as-received hot extruded material consisted of equiaxed α-Mg grains with β-Mg₁₇Al₁₂ and Al₂Ca compounds distributed along the grain boundaries. Friction stir welding produced much refined α-Mg grains accompanied by the dissolution of the eutectic β-Mg₁₇Al₁₂ phase, while Al₂Ca phase was dispersed homogeneously into the Mg matrix. An increase in rotation speed increased the α-Mg grain size but not significantly, while microstructure in the heat affected zone was almost not changed compared with the base material. The hardness tests showed uniform distributed and slightly increased harness in the stir zone. Results of transverse tensile tests indicated that the defect-free joints fractured at the base material, while longitudinal tensile tests showed that the strength of the defect-free welds was improved due to microstructural refinement and uniform distribution of intermetallic compounds.     

Microstructural and mechanical properties of friction stir welded Cu–30Zn brass alloy at various feed speeds: Influence of stir bands

In this study, the effect of various feed speeds on microstructure and mechanical properties of friction stir welded Cu–30Zn brass alloy is investigated. Rotation speed was fixed at 950 rpm and feed speed varied in the range of 190–375 mm/min. Examination of the microstructure showed very fine grains with some deformed grains in the stirred zone and some coarser grains in the thermo-mechanically affected zone and base metal. A unique deformation pattern, namely “stir band” in the stirred zone region was identified and its density increased by increase in feed speed. Results showed that the grain size profile was independent of feed speed and the hardness values decreased by increase in feed speed. Increase in feed speed led to a slight improvement of yield strength and ultimate tensile strength, associated to continuous spring-like morphology of stir bands acting as a strengthening structure. However, ductility reduces considerably from 57 to 27%. Moreover, it is observed that during tensile test, fracture cracks originate exactly adjacent to the stir bands.     

Microstructure and interface characterization of dissimilar friction stir welded lap joints between Ti–6Al–4V and AISI 304

The feasibility of dissimilar friction stir welding (FSW) in overlap configuration between Ti–6Al–4V alloy (Ti64) and AISI 304 austenitic stainless steels (304SS) was investigated. Sound joints were achieved when placing titanium as the upper workpiece. Joints were successfully produced by employing a welding speed of 1 mm/s and rotational speeds of 300 and 500 rpm. A lamellar microstructure was formed in the stir zone of Ti64, where grain size was found to increase with increasing rotational speed, and austenitic equiaxed grains were obtained near the interface of 304SS coupon. Energy dispersive X-ray spectroscopy (SEM-EDS) of the interface revealed a thin intermixed region and suggested intermetallic compound formation. Microhardness data in the titanium weld zone for both rotational speeds exhibited slightly lower values than the base material, with the lowest values in the heat affected zone, whereas the microhardness values in the stainless steel side around the weld center were found to be higher than those obtained for the base material.     

Microstructural evolution and mechanical properties of dissimilar Al–Cu joints produced by friction stir welding

5A02 aluminum alloy and pure copper were joined by friction stir welding (FSW). A defect-free joint was obtained when one of process parameters, i.e. the traverse speed was lowered from 40 mm/min to 20 mm/min. A good mixing of Al and Cu was observed in the weld nugget zone (WNZ). A large amount of fine Cu particles were dispersed in the upper part of the WNZ producing a composite-like structure. In the lower part, nano-scaled intercalations were observed and identified by transmission electron microscopy (TEM). These layered structures were subsequently confirmed as Al₄Cu₉ (γ), Al₂Cu₃ (ε), Al₂Cu (θ), respectively. Formation of these microstructures caused an inhomogeneous hardness profile. Particularly, a distinct rise in hardness was noticed at the Al/Cu interface. Excellent metallurgical bonding between Al and Cu gave rise to good behaviors in the tensile and bending strength.     

Effect of welding parameters on microstructure and mechanical properties of friction stir welded joints of a super high strength Al–Zn–Mg–Cu aluminum alloy

Samples made of a super high strength aluminum alloy with high Zn content were friction stir welded with rotation rates of 350–950 rpm and welding speeds of 50–150 mm/min. The effect of welding parameters on the microstructure and mechanical properties was investigated. It was observed that the grain size of the nugget zones decreased with the increasing welding speed or the decreasing tool rotation rate. Most of the strengthening precipitates in the nugget zone were dissolved back and the intragranular and grain boundary precipitates in the heat affected zone coarsened significantly. The greatest ultimate tensile strength of 484 MPa and largest elongation of 9.4 were obtained at 350 rpm−100 mm/min and 350 rpm−50 mm/min, respectively. The ultimate tensile strength and elongation deteriorated drastically when rotation rate increased from 350 to 950 rpm at a constant welding speed of 100 mm/min.     

Thermo-mechanical and microstructural issues in dissimilar friction stir welding of AA5086–AA6061

In this research, thermo-mechanical behavior and microstructural events in dissimilar friction stir welding of AA6061-T6 and AA5086-O have been evaluated. The thermo-mechanical responses of materials during the process have been predicted employing a three-dimensional model together with a finite element software, ABAQUS. Then, mechanical properties and microstructures of the weld zone were studied with the aid of experimental observations and model predictions. It is found that the mixing of material in the weld nugget is performed more efficiently when AA5086 is in the advancing side and also the temperature field is distributed asymmetrically resulting in larger thermally affected region in the AA6061 side. Besides, the microstructural studies shows that the microstructures of stirred zone consist of fine equiaxed grains where finer grains are produced in AA6061 side compared to AA5086 side.     

Fatigue behavior of friction stir welded Al–Mg–Sc alloy

The effect of Friction Stir Welding on the fatigue behavior of Al–Mg–Sc alloy has been studied. To reveal the influence of the welding parameters, different travel speeds of the welding tool have been used to provide weld seams with varying microstructural features. Crack initiation as well as crack propagation behavior under fatigue loading has been investigated with respect to the local microstructure at the crack initiation sites and along the crack path. Fatigue cracks were mostly initiated around the stir zone and the adjacent thermo-mechanical affected zone independent from hardness distributions in the weld seams. In some specimens, defect-like feature was observed at the crack origins, which shortened the fatigue lives. It has been found that while the effect of the tool travel speed on the fatigue lifetime seems to be little, the varying and complex local microstructure in the weld seam basically affects both the crack initiation sites and the crack propagation paths.     

Tensile properties of friction stir welded and friction stir welded-superplastically formed Ti–6Al–4V butt joints

A University and Industry collaborative research project was undertaken to evaluate the performance of as friction stir welded (FSW) and friction stir welded-superplastically formed Ti–6Al–4V alloy sheets. The purpose of this particular effort was to evaluate the tensile properties of friction stir welded and superplastically formed friction stir welded Ti–6Al–4V. Welds were produced out of both standard grain and fine grained titanium and tested in the as welded, stress relieved (SR) and superplastically formed (SPF) conditions. The preliminary results of the FSW and post FSW–SPF joint were found to be close to that of as received titanium with respect to strength, but elongations were decreased.     

Microstructure and mechanical properties of friction stir welded 18Cr–2Mo ferritic stainless steel thick plate

In this study, microstructure and mechanical properties of a friction stir welded 18Cr–2Mo ferritic stainless steel thick plate were investigated. The 5.4 mm thick plates with excellent properties were welded at a constant rotational speed and a changeable welding speed using a composite tool featuring a chosen volume fraction of cubic boron nitride (cBN) in a W–Re matrix. The high-quality welds were successfully produced with optimised welding parameters, and studied by means of optical microscopy (OM), scanning electron microscopy (SEM), electron back-scattered diffraction (EBSD) and standard hardness and impact toughness testing. The results show that microstructure and mechanical properties of the joints are affected greatly, which is mainly related to the remarkably fine-grained microstructure of equiaxed ferrite that is observed in the friction stir welded joint. Meanwhile, the ratios of low-angle grain boundary in the stir zone regions significantly increase, and the texture turns strong. Compared with the base material, mechanical properties of the joint are maintained in a comparatively high level.     

Effect of rotation speed on microstructure and mechanical properties of Ti–6Al–4V friction stir welded joints

The effect of tool rotation speed on microstructure and mechanical properties of friction stir welded joints was investigated for Ti–6Al–4V titanium alloy. Joints were produced by employing rotation speeds ranging from 400 to 600 rpm at a constant welding speed of 75 mm/min. It was found that rotation speed had a significant impact on microstructure and mechanical properties of the joints. A bimodal microstructure or a full lamellar microstructure could be developed in the weld zone depending on the rotation speeds used, while the microstructure in the heat affected zone was almost not influenced by rotation speed. The hardness in the weld zone was lower than that in the base material, and decreased with increasing rotation speed. Results of transverse tensile test indicated that all the joints exhibited lower tensile strength than the base material and the tensile strength of the joints decreased with increasing rotation speed.     

Microstructural evolution and mechanical properties of friction stir welded joint of Fe–Cr–Mn–Mo–N austenite stainless steel

2 mm thick Fe–18.4Cr–15.8Mn–2.1Mo–0.66N high nitrogen austenite stainless steel plate was successfully joined by friction stir welding (FSW) at 800 rpm and 100 mm/min. FSW did not result in the loss of nitrogen in the nugget zone. The arc-shaped band structure, consisting of a small amount of discontinuous ferrite aligning in the bands and fine austenite grains, was a prominent microstructure feature in the nugget zone. The discontinuous ferrite resulted from newly formed ferrite during welding and the remained ferrite, whereas the fine austenite grains were formed due to dynamic recrystallization of the initial austenite during FSW. The fine dynamically recrystallized grains in the nugget zone significantly increased the hardness compared to that of the base material. The strength of the joint was similar to that of the base material, with the joint failing in the base material zone.     

Effects of Al-Ni powder addition on dissimilar friction stir welding between AA7075-T6 and 304 L

Friction stir welding between AA7075-T6 aluminum alloy and 304 L stainless steel sheet metal was performed with the addition of Al−Ni powder between the joining interfaces to increase the joining performance. The welding tool was rotated at 200 min⁻¹ to 800 min⁻¹ with the constant traverse speed of 25 mm/min. The resulting joint interfaces were analyzed using a field emission-scanning electron microscope and energy-dispersive x-ray spectroscopy analysis. The tensile strength was greater for the Al−Ni powder added specimens at the lower tool rotational speeds. The tensile strength of 360 MPa was obtained for the ‘with-powder’ specimen as compared to 220 MPa for the ‘without-powder’ specimen at the 200 min⁻¹ tool speed. Electron microscope images of the stir zone showed a significant mixing of the Al−Ni powder with the base materials, increased contact at the interface, which resulted in increased joining strength at the lower tool rotational speeds. However, based on the images, intermetallic compound that may contribute to the joining strength in the vicinity of the interfacial region was not detected.