Comparison of the crushing performance of hollow and foam-filled small-scale composite tubes with different geometrical shapes for use in sacrificial cladding structures

This paper presents the quasi-static crushing performance of nine different geometrical shapes of small-scale glass/polyester composite tubes filled with polyurethane closed-cell foam for use in sacrificial cladding structures. The effect of polyurethane foam on the crushing characteristics and the corresponding energy absorption is addressed for each geometrical shape of the composite tube. Composite tubes with two different thicknesses (1 mm and 2 mm) have been considered to study the influence of polyurethane foam on the crushing performance. From the present study, it was found that the presence of polyurethane foam inside the composite tubes suppressed the circumferential delamination process and fibre fracturing; consequently, it reduced the specific energy absorption of composite tubes. Furthermore, the polyurethane foam attributed to a higher peak crush load for each composite tube. However, the presence of polyurethane foam inside the composite tubes significantly increased the stability of the crushing phenomena especially for the square and hexagonal cross-sectional composite tubes with 1 mm wall thickness. The results from this study are compared with our previous results for composite tubes without polyurethane foam [1].     

Progressive crushing of stitched glass/polyester composite cylindrical shells

This paper examines the effect of mode I interlaminar fracture toughness (G_Ic) on the specific energy absorption of stitched glass/polyester composite cylindrical shells under axial compression. The laminated composite cylindrical shells used as energy absorbers, absorb large amount of impact energy during collision. Since mode I delamination in the thin wall of axially collapsed shell is one of the major energy absorbing modes, contribution of G_Ic to specific energy absorption (SEA) of tubes is significant during collision. The G_Ic values are determined through double cantilever beam (DCB) test with stitched and unstitched planar specimens. The four and six-layered cylindrical tubes of D/t ratios 29.27 and 20, respectively, with G_Ic values ranging from 1.68 to 8.09 kJ/m² are prepared by stitching and are subjected to quasi-static axial compression. Increasing G_Ic up to certain value leads to controlled progressive crushing, which is a good energy absorbing mechanism, beyond which failure is uncontrolled. Cylindrical tubes having G_Ic up to 6.34 kJ/m² leads to 40% increase in SEA for four-layered tubes and 6.6% for six-layered tubes comparing with the corresponding unstitched tubes. When the tubes have G_Ic of 8.09 kJ/m², four-layered tubes undergo unstable failure, but six-layered tubes undergo stable progressive crushing with 22% increase in SEA. Transition from stable to unstable failure depends upon the thickness of tubes. An analytical model is developed based on energy approach to predetermine the steady state mean crush load of cylindrical composite shells under axial compression. The model results are validated by experimental results, and show good agreement.     

Axial crushing of thin-walled high-strength steel sections

Quasi-static and dynamic axial crushing tests were performed on thin-walled square tubes and spot-welded top-hat sections made of high-strength steel grade DP800. The dynamic tests were conducted at velocities up to 15 m/s with an impacting mass of 600 kg in order to assess the crush behaviour, the deformation force and the energy absorption. Typical collapse modes developed in the sections and the associated energy absorbing characteristics were examined and compared with previous studies on high-strength steel. A significant difference was observed between the quasi-static and the dynamic crushing tests in terms of the deformation force and impact energy absorption. As this difference is attributed to strain-rate and inertia effects, material tensile tests at elevated strain rates have been carried out. A comparison is made with analytical methods and the response was under-predicted. In addition, numerical simulations of the axial crushing of the thin-walled sections were performed and comparisons with the experimental results were satisfactory. The validated numerical model was used to study the energy absorption capacity of thin-walled sections with variations in the yield strength, sheet thickness, flange width and spot-weld spacing. Structural effectiveness differences have been captured through simulations between spot-welded top-hat sections made of mild steel and high-strength steel.     

Structural evolution of Aun (n = 29–35) clusters: A transition from hollow cage to amorphous packing

The structural evolution and competition between the hollow cage, amorphous, fcc-like and tubular structures for medium-sized Au_n (n = 29–35) clusters were investigated using density functional theory combined with empirical genetic algorithm search. Au_n (n = 29–32) clusters prefer the hollow cage structures. Amorphous core–shell configurations prevail over other kinds of structural motifs for Au_n (n = 33–35). A transition from hollow cage to amorphous packing occurs at n = 33. The size-dependent HOMO–LUMO gap, vertical ionization potential and electron density of states were discussed to illustrate the relationship between the electronic properties and the geometry structures.     

Preparation and microwave absorption of porous hollow ZnO by CO2 soft-template

The porous hollow ZnO samples were prepared by calcination of ZnCO₃ precursor at 450 °C. The structural properties were investigated using X-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDS), thermogravimetric analysis and differential thermal analysis (TG-DTA). A possible mechanism for the formation of porous hollow microstructure was proposed. The microwave absorption properties of the porous hollow structural ZnO have been investigated. The reflection loss (RL) of the ZnO was calculated based on the relative complex permeability and permittivity. A minimum reflection loss of the wax-composite with 25 wt% porous hollow ZnO is −36.3 dB at 12.8 GHz with a thickness of 4.0 mm. The results indicate that porous hollow structural ZnO can be used as a desirable material for the microwave absorption.     

Toughening of denture base resin with short deformable fibers

Fracture resistance of polymer reinforced with short fibers consists of a sum of contributions from matrix and fiber fracture, fiber debonding and pull-out. The existing models for predicting dependence of fracture toughness on structural variables were derived for the commercially important fiber volume fractions, i.e., for v_f ? 0.1. In this contribution, modification of the existing model for the dependence of the critical strain energy release rate, G_IC, on the fiber type, length and aspect ratio, interfacial adhesion and volume fraction has been attempted to allow predictions at low v_f < 0.10. The predictions based on the modified model were compared with experimental data on fracture toughness of lightly x-linked PMMA used to manufacture base of removable dentures toughened with short randomly oriented deformable fibers. The composite toughness was measured under impact loading to simulate typical mode of fracture of removable dentures. The G_IC for composites containing short Kevlar 29, S2-glass and poly(vinyl alcohol) (PVOH) fibers were obtained using instrumented Charpy impact tests at room temperature and impact speed of 1.0 m/s. Theoretical prediction based on the proposed model and experimental results agreed reasonably well.     

Static and high-rate loading of single and multi-bolt carbon–epoxy aircraft fuselage joints

Single-lap shear behaviour of carbon–epoxy composite bolted aircraft fuselage joints at quasi-static and dynamic (5 m/s and 10 m/s) loading speeds is studied experimentally. Single and multi-bolt joints with countersunk fasteners were tested. The initial joint failure mode was bearing, while final failure was either due to fastener pull-through or fastener fracture at a thread. Much less hole bearing damage, and hence energy absorption, occurred when the fastener(s) fractured at a thread, which occurred most frequently in thick joints and in quasi-static tests. Fastener failure thus requires special consideration in designing crashworthy fastened composite structures; if it can be delayed, energy absorption is greater. A correlation between energy absorption in multi-bolt and single-bolt joint tests indicates potential to downsize future test programmes. Tapering a thin fuselage panel layup to a thicker layup at the countersunk hole proved highly effective in achieving satisfactory joint strength and energy absorption.     

An experimental study of square tube crushing under impact loading using a modified large scale SHPB

This paper presents an experimental study on square tubes made from a rate insensitive material under static and impact loading. Rate insensitivity of the base material (Cu–Zn alloy) is confirmed by static and dynamic tests on small samples cut from the tubes. A direct impact large scale Hopkinson bar (80 mm diameter, 10 m length) system is used to perform tube crushing tests. A two-point measurement method is applied to extend measuring duration of the pressure bar, which is usually limited by its length. The proposed method permits to monitor the whole tube crushing process.Static and impact tests (7–15 m/s) on these square tubes reveal that there is a significant increase under impact loading of both initial and successive peak loads with respect to quasi-static loading. Such a study is useful for the understanding of strength enhancement under impact loading observed for cellular materials such as honeycombs.     

Quasi-static uni-axial compression behaviour of hollow glass microspheres/epoxy based syntactic foams

Hollow glass microspheres/epoxy foams of different densities were prepared by stir casting process in order to investigate their mechanical properties. The effect of hollow spheres content and wall thickness of the microspheres on the mechanical response of these foams is studied extensively through a series of quasi-static uni-axial compression tests performed at a constant strain rate of 0.001 s^?1. It is found that strength of these foams decreases linearly from 105 MPa (for the pure resin) to 25 MPa (for foam reinforced with 60 vol.% hollow microspheres) with increase in hollow spheres content. However, foams prepared using hollow spheres with a higher density possess higher strength than those prepared with a lower one. The energy absorption capacity increases till a critical volume fraction (40 vol.% of the hollow microspheres content) and then decreases. Failure and fracture of these materials occur through shear yielding of the matrix followed by axial splitting beyond a critical volume fraction.     

Characteristics of aluminum/CFRP short square hollow section beam under transverse quasi-static loading

Energy absorption capability and bending collapse behavior of an aluminum (Al)/carbon fiber reinforced plastic (CFRP) short square hollow section (SHS) beam were investigated under transverse quasi-static loading. The Al SHS beam was reinforced by CFRP, and the specimen was co-cured via an autoclave curing process. Three-point bending test was performed with five different lay-up sequences and three different laminate thicknesses. Stable bending collapse accompanying plastic hinge was observed in all specimens. Individual bending collapse behaviors were different depending on the lay-up sequences. The specific energy absorbed (SEA) was improved by up to 29.6% in the Al/CFRP SHS beam specimen with a [0/+45°/90°/−45°]_n lay-up sequence and laminate thickness of 1.168 mm (thickness ratio of Al: CFRP = 1: 0.87, 8 plies of prepreg) compared to the Al SHS beam. The SEA was not related with damage area of the Al/CFRP SHS beam. Finite element analysis and theoretical analysis based on Kecman’s model were performed to investigate the effect of reinforcement by CFRP on the Al SHS beam.     

Reprint of “Multiaxial fatigue property of Ti–6Al–4V using hollow cylinder specimen under push-pull and cyclic inner pressure loading”

This paper studies a multiaxial fatigue crack mode and a fatigue life of Ti–6Al–4V. Load controlled fatigue tests at room temperature were carried out using a hollow cylinder specimen under multiaxial loading with principal stress ratio λ equal to 0, 0.4, 0.5 and 1.0 and loading ratio R kept constant and equal to 0. λ is defined as λ = σ₂/σ₁, where σ₁ and σ₂ are maximum and intermediate/minimum principal stresses, respectively. Here, the test at λ = 0 is a uniaxial loading test and that at λ = 1.0 an equi-biaxial loading test. A testing machine employed was a newly developed multiaxial fatigue testing machine which can apply push-pull and reversed torsion loading with inner pressure into the hollow cylinder specimen. Based on the obtained results in this study, multiaxial fatigue properties are examined, where the fatigue life evaluation and the crack mode are discussed. The fatigue life is reduced with an increase of λ, due to cyclic ratcheting and crack mode in multiaxial loading. The crack mode is also affected by the surface condition resulting from cut-machining.     

Multiaxial fatigue property of Ti–6Al–4V using hollow cylinder specimen under push-pull and cyclic inner pressure loading

This paper studies a multiaxial fatigue crack mode and a fatigue life of Ti–6Al–4V. Load controlled fatigue tests at room temperature were carried out using a hollow cylinder specimen under multiaxial loading with principal stress ratio λ equal to 0, 0.4, 0.5 and 1.0 and loading ratio R kept constant and equal to 0. λ is defined as λ = σ₂/σ₁, where σ₁ and σ₂ are maximum and intermediate/minimum principal stresses, respectively. Here, the test at λ = 0 is a uniaxial loading test and that at λ = 1.0 an equi-biaxial loading test. A testing machine employed was a newly developed multiaxial fatigue testing machine which can apply push-pull and reversed torsion loading with inner pressure into the hollow cylinder specimen. Based on the obtained results in this study, multiaxial fatigue properties are examined, where the fatigue life evaluation and the crack mode are discussed. The fatigue life is reduced with an increase of λ, due to cyclic ratcheting and crack mode in multiaxial loading. The crack mode is also affected by the surface condition resulting from cut-machining.     

Influence of magnesium on hydrogenated ScAl1−xMgx alloys: A theoretical study

Ab initio total energy calculations, based on the projector augmented wave method and the exact muffin-tin orbitals method in combination with the coherent-potential approximation, are used to examine the effect of magnesium on hydrogen absorption/desorption temperature and phase stability of hydrogenated ScAl_1?xMg_x (0 ? x ? 0.3) alloys. According to the experiments, ScAl_1?xMg_x adopts the CsCl structure, and upon hydrogen absorption it decomposes into ScH₂ with CaF₂ structure and Al–Mg with face centered cubic structure. Here we demonstrate that the stability field of the hydrogenated alloys depends sensitively on Mg content and on the microstructure of the decomposed system. For a given microstructure, the critical temperature for hydrogen absorption/desorption increases with Mg concentration.     

Dynamic behavior of selected ceramic powders

An experimental setup has been developed on the continuous recording of the stress profiles in ceramic powders subject to shock loading with manganin gauges. A series of plate impact experiments on highly porous ceramic powders such as Al₂O₃, SiC and B₄C were conducted at the laboratory's single stage powder gun facility. The relationship between shock wave velocity and particle velocity was measured to obtain the Hugoniot data. Plate impact onto powder sample experiments were conducted at loading stresses ranging from 1.6 to 4.2 GPa. The experimental results show that the shock wave speeds in various ceramic powders vary between 1 and 2 km/s. Linear Hugoniot relations between shock velocity (D) and particle velocity (u) are observed. The loading stress–specific volume form of Hugoniot relations (P–V) was constructed using the data from quasistatic compression test results, Hopkinson bar dynamic compression test results and powder gun plate impact experiment results. The P–V diagram shows that the crush strength of ceramic powders is comparable to the loading stress level. The B₄C and SiC powders with bigger particle size more easily reach the solid state Hugoniot than the powders with smaller particle size at the same loading condition. In the case of Al₂O₃, the material shows less sensitivity to particle size difference at the same level of loading rate as compared to B₄C and SiC.     

Laser shock peening effect on the dislocation transitions and grain refinement of Al–Mg–Si alloy

This paper systematically investigates the effect of laser shock peening without coating parameters on the microstructural evolution, and dislocation configurations induced by ultra-high plastic strains and strain rates. Based on an analysis of optical microscopy, polarized light microscopy, transmission electron microscopy observations and residual stress analysis, the significant influence of laser shock peening parameters due to the effect of plasma generation and shock wave propagation has been confirmed. Although the optical microscopy results revealed no significant microstructural changes after laser shock peening, i.e. no heat effect zone and differences in the distribution of second-phase particles, expressive influence of laser treatment parameters on the laser shock induced craters was confirmed. Moreover, polarized light microscopy results have confirmed the existence of well-defined longish grains up to 455 μm in length in the centre of the plate due to the rolling effect, and randomly oriented smaller grains (20 μm × 50 μm) in the surface due to the static recrystallization effect. Laser shock peening is reflected in an exceptional increase in dislocation density with various configurations, i.e. dislocation lines, dislocation cells, dislocation tangles, and the formation of dense dislocation walls. More importantly, the microstructure is considerably refined due to the effect of strain deformations induced by laser shock peening process. The results have confirmed that dense dislocation structures during ultra-high plastic deformation with the addition of shear bands producing ultra-fine (60–200 nm) and nano-grains (20–50 nm). Furthermore, dislocation density was increased by a factor of 2.5 compared to the untreated material (29 × 10¹³ m^− 2 vs. 12 × 10¹³ m^− 2).     

Strong yellow emission of ZnO hollow nanospheres fabricated using polystyrene spheres as templates

ZnO hollow nanospheres were fabricated using polystyrene (PS) microspheres as templates were demonstrated in this paper. The structures and morphologies of obtained products were characterized by XRD, FESEM and TEM. The results revealed that ZnO hollow nanospheres possess a hexagonal wurtzite structure with a diameter around 450–500 nm. Ultraviolet–visible (UV–vis) analysis showed that ZnO hollow nanospheres had high absorption in the ultraviolet region and low absorption in the visible region. Room temperature photoluminescence (PL) spectrum showed a weak UV emission at 380 nm and a strong and broad yellow emission centered at 550 nm. The formation mechanism of hollow structure was also investigated.     

Experimental study on the dynamic compressive mechanical properties of concrete at elevated temperature

Strain rate effect and temperature effect are two important factors affecting the mechanical behavior of concrete. Each of them has been studied for several years. However, the two factors usually work together in the engineering practice. It is necessary to understand the mechanical responses of concrete under high strain rate and elevated temperature. A self-designed high temperature SHPB apparatus was used to study the dynamic compressive mechanical properties of concrete at elevated temperature. The results show that the dynamic compressive strength and specific energy absorption of concrete increase with strain rate at all temperatures. The elastic modulus decreases obviously with strain rate at room temperature and stabilizes at a level with slightly decrease at elevated temperature. The dynamic compressive strength of concrete at 400 °C increases by nearly 14% compared to the room temperature. However, it decreases at 200 °C, 600 °C and 800 °C with the decrease ratio of 20%, 16% and 48%, respectively. The dynamic elastic modulus decreases largely subjected to elevated temperature. The specific energy absorption at 200 °C, 400 °C and 600 °C is higher than room temperature and decreases to be lower than room temperature at 800 °C. Formulas are established under the consideration of mutual effect of strain rate and temperature.     

Damping behavior and acoustic performance of polyurethane/lead zirconate titanate ceramic composites

0–3 Type PU-based lead zirconate titanate ceramic (PZT) composites are prepared by in situ polymerization method, this PU/PZT composite material has excellent sound absorption property at low frequencies because of damping property and piezoelectric property. The dispersion of PZT particles in PU matrix, dielectric loss tangent (tan δ), dynamic storage modulus (E′), dynamic loss modulus (E″), and the acoustic absorption coefficient (α) of PU/PZT composites are studied by scanning electron microscopy (SEM), dynamic mechanical analysis (DMA) and two-microphone impedance tube, respectively. The results indicate that the modified PZT particles dispersed well in PU matrix with the content of 30 wt%; the tan δ, E′ and E″ are 0.62, 3.75 GPa and 6.05 GPa, respectively, when the composite with 30 wt% of polarizing PZT; the acoustic absorption coefficient is found to increase with an increase of PZT content, and the average acoustic absorption coefficient is 0.32 at low frequencies from 125 to 500 Hz.     

Effect of strain rate on the dynamic compressive mechanical behaviors of rock material subjected to high temperatures

Strain rate is not only an important measure to characterize the deformation property, but also an important parameter to analyze the dynamic mechanical properties of rock materials. In this paper, by using the SHPB test system improved with high temperature device, the dynamic compressive tests of sandstone at seven temperatures in the range of room temperature to 1000 °C and five impact velocities in the range of 11.0–15.0 m/s were conducted. Investigations were carried out on the influences of strain rate on dynamic compressive mechanical behaviors of sandstone. The results of the study indicate that the enhancement effects of strain rates on dynamic compressive strength, peak strain, energy absorption ratio of sandstone under high temperatures still exist. However, the increase ratios of dynamic compressive strength, peak strain, and energy absorption ratio of rock under high temperature compared to room temperature have no obvious strain rate effects. The temperatures at which the strain rates affect dynamic compressive strength and peak strain most, are 800, and 1000 °C, respectively. The temperatures at which the strain rates affect dynamic compressive strength and peak strain weakest, are 1000 °C, and room temperature, respectively. At 200 and 800 °C, the strain rate effect on energy absorption ratio are most significant, while at 1000 °C, it is weakest. There are no obvious strain rate effects on elastic modulus and increase ratio of elastic modulus under high temperatures. According to test results, the relationship formula of strain rate with high temperature and impact load was derived by internalizing fitting parameters. Compared with the strain rate effect at room temperature condition, essential differences have occurred in the strain rate effect of rock material under the influence of high temperature.