Laser welding of Ti–6Al–4V to Nitinol

Formation of brittle intermetallic phases in addition to different thermal expansion coefficients associated with dissimilar welding leads to the formation of transverse cracks in weld metal and eventually restricts widespread applications of dissimilar joints. Therefore, joining technology should be expanded in field of dissimilar welding in order to solve its difficulties. In the present study, an experimental work with pulsed Nd:YAG laser was performed for dissimilar welding of Ti–6Al–4V and Nitinol. Autogenous welding of these two alloys resulted in joints with poor strength and ductility due to the formation of transverse cracks in the weld metal. Therefore, the chemical composition of the weld metal has to be modified in order to reduce the formation of brittle phases and eliminate subsequent cracking. In this work, this was done by insertion of a copper interlayer with a thickness of 75 μm between the base metals. The results indicated that insertion of copper interlayer has a great influence on the reduction of the amount of Ti₂Ni brittle intermetallic phase, elimination of transverse cracks through the weld metal and eventually improvement of mechanical properties of the joints. Insertion of copper interlayer was very useful since it altered the cracked autogenous joint to a joint which could withstand a tensile stress of 300 MPa.     

Austenitic and ferritic stainless steel dissimilar weld metal evaluation for the applications as-coating in the petroleum processing equipment

The current study presents some fundamental observations on the effects of the welding heat input in the chemical composition, microstructure, hardness and petroleum corrosion resistance of the fusion zone, formed by the AWS E309MoL austenitic stainless steel covered electrode and the AISI 410S ferritic stainless steel, being a dissimilar welding procedure. Such welding configurations are widely used as an overlay of equipment in the petroleum and gas industries. The welds were performed with the application of three different levels in heat inputs (6, 9 and 12 kJ/cm). Samples of the weld metals were conventionally prepared for the microstructural characterization by light microscopy and scanning electron microscopy. A corrosion test with samples immersed in heavy oil heated at 300 °C, was carried out for a period of 60 h. The corrosion rate was determined by the weight loss given after the aforesaid test. The fusion zone microstructure has a typical δ-ferrite acicular morphology, from which the level of δ-ferrite was duly altered with the increases of the welding heat input, due to the variations in the composition of the weld metal caused by dilution. It was also concluded that the chemical composition and the weld metal microstructure had a slight influence in the material’s corrosion rate. As a matter of fact, the corrosion rate of the weld metals evaluated herein, was considered satisfactory with few variations between the welding heat inputs duly applied.     

Optimization of deep penetration laser welding of thick stainless steel with a 10 kW fiber laser

Deep penetration laser welding of 12 mm thick stainless steel plates was conducted using a 10 kW high-power fiber laser. The effect of the processing parameters on the weld bead geometry was examined, and the microstructure and mechanical properties of the optimal joint were investigated. The results show that the focal position is a key parameter in high-power fiber laser welding of thick plates. There is a critical range of welding speed for achieving good full penetration joint. The type of top shielding gas influences the weld depth. The application of a bottom shielding gas improves the stability of the entire welding process and yields good weld appearances at both the top and bottom surfaces. The maximum tensile stress of the joint is 809 MPa. The joint fails at the base metal far from the weld seam with a typical cup–cone-shaped fracture surface. The excellent welding appearance and mechanical properties indicate that high-power fiber laser welding of a 304 stainless steel thick plate is feasible.     

Ultrasonic spot welding of Al/Mg/Al tri-layered clad sheets

Solid-state ultrasonic spot welding (USW) was used to join Al/Mg/Al tri-layered clad sheets, aiming at exploring weldability and identifying failure mode in relation to the welding energy. It was observed that the application of a low welding energy of 100 J was able to achieve the optimal welding condition during USW at a very short welding time of 0.1 s for the tri-layered clad sheets. The optimal lap shear failure load obtained was equivalent to that of the as-received Al/Mg/Al tri-layered clad sheets. With increasing welding energy, the lap shear failure load initially increased and then decreased after reaching a maximum value. At a welding energy of 25 J, failure occurred in the mode of interfacial failure along the center Al/Al weld interface due to insufficient bonding. At a welding energy of 50 J, 75 J and 100 J, failure was also characterized by the interfacial failure mode, but it occurred along the Al/Mg clad interface rather than the center Al/Al weld interface, suggesting stronger bonding of the Al/Al weld interface than that of the Al/Mg clad interface. The overall weld strength of the Al/Mg/Al tri-layered clad sheets was thus governed by the Al/Mg clad interface strength. At a welding energy of 125 J and 150 J, thinning of weld nugget and extensive deformation at the edge of welding tip caused failure at the edge of nugget region, leading to a lower lap shear failure load.     

Microstructure and mechanical properties of mild steel joints prepared by a flat friction stir spot welding technique

With the successful application of the flat spot friction stir welding technology to aluminum alloys, this technique was expanded to the spot lap welding of 1 mm thick mild steel in this study. It reveals that sound joints can be successfully obtained with smooth surfaces and without any internal welding defects. Two welding strategies based on the welding parameter can be used to obtain the welds that fracture through plug failure mode at high shear tensile strength. One way is to weld the sheet at low heat input in the first step and the second step is used to generate large stir zone and flatten the sample surface. However, the microstructure in the stir zone is not homogeneous and a coarse columnar grain structure forms at the bottom of the stir zone. Another way is to make the stir zone penetrate into the lower sheet during the first step and the second step is only aimed to flatten the sample surface. In this case, the total heat input can be reduced and the microstructure of the stir zone can be remarkably refined. The sound joints fractured along the circumstance of the stir zone and reached about 6600 N during the shear tensile tests.     

Microstructure and mechanical properties of dissimilar Al alloy/steel joints prepared by a flat spot friction stir welding technique

The 6061-T6 Al alloy and mild steel plate with a thickness of 1 mm were successfully welded by the flat spot friction stir welding technique, which contains two steps during the entire welding process. The rotating tools with different probe lengths of 1.0, 1.3 and 1.5 mm were used in the first step, during which a conventional spot FSW was conducted above a round dent previously made on the back plate. However, sound Al/Fe welds with similar microstructure and mechanical properties can still be obtained after the second step, during which a probe-less rotating tool was used to flatten the weld surface. The sound welds have smooth surface without keyholes and other internal welding defects. No intermetallic compound layer but some areas with amorphous atomic configuration was formed along the Al/Fe joint interface due to the lower heat input. The shear tensile failure load can reach a maximum value of 3607 N and fracture through plug mode. The probe length has little effect on the weld properties, which indicates that the tool life can be significantly extended by this new spot welding technique.     

Microstructural development of diffusion-brazed austenitic stainless steel to magnesium alloy using a nickel interlayer

The differences in physical and metallurgical properties of stainless steels and magnesium alloys make them difficult to join using conventional fusion welding processes. Therefore, the diffusion brazing of 316L steel to magnesium alloy (AZ31) was performed using a double stage bonding process. To join these dissimilar alloys, the solid-state diffusion bonding of 316L steel to a Ni interlayer was carried out at 900 °C followed by diffusion brazing to AZ31 at 510 °C. Metallographic and compositional analyses show that a metallurgical bond was achieved with a shear strength of 54 MPa. However, during the diffusion brazing stage B₂ intermetallic compounds form within the joint and these intermetallics are pushed ahead of the solid/liquid interface during isothermal solidification of the joint. These intermetallics had a detrimental effect on joint strengths when the joint was held at the diffusion brazing temperature for longer than 20 min.     

EBSD study on microstructure and texture of friction stir welded AA5052-O and AA6061-T6 dissimilar joint

Friction stir welded AA5052-O and AA6061-T6 dissimilar joint has a more obvious impact on microstructure and texture evolution compared to single material welding due to differences in physical and chemical parameters between two aluminum alloys. Microstructure, texture evolution and grain structure of AA5052-O and AA6061-T6 dissimilar joint were investigated by means of OM,EBSD and TEM measurements. Experimental results showed that FS weld was generalized in four regions–nugget zone (NZ),thermomechanically affected zone (TMAZ),heat affected zone (HAZ) and base metals (BM), using standard nomenclatures. NZ exhibited the complex structure of the two materials with flowing shape and mainly composed of the advancing side material Subgrain boundaries in weld nugget zone gradually transformed into high angle grain boundaries by absorbing dislocation and accumulating misorientations. Grain refinement of weld nugget zone was achieved by dynamic recrystallization. In the friction stir welding process, the presence of the shear deformation in weld made {001} < 100 > C cube texture, {123} < 634 > S texture in BM gradually transformed into {111} < 1(−)12(−) > A1¹ shear texture. HABs distribution were most significant in nugget followed by RS and then by AS. In TMAZ and NZ, numerous precipitates and lots of dislocations were observed.     

Comparison between contact and immersion ultrasonic method to evaluate welding residual stresses of dissimilar joints

This paper presents a comparison of contact and immersion waves used to measure residual stresses. The residual stresses are produced due to a dissimilar welding of stainless steel (304) to carbon steel (A106). Longitudinal critically refracted (L_CR) wave propagated by 2 MHz contact and immersion ultrasonic transducers is employed to measure the residual stresses. A Finite Element (FE) model of welding process, which is validated by hole-drilling method, is used to verify the ultrasonic results while an acceptable agreement is achieved. The best agreement is observed in the parent material while the maximum difference is measured in the heat affected zone (HAZ). The results show no considerable difference between using contact and immersion transducers in ultrasonic stress measurement of dissimilar joints.     

Improving interfacial reaction nonhomogeneity during laser welding–brazing aluminum to titanium

Heterogeneous interfacial reactions were easily found along the Ti/Al interface due to high temperature gradient during laser welding–brazing of Ti/Al dissimilar alloys. To improve the nonhomogeneity, relative uniform energy distribution of laser beam and appropriate groove were attempted. The effects of these attempts on the nonhomogeneity of interfacial reactions were investigated by finite element method (FEM) numerical simulation and experimental validation. The results indicate that the V-shaped groove can make the interface roughly parallel to the isotherm of the temperature field. Moreover, the rectangular spot laser can further improve homogenization of the interfacial reaction along the interface in comparison with circular spot laser. Tensile test results show that the combination of rectangular spot laser welding–brazing and V-shaped groove can effectively control the fracture of Ti/Al joints in the seam in a wide processing parameters window, and the average tensile strength reaches 278 MPa.     

Investigation of laser welding on butt joints of Al/steel dissimilar materials

Dissimilar metals of AA6013 aluminum alloy and Q235 low-carbon steel of 2.5 mm thickness were butt joined using a 10 kW fiber laser welding system with ER4043 filler metal. The study indicates that it is feasible to join aluminum alloy to steel by butt joints when zinc layer was hot-dip galvanized at the steel’s groove face in advance, and better weld appearance can be obtained at appropriate welding parameters. The joints had dual characteristics of a welding joint on the aluminum side and a brazing joint on the steel side. The smooth Fe₂Al₅ layer adjacent to the steel matrix and the serrated-shape FeAl₃ layer close to the weld metal were formed at the brazing interface. The overall thickness of Fe–Al intermetallic compounds layers produced in this experiment were varied from 1.8 μm to 6.2 μm at various welding parameters with laser power of 2.85–3.05 kW and wire feed speed of 5–7 m/min. The Al/steel butt joints were failed at the brazing interface during the tensile test and reached the maximum tensile strength of 120 MPa.     

Effectiveness of amorphous silica encapsulation technology on welding fume particles and its impact on mechanical properties of welds

Stainless steel welding generates nano-sized fume particles containing toxic metals which may cause serious health effects upon inhalation. The objective of this study was to investigate the effectiveness of an amorphous silica encapsulation (ASE) technology by evaluating its silica coating efficiency (SCE), particle morphology, and its impact on the weld’s mechanical properties. Tetramethylsilane (TMS) added to the welding shielding gas decomposed at the high-temperature arc zone to enable the silica coating. Collected welding fume particles were digested by two acid mixtures with different degrees of silica solubility, and the measured mass differences in the digests were used to determine the SCE. The SCEs were around 48–64% at the low and medium primary shielding gas flow rates. The highest SCE of 76% occurred at the high shielding gas flow rate (30 Lpm) with a TMS carrier gas flow of 0.64 Lpm. Transmission electron microscopy (TEM) images confirmed the amorphous silica layer on the welding fume particles at most gas flow rates, as well as abundant stand-alone silica particles formed at the high gas flow rate. Metallography showed that welds from the baseline and from the ASE technology were similar except for a tiny crack found in one particular weld made with the ASE technology. Tensile tests showed no statistical difference between the baseline and the ASE welds. All the above test results confirm that welding equipment retrofitted with the ASE technology has the potential to effectively address the toxicity problem of welding fume particles without affecting the mechanical properties of the welds.     

Development of a process envelope for friction stir welding of DH36 steel – A step change

Friction stir welding of steel presents an array of advantages across many industrial sectors compared to conventional fusion welding techniques. However, the fundamental knowledge of the friction stir welding process in relation to steel remains relatively limited. A microstructure and property evaluation of friction stir welded low alloy steel grade DH36 plate, commonly used in ship and marine applications has been undertaken. In this comprehensive study, plates of 2000 × 200 × 6 mm were butt welded together at varying rotational and traverse speeds. Samples were examined microscopically and by transverse tensile tests. In addition, the work was complemented by Charpy impact testing and micro-hardness testing in various regions of the weld. The study examined a wide range of process parameters; from this, a preliminary process parameter envelope has been developed and initial process parameter sets established that produce commercially attractive excellent quality welds through a substantial increase in the conventionally recognised weld traverse speed.     

Effect of tool rotational speed and pin profile on microstructure and tensile strength of dissimilar friction stir welded AA5083-H111 and AA6351-T6 aluminum alloys

The relatively new welding process friction stir welding (FSW) was applied in this research work to join 6 mm thick dissimilar aluminum alloys AA5083-H111 and AA6351-T6. The effect of tool rotational speed and pin profile on the microstructure and tensile strength of the joints were studied. Dissimilar joints were made using three different tool rotational speeds of 600 rpm, 950 rpm and 1300 rpm and five different tool pin profiles of straight square (SS), straight hexagon (SH), straight octagon (SO), tapered square (TS), and tapered octagon (TO). Three different regions namely unmixed region, mechanically mixed region and mixed flow region were observed in the weld zone. The tool rotational speed and pin profile considerably influenced the microstructure and tensile strength of the joints. The joint which was fabricated using tool rotational speed of 950 rpm and straight square pin profile yielded highest tensile strength of 273 MPa. The two process parameters affected the joint strength due to variations in material flow behavior, loss of cold work in the HAZ of AA5083 side, dissolution and over aging of precipitates of AA6351 side and formation of macroscopic defects in the weld zone.     

Fatigue life assessment of friction spot welded 7050-T76 aluminium alloy using Weibull distribution

Friction spot welding is a solid state welding process suitable to obtain spot like-joints in overlap configuration. The process is particularly useful to weld lightweight materials in similar and dissimilar combinations, and therefore an interesting alternative to other joining techniques (rivets, resistance welding, etc.). Optimum process parameters have been defined using the Taguchi method by maximizing the response variable (the lap shear strength). A study of the fatigue life was carried out on specimens welded with the above mentioned optimized process parameters. Fatigue tests were performed using a stress ratio of R = 0.10. Two-parameter Weibull distribution was used to analyze statistically the fatigue life for the joined overlapped sheets. Subsequently, the Weibull plots were drawn, as well as S–N curves considering different reliability levels. The results show that for a relatively low load, corresponding to 10% of the maximum supported by the joint, the number of cycles surpasses 1 × 10⁶, hence infinite life of the service component can be attributed. Fatigue fracture surfaces were investigated for the highest and lowest loads tested using scanning electron microscope (SEM).     

Improving friction stir weldability of Al/Mg alloys via ultrasonically diminishing pin adhesion

Formation of intermetallic compounds (IMCs) during friction stir welding (FSW) of aluminum/magnesium (Al/Mg) alloys easily results in the pin adhesion and then deteriorates joint formation. The severe pin adhesion transformed the tapered-and-screwed pin into a tapered pin at a low welding speed of 30 mm/min. The pin adhesion problem was solved with the help of ultrasonic. The weldability of Al/Mg alloys was significantly improved due to the good material flow induced by mechanical vibration and the fragments of the IMCs on the surface of a rotating pin caused by acoustic streaming, respectively. A sound joint with ultrasonic contained long Al/Mg interface joining length and complex mixture of Al/Mg alloys in the stir zone, thereby achieving perfect metallurgical bonding and mechanical interlocking. The ultrasonic could broaden process window and then improve tensile properties. The tensile strength of the Al/Mg joint with ultrasonic reached 115 MPa.     

The effect of post-weld heat treatment on the notched tensile fracture of Ti–6Al–4V to Ti–6Al–6V–2Sn dissimilar laser welds

Dissimilar welding of the Ti–6Al–4V (Ti-6-4) to Ti–6A1–6V–2Sn (Ti-6-6-2) alloys was performed by CO₂ laser in this work. The effect of post-weld heat treatment (PWHT) on the notched tensile strength (NTS) of the dissimilar weld was evaluated. Moreover, the results were also compared with the homogeneous laser welds with the same PWHT. Similar to the Ti-6-4 welds, the NTS of the FZ for dissimilar welds was less sensitive to PWHT conditions; the NTS of the FZ for distinct dissimilar welds fell within the range of 1060–1180 MPa. The results indicated a minor rise in the Mo equivalent of the titanium alloy promoted the formation of fine α + β microstructures in the form of basket weave in the welds, which resulted in high hardness accompanied with low NTS of the welds.     

Research on fatigue behavior and residual stress of large-scale cruciform welding joint with groove

Fatigue fracture behavior of the 30 mm thick Q460C-Z steel cruciform welded joint with groove was investigated. The fatigue test results indicated that fatigue strength of 30 mm thick Q460C-Z steel cruciform welded joint with groove can reach fatigue level of 80 MPa (FAT80). Fatigue crack source of the failure specimen initiated from weld toe. Meanwhile, the microcrack was also found in the fusion zones of the fatigue failure specimen, which was caused by weld quality and weld metal integrity resulting from the multi-pass welds. Two-dimensional map of the longitudinal residual stress of 30 mm thick Q460C-Z steel cruciform welded joint with groove was obtained by using the contour method. The stress nephogram of Two-dimensional map indicated that longitudinal residual stress in the welding center is the largest.     

Feasibility study of friction spot welding of dissimilar single-lap joint between poly(methyl methacrylate) and poly(methyl methacrylate)-SiO2 nanocomposite

In this work, the feasibility of friction spot welding (FSpW) of a commercial poly(methyl methacrylate) (PMMA) GS grade and a PMMA 6 N/2 wt% silica (SiO₂) nanocomposite was investigated. Single-lap joints welded at rotational speeds of 1000, 2000 and 3000 rpm were produced. The analysis of the joint microstructure and material flow pattern indicated that joints could be produced using all of the tested welding conditions. However, the joint produced at 1000 rpm displayed sharp weld lines (weak links), indicating insufficient heat input, while the welds produced at 3000 rpm displayed excessive plastic deformation (bulging of the bottom plate), volumetric defects and a lack of material mixing in the welded area, associated with higher heat input. The weld produced at a rotational speed of 2000 rpm resulted in improved material mixing, which was indicated by the absence of weld lines and volumetric defects due to the more correct heat input. This welding condition was selected for further mechanical testing. Lap shear testing of PMMA GS/PMMA 6 N/2 wt% SiO₂ nanocomposite single lap joints welded at 2000 rpm resulted in an average ultimate lap shear strength of 3.9 ± 0.05 MPa. These weld strength values are equal to or better than those obtained using state-of-the-art welding techniques for PMMA materials, thereby demonstrating the potential of friction spot welding for thermoplastic nanocomposites.     

Effects of pulsed Nd:YAG laser welding parameters and subsequent post-weld heat treatment on microstructure and hardness of AISI 420 stainless steel

Martensitic stainless steels are often used in cases where high strength and medium corrosion resistance are required. In this study, pulsed Nd:YAG laser welding of AISI 420 martensitic stainless steel is considered. Welding of samples were carried out autogenously. The spacing between samples was set to almost zero. All samples were butt welded. The effect of welding parameters such as voltage, laser beam diameter, frequency, pulse duration, and welding speed on the weld dimensions were investigated and the optimum values were obtained for the 450 V voltage, 0.6 mm focal diameter, 6 Hz frequency, 5 ms pulse duration and 1.5 mm/s welding speed. Microstructure of weld pool and heat affected zone (HAZ) were investigated by optical microscopy (OM) and scanning electron microscopy (SEM). Micro-hardness studies were also carried out. The results showed the presence of some remaining delta-ferrite in the martensitic weld structure and coarsening of M₂₃C₆ carbides in HAZ. The magnitude of hardness in the HAZ was higher than that of the weld zone. To reduce the hardness of weld and HAZ and to increase the toughness in these regions, two types of post-weld heat treatments (PWHTs) were carried out. In type 1, samples tempered for 2 h. In type 2, samples austenitizied for 0.5 h at 1010 °C and then tempered for 2 h. In order to achieve high strength and toughness, optimum temper temperatures for type 1 and 2 heat treatments were obtained for 595 and 537 °C, respectively. The results showed higher toughness for type 2 than type 1.