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1.
The present study deals with the dehydrofreezing of apples. Fresh samples (700 % db) and samples dehydrated up to different water contents (200, 100, and 30 % db) were frozen at high practical freezing rate (PFR+) and low practical freezing rate (PFR?). The effects of water content (W) and practical freezing rate (PFR) were investigated in terms of freezing characteristics: initial freezing temperature (IFT), practical freezing time (PFT), specific freezing time (SFT), thaw exudate water (TEW), and texture (maximum puncture force as index of firmness). Only high W samples (700 and 200 % db) had a significant impact of PFR in terms of PFT, SFT, and TEW. IFT decreased sharply with the decrease in the sample W. PFT greatly depended on PFR for fresh apples. PFT varied from 86 to 329 min for fresh apples at PFR+ and PFR?, respectively, whereas it was lower than 32 min for samples with W?=?30 % db. SFT decreased, equally, with sample W decrease. The TEW of fresh frozen samples, during thawing, was approximately 12 g/100 g water for low PFR (PFR?), whereas it was lower than 3 g/100 g water for samples with W?=?200 % db at the same PFR. Moreover, the impact of PFR on TEW was significant and very important for high W samples. Finally, the firmness increased when W decreased for both PFR+ and PFR?. Nevertheless, an insignificant impact of PFR on apple firmness was found. Thus, partial removal of water constitutes a promising solution to prevent the negative impacts of freezing on apple fruit firmness.  相似文献   

2.
Potatoes are an important food in many regions of the world and are commonly used in a variety of food products. Thermal transition and thermo-physical properties of potatoes are important in order to design efficient food processes and select appropriate storage conditions. In this study, we determined the thermal transitions and thermophysical properties of raw and blanched/par-fried potato for a temperature range of ??32 to 21.1 °C. Using differential scanning calorimetry, we found an initial freezing point (Tf) at ??1.8?±?0.1 °C, an onset of melting (Tm) at ??9.9?±?0.2 °C and an unfreezable water content (Xw) for maximally freeze-concentrated raw potato at 0.21 kg water/kg potato. Corresponding values for blanched/par-fried potatoes were ??0.9?±?0.1 °C, ??11.0?±?0.2 °C and 0.18 kg water/kg potato. Results show that an increase in solids content decreased Tf of both raw and blanched potatoes. We modelled the relationship between them using the Chen model. The apparent specific heat (Capp) increased around Tf to 31.7?±?1.13 kJ/kg K for raw potato and 26.7?±?0.62 kJ/kg K for blanched/par-fried potato. For frozen raw potato at ??32 °C, thermal diffusivity (α) was 0.89?±?0.01?×?10??6 m2/s and thermal conductivity (k), 1.82?±?0.14 W/m K, respectively. These values were higher for frozen raw potato than for the unfrozen raw potato (0.15?±?0.01?×?10??6 m2/s and 0.56?±?0.08 W/m K, respectively at 21.1 °C). The apparent density (ρ) of frozen raw potato (992?±?4.00 kg/m3 at ??32 °C) was less than that for unfrozen raw potato (1053?±?4.00 kg/m3 at 21.1 °C), and a similar trend was obtained for blanched/par-fried potato (993?±?2.00 kg/m3 at ??32 °C and 1188?±?7.00 kg/m3 at 21.1 °C, respectively). This study established a correlation between thermo-physical properties and temperature. Findings may be used to inform the design and optimization of freezing processes and frozen storage for potato products.  相似文献   

3.
Storage potential and eating quality of guava (Psidium guajava L.) fruit depend on its maturity. Segregation of guava according to maturity and firmness measured using non-destructive technologies would help the industry to designate ripe fruit to immediate market and less ripe fruit for distant market (e.g., exportation). This research was conducted to evaluate the potential of experimental resonant frequency (f e) and elasticity index (EI) to estimate fruit firmness, which has been reported to be inversely correlated to its maturity. A maturity index (I m) was calculated as the ratio of total soluble solids/titratable acidity (TSS/TA). It was proved that TSS, TA, and I m were significantly correlated (P?<?0.05) to skin firmness (F s), flesh firmness (F f), stiffness (S), and analytical resonant frequency (ω n ), being S the attribute best fitted to I m (R 2?=?0.77). Since it was observed that f e and EI were sensitive to changes in fruit firmness, both of them were explored as alternatives to predict F s, F f, S, and ω n of guava fruit. In some cases, EI improved the models to predict guava firmness traits (e.g., F s vs f e had a coefficient of determination of R 2?=?0.58, whereas for F s vs EI, it was R 2?=?0.62). The best model occurred when plotting ω n vs f e (R 2?=?0.86), followed by S vs EI (R 2?=?0.84), making these promising features for the development of a new practical application using frequency response measurement as a non-destructive method to assess guava maturity.  相似文献   

4.
The present investigation studied the freezing of strawberries by immersion in CaCl2 solutions, analysing drip loss, pectin content and the degree of esterification of the pectins, total and cell-wall bonded calcium contents, the ratio bonded calcium/total calcium, and textural parameters. In addition, the effect of immersion in pectin methylesterase (PME) solutions prior to immersion freezing (IF) was analysed. The firmness of thawed fruit decreased by approximately 74% with respect to fresh strawberries, and neither IF-CA (freezing by immersion in CaCl2 solution) nor PME–IF-CA (immersion in PME solution + freezing by immersion in CaCl2 solution) provided significant benefit in maintaining firmness when compared to slow freezing (SF). However, IF provided a significant benefit in reducing drip loss of thawed strawberries when compared to SF, but pre-treatment with PME did not provide any additional benefit.  相似文献   

5.
The effects of freezing pre-treatment and ultrasound application during drying on microstructure, drying curves, and bioactive compounds of beetroot have been evaluated. Raw and previously frozen (at ? 20 °C) beetroots were convectively dried (40 °C and 1 m/s) with and without ultrasound application using two acoustic densities (16.4 and 26.7 kW/m3), and a diffusional model was proposed to simulate the drying curves. Freezing pre-treatment and ultrasound application caused significant disruptions in the beetroot microstructure and reduced the drying time, enhancing the mass transfer. The external mass transfer coefficient significantly (p < 0.05) increased by 28–49% when ultrasound was applied; moreover, the effective diffusion coefficient significantly (p < 0.05) increased by 60–73% and 204–211%, respectively, due to the ultrasound application on the drying of raw and pre-frozen samples. Freezing caused significant (p < 0.05) increases in betalain and total polyphenol contents and antioxidant activity compared with the raw sample (16–57%), probably due to the release of free forms from the food matrix; meanwhile, drying had the opposite effect (8–54% decrease). Significantly (p < 0.05) higher decreases (32–81%) in bioactive compounds and antioxidant activity were observed when drying was assisted by ultrasound compared with dying without ultrasound. Therefore, freezing pre-treatment and ultrasound application enhanced mass transfer during drying. However, significant changes in quality parameters of the final product were observed.  相似文献   

6.
Freezing characteristics (freezing time, latent heat of fusion of ice, and freezable water content) and quality parameters (drip loss, color, firmness, and l-ascorbic acid content) of broccoli (osmodehydrofrozen and ultrasound-assisted osmodehydrofrozen) during frozen storage were investigated. Freezing time, latent heat of fusion of ice, and freezable water content of osmodehydrated samples decreased significantly compared to samples which were not under osmotic dehydration. The changes of drip loss, color, firmness, and l-ascorbic acid content of osmodehydrofrozen and ultrasound-assisted osmodehydrofrozen broccoli during frozen storage were inhibited markedly compared to samples which were not submitted to osmotic dehydration before freezing. Compared to osmotic dehydration, the ultrasound-assisted osmotic dehydration shortened the needed dehydration time and better preserved the firmness and l-ascorbic acid content after osmotic dehydration pretreatment. In addition, the ultrasound-assisted osmotic dehydration minimized the drip loss and loss of l-ascorbic acid content and better maintained the color and firmness when stored at ?25 °C for 6 months. These findings indicate that it is promising to apply ultrasound-assisted osmodehydrofreezing in freezing and frozen storage of food.  相似文献   

7.
The consumption of apple chips is increasing in the last decades because of the consumer’s preferences towards healthy snacks. However, the enzymatic browning, which is attributed mainly to polyphenol oxidase (PPO, EC 1.10.3.1) activity, negatively affects the sensory, nutritional, and antioxidant properties of dried apples as a consequence of the oxidation of phenolic substrates during post-harvest stages. The antibrowning and antioxidant effects of dipping pre-treatments with unripe grape juice as well as reference formulations including a mixture of 1% w/v ascorbic acid and 1% w/v citric acid, 6% w/v NatureSeal®, and 0.1% w/v sodium metabisulfite were evaluated by spectrophotometric and colorimetric assays on dried “Golden Delicious” apple slices. Based on HPLC analysis, the treated apple slices were enriched with bioactive compounds which effectively improved antioxidant capacity and limited enzymatic browning by increasing lightness, reducing color change, and inhibiting PPO activity. Hence, the juice of unripe grapes recovered as agricultural wastes during bunch thinning of vineyards could be proposed as a safe, inexpensive, and eco-friendly alternative to conventional antibrowning treatments in apple processing.  相似文献   

8.
Microwave drying is usually combined with vacuum environment in conjunction with hot air flow to draw the moisture rapidly. The moisture content of the vegetables undergoing drying is hard to measure online. This research designed a microwave vacuum drying (MVD)-low-field nuclear magnetic resonance (NMR) smart device and investigated the feasibility of NMR method for online measurement of state of moisture during MVD. The relation between the signal amplitude (A 2) and the true moisture content (M 1) of six kinds of vegetables (mushroom, carrot, potato, lotus, edamame, vegetable corn) was fitted to estimate if NMR can measure the M 1 of vegetables directly. Results showed that A 2 and M 1 of different fresh vegetables had no single empirical mathematical model to fit. However, for each kind of these vegetables, the A 2 and corresponding M 1 in different MVD stages showed a significant linear relationship. The predicted moisture content (M 2) of mushroom: M 2 = 5.25351 × 10?4 A 2 ? 0.34042, R = 0.996; carrot: M 2 = 5.78756 × 10?4 A 2 ? 0.14108, R = 0.998; potato: M 2 = 3.10019 × 10?4 A 2 ? 0.10612, R = 0.991; lotus: M 2 = 2.32415 × 10?4 A 2 ? 0.01573, R = 0.998; edamame: M 2 = 3.13310 × 10?4 A 2 ? 0.4198, R = 0.996; vegetable corn: M 2 = 1.69461 × 10?4 A 2 ? 0.09063, R = 0.995. The linear models between M 2 and A 2 were able to estimate the end point (M 1 < 8%) of MVD with a high accuracy (P > 0.950).  相似文献   

9.
Two singleplex TaqMan methods were developed for the detection of potato targets: one for the detection of the tpinII terminator, which is an emerging terminator used in GM constructs, and one for the detection of the endogenous StLS gene of potato. Performance criteria such as specificity and sensitivity were successfully tested for the two methods, taking into account the recommendations of international guidelines. The presence of the StLS target was checked in 16 potato cultivars. The StLS target is present at low copy number and can be used for quantitation purposes, as demonstrated on transgenic potatoes in this paper. The StLS target is an excellent candidate to replace the presently recommended endogenous target based on the UGP gene, which shows several disadvantages due to its high copy number and lack of specificity. The research also indicates that DNA can easily be extracted from different parts of potato tubers with a classical cetyltrimethylammonium bromide method.  相似文献   

10.
A modified diffusion-based mathematical model is proposed to describe the moisture movement during continuous and intermittent drying of Eucalyptus saligna. This model includes the temperature change, the surface drying coefficient (β n ) and 2 diffusion coefficients [from green to FSP (D f ) and from FSP to dry condition (D o )] as important parameters. The final model expression obtained was M?=?exp (??25 β n 2 D t /l2) with the β n used was 1.5807 kg m?2 s?1, the D f was 2.26?×?10?11 m2 s?1, and the D o was 5.85?×?10?12 m2 s?1. The range of temperature change between heating and non-heating phases in the intermittent drying regimes was from 24.9 to 31.8 °C. The R2 values obtained when the model was fitted into the drying data of different intermittent regimes ranged from 71.5 to 85.9%. The R2 value was 87.4% when the model was fitted into continuous trial data. The high values of R2 indicate that the model can be used to understand the moisture reduction both in intermittent and continuous regimes.  相似文献   

11.
Seeds from fruits such as Citrullus (C.) lanatus (watermelon) and Limonia (L.) acidissima (wood apple) are not commonly utilized but could be suitable in numerous food formulations. It was shown that the protein content of defatted seed flours was 71.38 and 49.51 % and that these contained considerable amounts of minerals such as Na, Mn, Mg, K, Cu, Fe and Zn. The defatted L. acidissima seed flour was superior to C. lanatus in essential amino acids. The flours obtained from both seeds were also evaluated for functional properties and characterized by X-ray diffraction, differential scanning calorimeter and scanning electron microscope (SEM). Amorphous nature was observed in defatted C. lanatus and L. acidissima flours due to the low percentage of degree of crystallinity. Spherical morphologies were observed through SEM. The exothermic peak was recorded in defatted C. lanatus and L. acidissima flour.  相似文献   

12.
In order to identify the geographical origin of pure milk, different proteins and milk water were extracted from pure milk originated from Australia and New Zealand, Germany and France, the USA, and China. Then, δ 13C and δ 15N values of the extracted proteins and δ 2H and δ 18O values of milk water were determined by element analyzer-isotope ratio mass spectrometry (EA-IRMS). The results indicated that pure milk from these regions could be potentially discriminated by using analyte δ 13C, δ 15N, δ 2H, and δ 18O. The P value analysis of them was highly significant (P?<?0.01) considering the origins. 3D distribution of δ 13C, δ 15N, δ 2H, and δ 18O can also clearly present regional concentration phenomena according to the regions of pure milk. Therefore, it can be concluded that δ 13C, δ 15N, δ 2H, and δ 18O analysis could potentially be rapid and routine for origin discrimination of pure milk.  相似文献   

13.
Results are presented of research, the aim of which has been to determine the selected physicochemical qualities, including electric quantities, of apple purées and pulpy juices obtained from them. The characteristics of the electric properties have covered the measurements of impedance (Z) and effective resistance (R), admittance (Y) and conductance (G), as well as equivalent parallel capacitance (Cp) and equivalent series capacitance (Cs). Changes have been determined in the purée properties relating to the technology of production as well as the function of diluting and the storage period. Apple purées, depending on the production technology, are characterized by the diversified, characteristic ranges of the resistivity and conductivity values. As the degree of the purée dilution rises, conductivity of juices falls. These relationships remain true throughout the purée storage period. In the conditions of the experiment, the measured values of resistivity and conductivity of pulpy juices clearly determine the content of apple purées in juices.  相似文献   

14.
The quantitative analytical methods for seven N-nitrosamines including N-nitrosodimethylamine (NDMA), N-nitrosomethylethylamine (NMEA), N-nitrosodiethylamine (NDEA), N-nitrosodibutylamine (NDBA), N-nitrosopiperidine (NPIP), N-nitrosopyrrolidine (NPYR), and N-nitrosomorpholine (NMOR) were established for agricultural food matrices. Four food matrices were used for the method development: rice soup as a fatless solid matrix, apple juice as a fatless liquid matrix, corn oil as a fat-rich liquid matrix, and 20 % alcohol as an alcohol matrix. A combination of solid-supported liquid-liquid extraction (SLLE) using Extrelut NT and a solid phase extraction (SPE) using Florisil was employed for fatless matrices. For an alcohol matrix, only SLLE was used without SPE, and liquid-liquid extraction (LLE) was established for a fat-rich matrix. The extract was analyzed by gas chromatography-positive chemical ionization-tandem mass spectrometry (GC-PCI-MS/MS) using ammonia gas as an ion source. Linearity, recovery, repeatability, inter-day precision, reproducibility, and uncertainty were evaluated for method validation using four matrices. Method detection limits for all of the investigated N-nitrosamines were ranged from 0.10 to 0.18 μg/kg for the rice soup, from 0.10 to 0.19 μg/kg for the apple juice, 0.10 μg/kg for the corn oil, and from 0.10 to 0.25 μg/kg for 20 % alcohol, depending on N-nitrosamines. Established methods were applied to determine seven N-nitrosamines in some agricultural food products.  相似文献   

15.
The effect of ultrasound (US) (40 kHz, 200 W, 3 min), blanching (85 °C, 3.5 min), and the combination of both methods was evaluated on the quality of vacuum-packaged potato strips stored at 3 ± 1 °C for up to 10 days. For this study, two cultivars of potatoes were assessed. For blanched Agata samples, the lightness (L*) decreased over 12 % (p < 0.05). Moreover, their hue increased up to 100, obtaining lesser yellow potato strips. In contrast, US did not affect the hue values. The losses of firmness of blanched potato strips were notable (35 % for Agata and 51 % for Agria), whereas US did not change this property (p < 0.05). Nevertheless, no significant differences were found in the total starch content at 10 days. Agata and Agria showed different metabolic behaviors of sucrose in the refrigerated storage. Therefore, Agria cultivar retained better color after frying. These results suggest that US had less impact on color and improve the firmness in vacuum-packaged potato strips with no added chemicals.  相似文献   

16.
Urea formaldehyde (UF) resin-impregnated Chinese fir (Cunninghamia lanceolata (Lamb.)Hook.) was dried at different temperatures in an atmospheric pressure superheated steam dryer. Drying characteristics, moisture content, drying rate, temperature profile, drying defects, and color change were investigated. The moisture content was reduced from 66.21 to 11.79% within 30 h without causing severe drying defects; in contrast, the conventional hot air process required 7–8 days. After 25 h of drying, the temperatures at both the center and the surface of wood remained stable. After 34.5 h, the surface temperature gradually approached the steam temperature. The color of the superheated steam dried Chinese fir appeared slightly more intense yellow and red than the control. Investigation of the UF-impregnated Chinese fir wood by scanning electron microscopy (SEM) revealed that the majority of the lumens and voids, including the microvoids in wood structure, was filled with urea formaldehyde resin.  相似文献   

17.
Trypsin inhibitor activity (TIA) in soybean is attributed to two polypeptides, namely, Kunitz trypsin inhibitor (KTI) and Bowman-Birk inhibitor (BBI). Standard spectrophotometric protocol widely followed for estimation of TIA is cumbersome and does not distinguish KTI from BBI. In the present investigation, extraction conditions for KTI were optimized and different forms of this polypeptide were resolved in 180 soybean genotypes of Indian and exotic origin through native PAGE. This led to the identification of three KTI alleles, namely, Tia, Tib, and Tic, with Tia occurring in most of the Indian genotypes. Trypsin-KTI complex assay exhibited binding of Tia polypeptide with 2.51 fold concentration of trypsin. Subsequently, seeds of selected genotypes were subjected to estimation of KTI and BBI activity through densitometry and enzyme-linked immunosorbent assay (ELISA), respectively; and total TIA through standard spectrophotometric protocol. Summation of KTI and BBI was significantly (P?<?0.05) lower than that of TIA determined through the spectrophotometric method.  相似文献   

18.
Structural and rheological characterization of reconstituted hydrogels developed from A. vera non-fibrous alcohol insoluble residue (NFAIR) powder using different methods [viz., shaking (S), heating-shaking (HS), and heating (H)] and concentrations (viz., 0.2–1.6 %, w/v) was carried out. Functional group distribution by FTIR spectroscopy and Congo red (CR) method revealed the presence of acetylated acemannan in A. vera powder. Dynamic oscillation studies of A. vera (NFAIR) fluids at all concentrations of 0.2–1.6 %, w/v, showed gel strength in the order of H > HS > S method. However, in H method, increase in concentration from 0.2 to 1.6 %, w/v showed the conformational transition from semi-diluted solution to weak gel nature. Rheological models described the effect of heating temperatures (HT); 30–90 °C, and times (Ht); 15–60 min on viscoelastic behavior in reconstituted A. vera fluids. The reconstituted A. vera hydrogel prepared with a concentration of 1.6 %, w/v using 50 °C (HT) and 30 min (Ht) condition showed a good agreement with the Power law (storage modulus, G′) and Weak gel model (complex modulus, G*) fitted data (R2 > 0.94) resulting higher viscoelastic moduli intercepts; G0 (71.5 Pa s n), G0 (33.5 Pa s n), lower slopes; n′ (0.22), n″ (0.06), higher network strength (A F , 121.3 Pa s1/z ) and number of network (z, 5.3) values. The obtained results suggested that heating at 50 °C/30 min can develop aqueous weak gel networks of A. vera with enhanced gel strength which may be utilized as a novel gelling agent for wide variety of targeted applications in food and pharmaceutical sectors.  相似文献   

19.
Shredded cabbage (50 % v/v) and Daikon radish cubes (57 % v/v) with different salt concentrations (0.15, 0.5, 1, 1.5, and 1.85 %) were heated from 30 to 70 °C in a static ohmic heating cell at different voltages (65, 80, 100, 120, and 135 V) and frequencies (60, 2070, 5030, 7990, and 10,000 Hz) to evaluate their ohmic heating behaviour. Radish heated under 1.5 % salt, 120 V and 7990 Hz or 1 % salt, 135 V and 5030 Hz conditions gave the shortest heating time of 6 min from 30 to 70 °C, and cabbage gave the longest time of 128 min at 0.15 % salt, 100 V, and 5030 Hz. Regression models of heating rate as a quadratic function of the sample temperature gave R2 >0.98. The general trend observed was that the magnitude of the heating rate increased with frequency at high voltage but decreased at low voltage for cabbage, while the opposite trend was observed for radish. Heating was more efficient at higher salt concentration and applied voltage. Radish heated more rapidly than cabbage. A slight slope change was observed in all cases between 50 and 60 °C. The response surface models revealed linear, cross products and quadratic effects to be significant with R 2 over 0.98.  相似文献   

20.
Factor analysis (FA) method was tested to assess quality of chicken breast fillets with the visible/near-infrared (Vis/NIR) spectroscopy with wavelength range between 400 and 2500 nm. According to inherent correlation, three factors were extracted from the measured eight quality traits (L*, a*, b*, pH, moisture, drip loss, expressible fluid, and salt-induced water gain). The extracted “grade factor” (F 1), “color factor” (F 2), and “moisture factor” (F 3) could respectively represent the characteristics and the variation tendency of the corresponding quality traits and were defined as three new quality assessment indexes. Furthermore, partial least squares regression (PLSR) models were established to quantitatively relate spectral information to eight individual quality traits and three factors. The results indicated that the models for predicting each factor performed better than those for individual quality traits. Key wavelengths of each quality trait were then selected, and the corresponding spectra were taken to build new PLSR prediction models. The selected key wavelengths showed obvious practical significance, and the new models had comparable predictive performance to those models developed based on the full spectra, among which the new models of F 1 and F 2 had acceptable and robust predictive abilities (R2p?=?0.73, RPD?=?1.91; R2p?=?0.74, RPD?=?1.97). Our results in the present study demonstrate the potential for FA and Vis/NIR spectroscopy as a useful method to assess the quality of chicken breast fillets.  相似文献   

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