Effect of microstructure on the fatigue crack growth behaviour of a near-α Ti alloy

Fatigue crack growth behaviour of Ti–6Al–2Zr–1.5Mo–1.5V (VT-20 a near-α Ti alloy) was studied in lamellar, bimodal and acicular microstructural conditions. Fatigue crack growth tests at both increasing and decreasing stress intensity factor range values were performed at ambient temperature and a loading ratio of 0.3 using compact tension samples. Lamellar and acicular microstructures showed lower fatigue crack growth rates as compared to the bimodal microstructure due to the tortuous nature of cracks in the former and the cleavage of primary α in the latter. The threshold stress intensity factor range was highest for acicular microstructure.     

Effects of microstructure on mixed-mode, high-cycle fatigue crack-growth thresholds in Ti-6Al-4V alloy

Effect of microstructure on mixed‐mode (mode I + II), high‐cycle fatigue thresholds in a Ti‐6Al‐4V alloy is reported over a range of crack sizes from tens of micrometers to in excess of several millimeters. Specifically, two microstructural conditions were examined—a fine‐grained equiaxed bimodal structure (grain size ～20 µm) and a coarser lamellar structure (colony size ～500 µm). Studies were conducted over a range of mode‐mixities, from pure mode I (ΔK_II/ΔK_I = 0) to nearly pure mode II (ΔK_II/ΔK_I ～ 7.1), at load ratios (minimum load/maximum load) between 0.1 and 0.8, with thresholds characterized in terms of the strain‐energy release rate (ΔG) incorporating both tensile and shear‐loading components. In the presence of through‐thickness cracks—large (> 4 mm) compared to microstructural dimensions—significant effects of mode‐mixity and load ratio were observed for both microstructures, with the lamellar alloy generally displaying the better resistance. However, these effects were substantially reduced if allowance was made for crack‐tip shielding. Additionally, when thresholds were measured in the presence of cracks comparable to microstructural dimensions, specifically short (～200 µm) through‐thickness cracks and microstructurally small (< 50 µm) surface cracks, where the influence of crack‐tip shielding would be minimal, such effects were similarly markedly reduced. Moreover, small‐crack ΔG_TH thresholds were some 50–90 times smaller than corresponding large crack values. Such effects are discussed in terms of the dominant role of mode I behaviour and the effects of microstructure (in relation to crack size) in promoting crack‐tip shielding that arises from significant changes in the crack path in the two structures.     

Rissfortschritts‐ und Ermüdungsverhalten der Aluminiumlegierung EN AW‐6060 nach ECAP und nachgelagerter Wärmebehandlung

Crack growth and high cycle fatigue behaviour of an AA6060 aluminium alloy after ECAP combined with a subsequent heat treatment Crack growth properties of the Al‐Mg‐Si alloy AA6060 as well as the high cycle fatigue behaviour have been investigated after equal‐channel angular pressing (ECAP). In our study, experiments have been conducted on different stages of microstructural breakdown and strain hardening of the material as they were present after different numbers of ECAP passes. A bimodal condition, obtained after two pressings, and a homogeneously ultrafine‐grained condition after eight repetitive pressings have been investigated. Furthermore, optimized conditions with an enhanced ductility, produced by ECAP processing combined with a following short‐time aging treatment were included into the study. Crack growth experiments have been conducted in the near‐threshold regime and the region of stable crack growth, covering a range of load ratios from R = 0.1 up to 0.7. It was found that the lowered fatigue threshold ΔK_th of the as‐extruded material can be enhanced by the combination of ECAP and short‐time aging, owing to the increased ductility and strain hardening capability of this material. By means of SEM investigations and tensile tests, the crack growth properties of the different conditions were related to microstructural and mechanical features. In fatigue tests, load reversals up to failure and the fatigue limit for an as‐extruded condition and an optimized condition after two ECAP‐passes have been compared to the coarse grained initial condition and a remarkable increase in fatigue strength was noted.     

Richtungsabhängigkeit der Rissausbreitung bei einem gefügebedingten Übergang von rauigkeits‐ zu plastizitätsinduzierter Rissschließung an der Legierung Ti‐6Al‐4V

On the titanium alloy Ti‐6Al‐4V a rugged transition from equiaxed to lamellar microstructure was produced by a specific thermomechanical treatment. Equiaxed microstructures of this alloy show plasticity induced crack closure over a wide range of ΔK whereas for lamellar microstructures roughness induced crack closure is observed up to relatively high loadings. Thus by the obtained microstructural transition the observation of a change of the crack closure mode becomes feasible at constant loading ΔK. For the crack propagation from equiaxed to lamellar microstructure, i. e. from plasticity to roughness induced crack closure, the closure load corresponds always to the particular microstructure at the crack tip. In the opposite direction significant closure effects in the crack path interfere leading to an increase of the crack closure load and consequently to a reduction of the crack velocity. Hereby for constant ΔK the crack velocity becomes dependent on the crack propagation direction.     

Local strain accumulation in fatigue crack propagation process of Ti‐6Al‐4V alloy

Fatigue crack growth behaviours of the titanium alloy Ti‐6Al‐4V, with two different microstructures, at different maximum stresses were identified by digital image correlation technique. Full‐field strains were monitored around fatigue cracks after consecutive cycles in fatigue crack growth experiments. Results indicated that the Ti‐6Al‐4V alloy with a bi‐modal microstructure had a better fatigue resistance than that with a primary‐α microstructure. Typical behaviours of small cracks and the evolution of multi‐scale fatigue cracks were clarified. The strain accumulations around the micro‐notch and fatigue crack increased with increasing number of load cycles. On the basis of von Mises strain mapping, it was found that crack growth rate could be characterized by crack‐tip plastic zone size.     

Short fatigue cracks in intermetallic γ‐TiAl‐alloys

Fatigue crack growth at room temperature and its relation to the local microstructure is studied for four different γ‐TiAl‐alloys with microstructures ranging from coarse and fully lamellar to fine and partly lamellar. It is shown that the number of cycles to failure depends strongly on the efficiency of the first barrier to crack extension, as crack growth rates may increase rapidly once this barrier has been breached by a specific crack. The crack extension behaviour for two typical barriers (colony boundary and twin boundary) is studied using high‐resolution optical and scanning electron microscopy.     

Influence of microstructure of (α+β) Ti-6.2.4.6 alloy on high-cycle fatigue and tensile test behaviour

Tensile and gigacyclic fatigue behaviour of Ti–6Al–2Sn–4Zr–6Mo alloy were investigated as a function of lamellar primary α- and β-transformed microstructures. Three thermomechanical processes (TP1, TP2, TP3) were selected to produce different combinations of microstructural features on two slightly different compositions of the alloy (A and B). Ultrasonic fatigue tests were performed in air and liquid nitrogen at a frequency of 20 kHz ( R = −1, T  = 300 and 77 K), giving fatigue tests up to 10⁹ cycles. Microstructural features and the fracture initiation dependence on the primary α lamellar phase were observed by SEM and/or characterized by quantitative image analysis. It has been found that the microstructure of alloy B produced by TP1 represents a better compromise between resistance to initiation and resistance to microcrack growth. Quicker initiation occurs in coarser α-platelets (TP2, alloy B), and the continuous partially transformed β matrix appears to effectively decrease the tensile and HCF resistance. The bimodal structure (TP3, alloy B) has the best resistance at room temperature, but the presence of a coarse globular phase decreases this fatigue resistance at low temperature.     

Fatigue crack growth behaviour of gas tungsten arc,electron beam and laser beam welded Ti–6Al–4V alloy

The present investigation is aimed to evaluate fatigue crack growth parameters of gas tungsten arc, electron beam and laser beam welded Ti–6Al–4V titanium alloy for assessing the remaining service lives of existing structure by fracture mechanics approach. Center cracked tensile specimens were tested using a 100 kN servo hydraulic controlled fatigue testing machine under constant amplitude uniaxial tensile load. Crack growth curves were plotted and crack growth parameters (exponent and intercept) were evaluated. Fatigue crack growth behavior of welds was correlated with mechanical properties and microstructural characteristics of welds. Of the three joints, the joint fabricated by laser beam welding exhibited higher fatigue crack growth resistance due to the presence of fine lamellar microstructure in the weld metal.     

Comparative study of fatigue and fracture in friction stir and electron beam welds of 24 mm thick titanium alloy Ti‐6Al‐4 V

In this study, friction stir welding of Ti‐6Al‐4 V was demonstrated in 24 mm thickness material. The microstructure and mechanical properties, fatigue, fracture toughness and crack growth of these thick section friction stir welds were evaluated and compared with electron beam welds produced in the same thickness material. It was found that the friction stir welds possessed a relatively coarse lamellar alpha transformed beta microstructure because of slow cooling from above the transus temperature of the material. The electron beam welds had a fine acicular alpha structure as a result of rapid solidification. The friction stir welds possessed better ductility, fatigue life, fracture toughness and crack growth resistance than the base meal or electron beam welds. Thus, even though friction stir welding is a relatively new process, the performance benefits it offers for the fabrication of heavy gage primary structure make it a more attractive option than the more well‐established electron beam welding method.     

The effect of microstructures on fatigue crack growth in Q345 steel welded joint

It is a traditional that the fatigue crack growth behavior is sensitive to microstructure in threshold regime, while it is sensitive to R‐ratio in Paris regime. Fatigue test is carried out for welded joints of a Q345 steel where the compact tension specimens with 3.8 and 12.5 mm thickness are used, and comparisons of fatigue crack growth behavior between base metal and a few different locations in the welded joint are considered in Paris regime. Welding residual stresses are removed by heat treatment to focus the study on the microstructural effect. It is shown that fatigue crack growth rate (FCGR) in the base metal is not sensitive to R‐ratio, but the FCGR increases in the overheated zone, the fusion zone and the weld metal zone with R‐ratio increasing. To the low R‐ratio, FCGR in the three zones is smaller than that in the base metal, but they approximate the same with base metal under the high R‐ratio. The mechanism of fatigue crack growth is analyzed through crack path in microstructures and SEM fractograph. The coarse‐grained ferrite in the base metal is of benefit to relaxation of the average stress at the crack tip, and the fatigue crack growth predicts branching and deflection within above different locations in the welded joint. These tortuous crack paths with crack branching and deflection will promote crack closure as well as crack‐tip stress shielding and then resulted in higher crack growth resistance.     

Effects of microstructural through‐thickness non‐uniformity and crack size on fatigue crack propagation and fracture of rolled Al‐7075 alloy

Some of the fatigue tests performed using the standard compact tension (CT) and a non‐standard specimen made of rolled 7075 aluminium alloy exhibit fatigue crack growth (FCG) lagging in a small region along the crack front. Through‐thickness microstructural evaluation shows that material grains in this region did not flatten as much as other regions. In the non‐standard specimen, surface cracks are either grown under fatigue loading or broken under monotonically increasing quasi‐static loads at different crack sizes. The aforementioned lagging also exists in a narrow region of 3‐D FCG for specimens with microstructural through‐thickness non‐uniformity. A more important feature for this type of specimen with surface crack is the deflection of fast fracture direction into the grain interfaces, namely from L‐T orientation to S‐L and S‐T directions. It is proved that this is due to significant levels of second principal stresses near the free surface for small cracks and lower fracture toughness of the material in S‐L and S‐T directions.     

Ausbreitungsverhalten mikrostrukturell kurzer Ermüdungsrisse – experimentelle Charakterisierung und mechanismenorientierte Simulation

Propagation behaviour of microstructural short fatigue cracks – experimental characterization and mechanism‐based simulation This paper presents results of an interdisciplinary research project, which was undertaken by the authors during the past seven years on the subject of experimental characterization and modelling of microstructurally short fatigue crack growth. Fatigue testing was carried out on the austenitic‐ferritic duplex stainless steel X2 CrNiMoN 22–5‐3. It was shown clearly that microstructural features like grain size, phase distribution or yield stress of the grain containing the crack tip control an advancing short crack. On the basis of these findings, a mechanism‐oriented model was established, which is able to simulate the growth of microstructurally short fatigue cracks in a physically reasonable way. Microstructural parameters like grain size, grain distribution, grain orientation etc. are taken into account by assigning measured values to a modelled microstructure, in which the crack growth simulation takes place. The comparison of experimentally observed and calculated values shows excellent agreement.     

Effect of stress ratio on fatigue crack growth in TiAl intermetallics at room and elevated temperatures

The fatigue crack growth behavior of γ-based titanium aluminides (TiAl) with a fine duplex structure and lamellar structure has been investigated by scanning electron microscope (SEM) in situ observation in vacuum at 750°C and room temperature. For the duplex structured material the fatigue crack growth rates are dominated by the maximum stress intensity, particularly at 750°C. The threshold stress intensity range for fatigue crack growth at 750°C is lower than that at room temperature for any corresponding stress ratio. The fatigue crack growth rate at 750°C is affected by creep deformation in front of the crack tip. The severe crack blunting occurs when the stress ratio is 0.5. For the lamellar structured material the scatter of fatigue crack growth data is very large. Small cracks propagate at the stress intensity range below the threshold for long fatigue crack growth. The effects of microstructure on fatigue crack growth are discussed.     

MICROSTRUCTURAL EFFECTS ON SMALL FATIGUE CRACK INITIATION AND GROWTH IN Ti6A14V ALLOYS

Abstract— The nucleation and growth of small naturally initiated cracks have been investigated on Ti 6 Al 4V alloys, with bimodal or globular microstructures. Tests have been performed in air at a stress amplitude near 0.75 of the yield stress. The influence of microstructure on fatigue damage is described and the differences in fatigue life of some titanium alloys are explained. The effect of microstructure on fatigue resistance is mainly related to the early stages of damage including initiation and small crack growth. Coalescence processes favoured by a high density of initiated surface microcracks in fine α grain material, or rapid initiation of large cracks in coarse α colonies, explains low fatigue resistance or lifetime scattering in globular alloys. Small crack growth retardation due to α/β barriers associated with a low surface crack density, limiting coalescence processes, explains the highest resistance of bimodal structures.     

Effect of post-weld heat treatment on fracture toughness and fatigue crack growth behaviour of electron beam welds of a titanium (α+β) alloy

The effects of a post-weld heat treatment on the fracture toughness and fatigue crack growth behaviour of electron beam welds of an α + β titanium alloy, Ti–6.5Al–1.9Zr–0.25Si have been studied. Welds in the stress-relieved condition exhibited poor fracture toughness due to poor energy absorbing capacity of the thin α and α' phases. Post-weld heat treatment which resulted in the decomposition of α' to α + β and the coarsening of intragranular and intergranular α resulted in improved toughness. This improvement in the toughness is related to improved ductility leading to crack blunting, crack path deviation at the thick intragranular and intergranular α phase. Fatigue crack growth resistance of welds was superior to the base metal in the α + β heat-treated condition. The superior crack growth resistance of the welds is due to the acicular α microstructure which results in a tortuous crack path and possible crack closure arising from crack path tortuosity.     

Fusion zone microstructure and fatigue crack growth behaviour in Ti-6Al-4V alloy weldments

Abstract

The fatigue crack growth resistance of α–β titanium alloys can be altered by microstructural modification. During welding, the fusion zone microstructure depends on cooling rate. In the present work, the alloy Ti-6Al-4V was welded over a range of heat inputs, using electron beam and gas tungsten arc welding. The weld microstructure varied from predominantly martensitic under rapid cooling conditions to a mixture of martensite and diffusional products on slower cooling. Post-weld heat treatment resulted in a basketweave α–β aggregate that coarsened with temperature and time. In all welded and heat treated conditions, the fusion zone exhibited a fatigue crack growth resistance superior to that of the base material, which was in part attributed to the lamellar microstructure of the fusion zone. Welding residual stresses also played a beneficial role in the as welded condition. Post-weld heat treatment eliminated the advantage resulting from the welding stresses but not that as a result of microstructure.     

Microstructurally-dependent model for predicting the kinetics of physically small and long fatigue crack growth

Based on the proposed concept of the fatigue threshold stress intensity factor ranges, a model has been developed that describes the kinetics of physically small fatigue crack and long fatigue crack growth. The model allows the calculation of the crack growth rate under the regular fully-reversed uniaxial loading from the data on the static characteristics of mechanical properties and the microstructure of the initial material. The crack depth at which the cyclic plastic zone size ahead of the crack tip will exceed the grain size should be considered as a criterion of the small-to-long crack transition. Under high-cycle fatigue conditions physically small fatigue crack growth will be divided into two phases of growth: the first phase is when the crack propagates along the slip planes of individual grains, and the second one is when the crack changes the mechanism of growth and propagates in the plane perpendicular to the loading direction. The model validity has been tested using the experimental data on the growth of the long cracks in specimens of titanium alloy VT3-1 in seven microstructural states and the small cracks in specimens of titanium alloy Ti–6Al–4V and aluminum alloy 2024-T3. Good agreement between the calculated and experimental results is obtained.     

The effect of bi-modal and lamellar microstructures of Ti-6Al-4V on the behaviour of fatigue cracks emanating from edge-notches

This paper is aimed at evaluating the influence of bi‐modal and lamellar microstructures on the behaviour of small cracks emanating from notches in α+β titanium Ti‐6Al‐4V alloy. Pulsating four point bending tests were performed at a nominal stress ratio of 0.1 and a frequency of 15 Hz on double‐edge‐notched specimens. The conditions of initiation and early propagation of fatigue cracks were investigated at two relatively high nominal stress levels corresponding to 88 and 58% of the 0.2% material yield stress. Crack closure effects were measured by an extensometric technique and discussed. Variations in crack aspect ratio were determined and considered in the ΔK calculation. Corresponding results were discussed by considering the effect of the yielded region at the notch tip calculated by elastic–plastic finite element modelling of the fatigue tests. The importance of the bi‐modal and lamellar microstructures on the material damage was highlighted and correlated to the observed oscillations in the crack growth rate. The crack growth rate data obtained were compared with those measured using standard C(T) specimens (long crack).     

Fractographic and microstructural analysis of fatigue crack growth in a Ti-6Al-4V fan disc forging

The constant amplitude fatigue crack growth behaviour of a conventionally (+β) solution treated and aged Ti-6Al-4V fan disc forging was examined by fractographic and microstructural analysis. The crack growth process was complex with many interrelated fracture features. A transition in the fatigue crack growth curve correlated with a change from structure-sensitive to continuum-mode crack growth, primarily in the transformed and aged β grains, and a decrease in fracture surface roughness. The transition was probably caused by the cyclic plastic zone size becoming equal to and exceeding the average platelet packet size. The significance of such transitions for prediction of fatigue crack growth and service failure analysis is discussed.     

Fatigue crack growth resistance of 7075 Al alloy after equal channel angular pressing

This work presents experimental results on effects of severe plastic deformation (SPD) and subsequent natural ageing on tensile mechanical properties and fatigue crack growth resistance of fine‐grained 7075 Al alloy. The alloy was subjected to equal channel angular pressing (ECAP) after solution treatment. Fatigue crack propagation tests were conducted in room condition, at load ratio R = 0.1 and different load ranges on small disk shaped compact tension specimens. Fatigue fracture surface is also investigated using scanning electron microscopy observations and showed more ductile fatigue crack growth in the unECAPed specimen. Despite the increased tensile strength after ECAP, the ductility that controls low‐cycle fatigue behaviour has decreased. It is found that ECAP has resulted in a remarkable change in Paris regime parameters and a significant increase in fatigue crack growth rate. The decrease in fatigue crack growth resistance and ΔK_c after ECAP can be attributed to the decrease in alloy's ductility.