玻璃铝基复合材料高温压缩流变行为研究

利用Cleeble－1500对玻璃铝基复合材料在温度为573—723K、应变速率为0．01s^-1～10s^-1的条件下进行高温压缩变形行为的研究。结果表明，应变速率和变形温度变化强烈影响复合材料的流变应力，流变应力随变形速率的提高而增大，随变形温度的升高而降低；玻璃铝基复合材料高温塑性变形时的流变行为可用Zener·Hollomon参数的双曲正弦函数来描述。     

铍中铁铝杂质对铍材性能的影响

综述了铍中不同存在形式的铁铝杂质对铍材性能的影响,指出通过合适的时效热处理使铁、铝结合生成AlFeBe4物可改善铍材性能,探明了适宜的铁／铝比是生成AlFeBe4化合物的必要条件,并通过选取铍珠或控制粉末酸处理浓度,能制备出符合此铁／铝比要求的原料。     

玻璃铝基复合材料高温压缩变形行为研究

利用Gleeble-1500对玻璃铝基复合材料在温度为573～723K、应变速率为0．01s^-1～10s^-1的条件下进行高温压缩变形行为的研究。结果表明：应变速率和变形温度的变化强烈影响复合材料的流变应力,流变应力随变形速率的提高而增大,随变形温度的升高而降低;玻璃铝基复合材料高温塑性变形时的流变行为可用Zener-Hollomon参数的双曲正弦函数来描述。     

铍中铁铝杂质对铍材性能的影响

综述了铍中不同存在形式的铁、铝杂质对铍材性能的影响。指出,通过合适的时效热处理,使铍中的铁、铝结合生成ＡｌＦｅＢｅ４化合物,可改善铍材性能。分析并阐明了适宜的Ｆｅ／Ａｌ比为生成ＡｌＦｅＢｅ４化合物的必要条件,并了通过选取铍珠或控制粉末酸处理浓度,制备符剑此Ｆｅ／Ａｌ比要求的铍材原料的方法。     

一种新型Al-Cu-Li系合金的热压缩流变应力

采用Gleeble-1500热模拟机高温等温压缩试验,研究了一种新型Al-Cu-Li系合金在应变速率为0.01～10s^-1、变形温度为3130～500℃条件下的流变应力特征,结果表明：流变应力随变形温度的升高而降低,随变形速率的提高而增大;采用Z参数的双曲正弦函数描述该合金高温变形的峰值流变应力,获得了峰值流变应力解析式,其热变形激活能为239.02kJ·mol^-1.     

新型Al-Zn-Mg-Cu合金热变形流变应力特征

采用Gleeble-1500热模拟机进行热压缩变形实验,研究了一种新型Al-7.5Zn-1.6Mg-1.4Cu-0.12Zr合金在变形温度为380-460℃、应变速率为0.001～0.1 s-1条件下的流变应力特征,并利用TEM分析了合金在不同变形条件下的组织形貌特征.结果表明,应变速率和变形温度对合金流变应力的大小有显著影响,流变应力随变形温度的升高而降低,随应变速率的提高而增大;合金平均亚晶尺寸随温度补偿应变速率Zener-Hollomon参数的升高而减小.可用Zener-Hollomon咖参数描述该Al-Zn-Mg-Cu合金热变形时的流变应力行为.     

钛酸铝对镁阿隆复合材料性能的影响

将钛酸铝作为弥散相加到镁阿隆基材料中，并研究其组成和加入量对复合材料性能的影响。结果表明：钛酸铝能显著的提高复合材料的热态强度和热震稳定性，合理设计钛酸铝的加入量可以获得性能优化的复合材料。     

纯钼高温塑性变形及流变应力行为

采用MMS-300热模拟实验机研究纯钼在变形温度为900~1 300℃和应变速率为0.004~1 s-1条件下的高温塑性变形行为。分析了纯钼流变应力与应变速率、变形温度之间的关系,计算了纯钼高温塑性变形时的变形激活能。研究结果表明:纯钼在热变形过程中流变应力随应变速率的增加而增加,随温度的升高而降低,且其高温塑性变形行为可以用Zener-Hollomon参数的流变应力方程进行描述。该纯钼在实验条件范围内发生了明显的动态回复与动态再结晶。     

用蠕变方程建立高强微合金钢的流变应力预测模型

利用Gleeble 2000热模拟试验机对一种屈服强度为700MPa级的微合金钢的热变形行为进行了试验研究。分析了不同变形条件下的流变应力与应变的关系，并根据Roberts提出的用蠕变方程预测不同应变对应的流变应力的方法，用扩展的蠕变方程建立了试验钢的流变应力模型。用建立的模型预测了不同变形条件下的流变应力，预测结果与试验结果基本吻合。     

5083铝合金高温变形的流变应力

在Oleeble-1500热模拟机上,对5083铝合金进行高温等温压缩热模拟,分析了流变应力与应变速率、变形温度之间的关系和高温变形的内在机理,同时血对合金元素对流变应力的影响进行了分析。结果表明：在应变速率为0．01s^-1、0．1s^-1、1s^-1（400℃、450℃）和0．01s^-1（350℃）,其流变应力出现明显的峰值应力,表现出连续动态冉结品特征;在0．1s^-1、1s^-1（350℃）,表现为稳态流变,为动态回复。采用双曲正弦形式的Arrhenius关系来描述5083铝合金高温变形时的流变应力,获得5083的材料常数A、α、n和Q分别为0．06918s^-1、0．01002MPa^-1、3．2819和149．67kJ／mol。在不同的应变率比值下计算应变率敏感（SRS）系数（m=dlnσ／dlnε）,发现随着温度升高,应变增大,m值增大。     

Effect of magnesium on the aging behavior of Al-Zn-Mg-Cu/Al2O3 metal matrix composites

The effect of magnesium content on the aging behavior of Al-Zn-Mg-Cu alloy reinforced with alumina (A1₂O₃) was studied by using the differential scanning calorimetry (DSC) technique and hardness measurement. The magnesium contents were studied in the range from 1.23 to 2.97 wt pct. The addition of magnesium was found to increase the coherent Guinier-Preston (GP) zones in com-posites. The apparent formation enthalpy of GP zones of composites (0.1V _f) was 0.932 cal/g for 1.23 wt pct magnesium content and 1.375 cal/g for 2.97 wt pct magnesium content. The precipitation time to achieve the maximum hardness in the composites depends on the magnesium content. The time changed from 12 to 48 hours as the magnesium content increased from 1.23 to 2.97 wt pct. Both Vickers microhardness and Rockwell hardness increased with increasing magnesium content. The maximum hardness occurred in the composites that contained maximum amounts of GP zones and η′ precipitates. However, the microhardness of the composites was always lower than that of monolithic alloys due to the alumina fibers which caused the suppression of GP zones and η′ for-mation in the composites.     

Effect of volume fraction of SiC p reinforcement on the processing maps for 2124 Al matrix composites

The hot working characteristics of 2124 Al alloy matrix composites reinforced with 0, 5, 10, 15, and 20 vol pct of SiC particulate, produced by the powder metallurgy route, were studied using processing maps. The maps based on the dynamic materials model were generated from the flow stress data obtained from hot compression tests, carried out at strain rates ranging from 0.001 to 10 s⁻¹ and temperatures ranging from 300°C to 525°C. All the compositions studied exhibited domains of dynamic recrystallization (DRX) and superplasticity. Flow instabilities were found at higher strain rates and lower temperatures. The composite with 10 vol pct SiC showed a tendency for abnormal grain growth at lower strains, which manifested itself as a shift in the DRX domain to lower strain rates and the disappearance of the superplasticity domain.     

Solid state sintering and consolidation of Al powders and Al matrix composites

As an attempt to depart from conventional transient liquid phase sintering practice, solid state vacuum sintering was studied in loose powder and in hot quasi-isostatically forged samples composed of commercial inert gas atomized (CIGA) or high purity Al powder. The high purity Al powder was generated by a gas atomization reaction synthesis (GARS) technique that results in spherical powder with a far thinner surface oxide. After vacuum sintering at 525 °C for up to 100 h, SEM results showed that the GARS Al powder achieved significantly advanced sintering stages, compared to the CIGA Al powder. Tensile results from the forged samples also showed that although its ultimate tensile strength is lower, 95 vs. 147 MPa, the ductility of the GARS pure Al sample is higher than the CIGA Al sample. Forging also consolidated a model powder-based composite system composed of an Al matrix reinforced with quasi-crystalline Al–Cu–Fe powders, where the same powder synthesis methods were compared. Auger surface analysis detected evidence of increased matrix/reinforcement interfacial bonding in the composite sample made from GARS powder by alloy interdiffusion layer measurements, consistent with earlier tensile property measurements. The overall results indicated the significant potential of using Al powders produced with a thin, high purity surface oxide for simplifying current Al powder consolidation processing methods.     

Interface characterization of fiber-reinforced Ni3Al matrix composites

The interfacial reaction characteristics of SCS-6, Sigma, and B₄C/B fibers with nickel aluminide (Ni₃Al) matrix have been investigated between 780°C to 980°C for times ranging from 1 to 100 hours. The microstructure and elemental compositions across the reaction zone have been analyzed quantitatively using microscopy and electron probe microanalyses, respectively. The results show that Ni₃Al reacts extensively with SCS-6, Sigma, and B₄C/B fibers to form complex reaction products, and Ni is the dominant diffusing species controlling the extent of reaction. In the SiC/Ni₃Al composite, the C-rich layer on the SiC surface can slow down but cannot stop the inward diffusion of Ni into SiC fiber. When the C-rich layer is depleted, a rapid increase in reaction zone thickness occurs. Diffusion barrier coating on the fibers is required to minimize the interfacial reactions.     

The effect of matrix microstructure on the tensile and fatigue behavior of SiC particle-reinforced 2080 Al matrix composites

The effect of matrix microstructure on the stress-controlled fatigue behavior of a 2080 Al alloy reinforced with 30 pct SiC particles was investigated. A thermomechanical heat treatment (T8) produced a fine and homogeneous distribution of S′ precipitates, while a thermal heat treatment (T6) resulted in coarser and inhomogeneously distributed S′ precipitates. The cyclic and monotonic strength, as well as the cyclic stress-strain response, were found to be significantly affected by the microstructure of the matrix. Because of the finer and more-closely spaced precipitates, the composite given the T8 treatment exhibited higher yield strengths than the T6 materials. Despite its lower yield strength, the T6 matrix composite exhibited higher fatigue resistance than the T8 matrix composite. The cyclic deformation behavior of the composites is compared to monotonic deformation behavior and is explained in terms of microstructural instabilities that cause cyclic hardening or softening. The effect of precipitate spacing and size has a significant effect on fatigue behavior and is discussed. The interactive role of matrix strength and SiC reinforcement on stress within “rogue” inclusions was quantified using a finite-element analysis (FEA) unit-cell model.     

Damping behavior of 6061Al/Gr metal matrix composites

The damping behavior of graphite particulate-reinforced 6061A1 alloy metal matrix composites (MMCs) processed by spray atomization and codeposition is studied. Four spray deposition experiments are made, yielding materials with graphite volume fractions of 0, 0.05, 0.07, and 0.10. A dynamic mechanical thermal analyzer is used to measure the damping capacity and elastic modulus at 0.1, 1, and 10 Hz over the temperature range of 30 °C to 250 °C. The damping capacity of the materials is shown to increase with increasing volume fraction of graphite. Hot extrusion of the spray-deposited MMCs is shown to further increase the damping capacity. The elastic moduli of the spray-deposited MMCs are reduced with the addition of graphite but are improved by hot extrusion. At low temperatures (below 150 °C), the high damping capacity of the MMCs is attributed primarily to thermal expansion mismatch-induced dislocations and the high intrinsic damping of graphite. At high temperatures (above approximately 200 °C), the damping capacity is attributed to Al/graphite interface viscosity, preferred orientation of the graphite, and the presence of dislocations.     

SiC和Si混合颗粒增强铝基复合材料的研究现状

SiC颗粒增强含Si铝基复合材料在制备过程中由于Si颗粒的析出,使其成为SiC和Si混合颗粒增强铝基复合材料。SiC和Si混合颗粒增强铝基复合材料具有比强度和比刚度高、耐磨性和耐疲劳性好、尺寸稳定性强、轻质等性能,广泛应用于航空、航天、电子电器等工业领域。主要介绍了SiC和Si混合颗粒增强铝基复合材料的研究现状及几种制备工艺,分析了其显微组织中存在的缺陷及复合材料性能的影响因素;展望了SiC和Si混合颗粒增强铝基复合材料的应用前景。