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1.
Single-pulse and double-pulse optical emission spectroscopy （OES） analyses were carried out in air by using ultrashort laser pulses at atmospheric pressure. The aim of this work is to use spectroscopic methods to analyze the early phase of laser-induced plasma after the femtosecond laser pulse. The temporal behavior of emission spectra of air plasma has been characterized. In comparison with the single-pulse scheme, the plasma emission obtained in the double-pulse scheme presents a more intense continuum along with several additional ionic lines. As only one line is available in the single-pulse scheme, the plasma temperature measurements were performed using only the relative line-to-continuum intensity ratio method, whereas the relative line-to-line intensity ratio method and the relative line-to-continuum intensity ratio method were used simultaneously to estimate the electron temperature in the double-pulse scheme. The results reveal that the temperature values obtained by the two methods in the double-pulse scheme agree. Moreover, this shows that the relative line-to-continuum intensity ratio method is suitable for early phase of laser-induced plasma diagnostics. The electron number density was estimated using the Stark broadening method. In the early phase of laser-induced plasma, the temporal evolution of the electron number density exhibits a power law decrease with delay time. 相似文献
2.
In this work,we studied the effects of the discharge current,gas flow rate and vessel pressure on the electron temperature and density of Ar plasma by Langmuir probe measurement.The argon plasma was created by a one-cathode arc source.The experimental results show that with increasing discharge current and gas flow rate,the electron temperature and density increase.It is found that when the discharge current is 70 A,90 A and HO A at an argon flow rate of2000 seem,the electron densities at about 0.186 m distance from the nozzle are 13.00×10~(18) m~(-3),14.04×10~(18) m~(-3) and 15.62×10~(18) m~(-3),and the electron temperatures are 0.38 eV,0.58 eV and0.71 eV,respectively.The positive I-V characteristic is explained. 相似文献
3.
Investigation of E–H mode transition in magnetic-pole-enhanced inductively coupled neon–argon mixture plasma 
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下载免费PDF全文 In this paper, E–H mode transition in magnetic-pole-enhanced inductively coupled neon–argon mixture plasma is investigated in terms of fundamental plasma parameters as a function of argon fraction(0%–100%), operating pressure(1 Pa, 5 Pa, 10 Pa and 50 Pa), and radio frequency(RF) power(5–100 W). An RF compensated Langmuir probe and optical emission spectroscopy are used for the diagnostics of the plasma under study. Owing to the lower ionization potential and higher collision cross-section of argon, when its fraction in the discharge is increased, the mode transition occurs at lower RF power; i.e. for 0% argon and1 Pa pressure, the threshold power of the E–H mode transition is 65 W, which reduces to 20 W when the argon fraction is increased. The electron density increases with the argon fraction at afixed pressure, whereas the temperature decreases with the argon fraction. The relaxation length of the low-energy electrons increases, and decreases for high-energy electrons with argon fraction, due to the Ramseur effect. However, the relaxation length of both groups of electrons decreases with pressure due to reduction in the mean free path. The electron energy probability function(EEPF) profiles are non-Maxwellian in E-mode, attributable to the nonlocal electron kinetics in this mode; however, they evolve to Maxwellian distribution when the discharge transforms to H-mode due to lower electron temperature and higher electron density in H-mode. The tail of the measured EEPFs is found to deplete in both E-and H-modes when the argon fraction in the discharge is increased, because argon has a much lower excitation potential(11.5 eV) than neon(16.6 eV). 相似文献
4.
An improved surface wave plasma source equipped with a cylindrical quartz rod has been developed, which has great potential in processing inner wall of cylindrical workpieces. A cylindrical quartz rod not only excites the plasma around the rod, but also guides surface wave plasma along the rod. The distributions of plasma density and plasma temperature under different incident microwave powers and pressures are diagnosed by a Langmuir probe. The electron density near the rod is around the order of 10^11cm^-3. When the incident power is 450 W, the length of surface wave plasma column can reach up to 420 mm at 20 Pa. 相似文献
5.
采用光谱仪测量了等离子体点火器出口射流的发射光谱,利用玻尔兹曼曲线斜率法计算了射流的电子温度,并通过电离平衡方程计算了射流气体温度,获得点火器出口射流长度、射流速度、电子温度和射流温度随弧电流及进口氩气流量的变化规律。并分析了航空等离子体电弧射流中是否可使用电子温度来代替射流气体温度。实验表明：弧电流随着进口氩气流量的增大而减小;出口射流长度和速度随弧电流的增大而增大,随进口氩气流量的增大先增大后减小;出口电子温度、电子密度和射流温度随弧电流的增大而升高,随氩气流量的增大而降低。 相似文献
6.
We studied the spatial evolution of the Fe-Ni plasma generated by the fundamental (1064 nm) and second (532 nm) harmonics of a Q-switched Nd: YAG laser. The experimentally observed line profiles of the neutral iron (Fe I) have been used to extract the plasma temperature (T e ) using the Boltzmann plot method, whereas the electron number density (N e ) has been deter- mined from the Stark broadening. In addition, we studied the spatial behavior of T e and N e with the variation of laser energy for iron plasma by placing the target material (iron-nickel alloy) in air at atmospheric pressure for both modes of the Nd: YAG laser. 相似文献
7.
Laser-induced steel plasma is generated by focusing a Q-switched Nd:YAG visible laser(532 nm wavelength) with an irradiance of 1 x 109 W/cm2 on a steel sample in air at atmospheric pressure.An Echelle spectrograph coupled with a gateable intensified charge-coupled detector is used to record the plasma emissions.Using time-resolved spectroscopic measurements of the plasma emissions,the temperature and electron number density of the steel plasma are determined for many times of the detector delay.The validity of the assumption by the spectroscopic methods that the laser-induced plasma(LIP) is optically thin and is also in local thermodynamic equilibrium(LTE) has been evaluated for many delay times.From the temporal evolution of the intensity ratio of two Fe I lines and matching it with its theoretical value,the delay times where the plasma is optically thin and is also in LTE are found to be 800 ns,900 ns and 1000 ns. 相似文献
8.
In order to deposit good films, we need to study the uniformity of plasma density and the plasma density under different gas pressures and powers. The plasma density was diagnosed by a Langmuir probe. The optical emission spectroscopy （OES） of CH4 and H2 discharge was obtained with raster spectroscopy, with characteristic peaks of H and CH achieved. Diamond-like carbon films were achieved based on the study of plasma density and OES and characterized by atomic force microscope （AFM）, X-ray diffraction instrument （XRD）, Raman spectroscope and profiler. 相似文献
9.
Two techniques are applied to diagnose characteristic parameters of plasma created by hypervelocity impact, such as electron temperature and electron density. The first technique is a sweep Langmuir probe （SLP）, which is a new apparatus based on a dual channel circuit that can compensate for stray capacitance and obtain a good synchronicity, so that electrostatic turbulence with a good temporal resolution can be acquired. The second technique is a triple Langmuir probe （TLP）, which is an electrostatic triple Langmuir probe diagnostic system, in which no voltage and frequency sweep is required. This technique allows to measure electron temperature, electron density as a function of time. Moreover, the triple Langmuir probe diagnostic system allows the direct display of electron temperature and semidirect display of electron density by an appropriate display system, the system permits us to eliminate almost all data processing procedures. SLP and TLP were applied to obtain fluctuations of the characteristic parameters of plasma generated by hypervelocity impact. As an example of their application to time-dependent plasma measure- ment, the electron temperature and electron density of plasmas were acquired in hypervelocity impact experiments. Characteristic parameters of plasma generated by hypervelocity impact were compared by the two kinds of diagnostic techniques mentioned above. 相似文献
10.
Zeyu HAO 《等离子体科学和技术》2019,21(7):75401-118
The effects of driving frequency on plasma parameters and electron heating efficiency are studied in cylindrical inductively coupled plasma (ICP) source. Measurements are made in an Ar discharge for driving frequency at 13.56/2 MHz, and pressures of 0.4–1.2 Pa. In 13.56 MHz discharge, higher electron density (ne) and higher electron temperature (Te) are observed in comparison with 2 MHz discharge at 0.6–1.2 Pa. However, slightly higherne andTe are observed in 2 MHz discharge at 0.4 Pa. This observation is explained by enhanced electron heating efficiency due to the resonance between the oscillation of 2 MHz electromagnetic field and electron-neutral collision process at 0.4 Pa. It is also found that the variation ofTe distribution is different in 13.56 and 2 MHz discharge. For ICP at 13.56 MHz, Te shows an edge-high profile at 0.4–1.2 Pa. For 2 MHz discharge,Te remains an edge-high distribution at 0.4–0.8 Pa. However, the distribution pattern involves into a center-high profile at 0.9–1.2 Pa. The spatial profiles ofne remain a center-high shape in both 13.56 and 2 MHz discharges, which indicates the nonlocal kinetics at low pressures. Better uniformity could be achieved by using 2 MHz discharge. The effects of gas pressure on plasma parameters are also examined. An increase in gas pressure necessitates the rise ofne in both 13.56 and 2 MHz discharges. Meanwhile, Te drops when gas pressure increases and shows a flatter distribution at higher pressure. 相似文献
11.
As advanced linear plasma sources, cascaded arc plasma devices have been used to generate steady plasma with high electron density, high particle flux and low electron temperature. To measure electron density and electron temperature of the plasma device accurately, a laser Thomson scattering(LTS) system, which is generally recognized as the most precise plasma diagnostic method, has been established in our lab in Dalian University of Technology. The electron density has been measured successfully in the region of 4.5?×?10(19)m~(-3) to7.1?×?10~(20)m~(-3) and electron temperature in the region of 0.18 eV to 0.58 eV. For comparison,an optical emission spectroscopy(OES) system was established as well. The results showed that the electron excitation temperature(configuration temperature) measured by OES is significantly higher than the electron temperature(kinetic electron temperature) measured by LTS by up to 40% in the given discharge conditions. The results indicate that the cascaded arc plasma is recombining plasma and it is not in local thermodynamic equilibrium(LTE). This leads to significant error using OES when characterizing the electron temperature in a non-LTE plasma. 相似文献
12.
This work reports spectroscopic studies of uranium containing plasma generated in air and argon environments. The 532 nm Q-switched Nd:YAG laser generates the optical breakdown plasma, which was recorded by a spectrometer and an intensified charge coupled device having a resolution of 25 pm. Neutral and ionized uranium lines in the wavelength range of 385.8–391.9 nm indicate significant width and shift variations during the first few microseconds. Electron temperature and density of the plasma are determined using the Boltzmann plot and the Saha–Boltzmann equation at various time delay. The study reveals the power law decay pattern of electron temperature and density, which changes to exponential decay pattern if large gate- width is used to acquire the signal, due to an averaging effect. 相似文献
13.
Maryam RIAZ;Shazia BASHIR;Asma HAYAT;Zarish NAZ 《等离子体科学和技术》2023,25(3):035508-035508
This study deals with the investigation of Nd: YAG laser-assisted ablation and plasma formation of Ti at irradiance of 0.85 GW cm-2 under Ar and Ne environment at various pressures ranging from 10–120 Torr. Laser-induced breakdown spectroscopy is used to evaluate plasma parameters, whereas quartz crystal microbalance is used for ablation yield measurements. The crater depth is evaluated by optical microscopy. The surface features are explored by scanning electron microscope (SEM) analysis and the micro-hardness is measured by a Vickers hardness tester. It is observed that the plasma parameters are higher in Ar than in Ne, and are strongly correlated with the ablation yield, ablation depth, surface features and hardness of laser-ablated Ti. These parameters increase with increasing the pressure of environmental gases, attain their maxima at 40 Torr for Ar and at 60 Torr for Ne. Afterwards, they show a decreasing trend up till a maximum pressure of 120 Torr. The maximum value of the electron temperature (T e) is 5480 K, number density (n e) is
14.
《等离子体科学和技术》2016,18(9):902-906
The spectral emission and plasma parameters of SnO_2 plasmas have been investigated.A planar ceramic SnO_2 target was irradiated by a CO2 laser with a full width at half maximum of 80 ns.The temporal behavior of the specific emission lines from the SnO_2 plasma was characterized.The intensities of Sn I and Sn II lines first increased,and then decreased with the delay time.The results also showed a faster decay of Sn I atoms than that of Sn II ionic species.The temporal evolutions of the SnO_2 plasma parameters(electron temperature and density) were deduced.The measured temperature and density of SnO_2 plasma are 4.38 eV to0.5 eV and 11.38×10~(17) cm~(-3) to 1.1×10~(17) cm~(-3),for delay times between 0.1 μs and 2.2 μs.We also investigated the effect of the laser pulse energy on SnO_2 plasma. 相似文献
15.
Determination of the negative ion number density of O~-_2and O~-in a DC discharge of oxygen plasma was made employing Langmuir probe in conjunction with eclipse laser photodetachment technique.The temporal evolution of the extra electrons resulting from the photodetachment of O~-_2and O~-were used to evaluate the negative ion number density.The ratio of O~-_2number density to O~-varied from 0.03 to 0.22.Number density of both O~-_2and O~-increased with increasing power and decreased as the pressure was increased.Electron number density was evaluated from the electron energy distribution function(EEDF)using the I–V recorded characteristic curves.Electron temperature between 2 and 2.7 eV were obtained.Influence of the O_2(a~1Δ_g)metastable state is discussed. 相似文献
16.
Filtered cathodic vacuum arc (FCVA) deposition is regarded as an important technique for the synthesis of tetrahedral amorphous carbon (ta-C) films due to its high ionization rate, high deposition rate and effective filtration of macroparticles. Probing the plasma characteristics of arc discharge contributes to understanding the deposition mechanism of ta-C films on a microscopic level. This work focuses on the plasma diagnosis of an FCVA discharge using a Langmuir dual-probe system with a discrete Fourier transform smoothing method. During the ta-C film deposition, the arc current of graphite cathodes and deposition pressure vary from 30 to 90 A and from 0.3 to 0.9 Pa, respectively. The plasma density increases with arc current but decreases with pressure. The carbon plasma density generated by the arc discharge is around the order of 1010 cm−3. The electron temperature varies in the range of 2‒3.5 eV. As the number of cathodic arc sources and the current of the focused magnetic coil increase, the plasma density increases. The ratio of the intensity of the D-Raman peak and G-Raman peak (I D/I G) of the ta-C films increases with increasing plasma density, resulting in a decrease in film hardness. It is indicated that the mechanical properties of ta-C films depend not only on the ion energy but also on the carbon plasma density. 相似文献
17.
A low power atmospheric pressure plasma jet driven by a 24 kHz AC power source and operated with a CH_4/air gas mixture has been investigated by optical emission spectrometer.The plasma parameters including the electron excitation temperature,vibrational temperature and rotational temperature of the plasma jet at different discharge powers are diagnosed based on the assumption that the kinetic energy of the species obeys the Boltzmann distribution.The electron density at different power is also investigated by H_β Stark broadening.The results show that the plasma source works under non-equilibrium conditions.It is also found that the vibrational temperature and rotational temperature increase with discharge power,whereas the electron excitation temperature seems to have a downward trend.The electron density increases from 0.8×10~(21) m~(-3) to 1.1×10~(21)m~(-3) when the discharge power increases from 53 W to 94 W. 相似文献
18.
Due to the growing interest in studying the compression and disruption of the plasma filament in magnetic fusion devices and Z-pinches, this work may be important for new developments in the field of controlled thermonuclear fusion. Recently, on a coaxial plasma accelerator, we managed to obtain the relatively long-lived (∼300 μs) plasma filaments with its self-magnetic field. This was achieved after modification of the experimental setup by using high-capacitive and low-inductive energy storage capacitor banks, as well as electrical cables with low reactive impedance. Furthermore, we were able to avoid the reverse reflection of the plasma flux from the end of the plasma accelerator by installing a special plasma-absorbing target. Thus, these constructive changes of the experimental setup allowed us to investigate the physical properties of the plasma filament by using the comprehensive diagnostics including Rogowski coil, magnetic probes, and Faraday cup. As a result, such important plasma parameters as density of ions and temperature of electrons in plasma flux, time dependent plasma filament's azimuthal magnetic field were measured in discharge gap and at a distance of 23.5 cm from the tip of the cathode. In addition, the current oscillograms and I–V characteristics of the plasma accelerator were obtained. In the experiments, we also observed the charge separation during the acceleration of plasma flow via oscillograms of electron and ion beam currents. 相似文献
19.
The plasma shielding effect is one of the major weaknesses of laser-induced breakdown spectroscopy(LIBS) as it causes non-linearity in signal strength. Although LIBS is typically carried out in constant laser energy, this non-linearity causes a reduction in sensitivity. In this work, we systematically examine laser-induced plasma, formed by two different excitation source modes, i.e. single pulse(SP)-excitation and single-beam-splitting double-pulse(SBSDP)-excitation over Zr-2.5% Nb alloy. The two most important plasma parameters influencing the emission line intensity, plasma temperature(T_e) and electron density(N_e) were studied and compared for both modes of laser excitation. Comparison of the results conclusively demonstrates that due to the splitting of the laser energy in the SBS-DP mode, the plasma shielding effect is significantly reduced. The reduced plasma shielding translates to an increased laser–sample coupling under SBS-DP mode. Temporal imaging of the total intensity of the laserinduced plasma in both excitation modes was also studied. The study shows how the plasma shielding effect can be reduced to improve the analytical quality of the LIBS methodology. 相似文献
20.
Yang YU 《等离子体科学和技术》2020,22(1):15502-015502
The spectral characteristic of laser-induced plasma in soil was studied in this work, laser-induced breakdown spectroscopy was used to analyze the spectral characteristic of plasma under the condition of different time delays and irradiances. Moreover, the time evolution characteristics of plasma temperature and electron density were discussed. Within the time delay range of 0-5 μs,the spectral intensity of the characteristic lines of Si I: 288.158 nm, Ti I: 336.126 nm, Al I:394.400 nm and Fe I: 438.354 nm of the four main elements in two kinds of national standard soil decayed exponentially with time. The average lifetime of the spectral lines was nearly 1.56 μs. Under the condition of different time delays, the spectral intensity of Pb I: 405.78 nm in soil increased linearly with laser energy. However, the slope between the spectral intensity and laser energy decreased exponentially with the increase in time delay, from 4.91 to 0.99 during 0-5 μs. The plasma temperature was calculated by the Boltzmann plot method and the electron density was obtained by inversion of the full width at half maximum of the spectrum. The plasma temperature decreased from 8900 K to 7800 K and the electron density decreased from 1.5 × 10~(17) cm~(-3) to 7.8 × 10~(16) cm~(-3) in the range of 0-5 μs. 相似文献