Interfacial bond strengths of amalgam bonded to amalgam and resin composite bonded to amalgam

A preparative method for the preparation of large peptides is described. An advantageous theoretical weight of peptide/weight of starting resin ratio (tPw/Rw) of about 0.3 was successfully experimented. The esterification of the first amino acid was realized with a racemization of less than 1%. The study of the coupling conditions led to the use of a diluted acylating mixture that allowed a 56% consumption of the amino acid derivatives (percentage use of amino acids) introduced in the synthesis. The cost analysis of the synthesis showed that the recovery of the amino acid derivatives was not worthwhile.     

Shear bond strength of amalgam adhesives to dentin

Recent studies have suggested that failure of pentamidine prophylaxis against Pneumocystis carinii pneumonia (PCP) may be due to reduced deposition of pentamidine in the upper lobes. In this study, we performed bronchoalveolar lavage from the apical segment of the upper lobe and the middle lobe in 51 HIV-positive patients, all of whom were receiving prophylaxis with aerosolized pentamidine, who had presented with acute respiratory symptoms. Lavage fluid from each lobe was assayed for pentamidine using high-performance liquid chromatography (HPLC). The number of clusters of P carinii were counted after staining with a Wright-Giemsa stain. The patients were subclassified as PCP-positive (32 patients) and PCP-negative (19 patients) on the basis of the presence/absence of P carinii clusters in their BAL fluid. The concentration of pentamidine in the upper lobe compared with the middle lobe was no different (using paired Student's t tests) for either PCP-positive patients or PCP-negative patients. In comparing the positive with the negative subjects, using unpaired Student's t test, there was no difference in the concentration of pentamidine in the upper lobe or the middle lobe. For PCP-positive patients, the numbers of P carinii clusters were on average higher in the upper lobes (mean +/- SD: upper = 14.9 +/- 16.6, middle 7.5 +/- 10.8, p = 0.013, paired Student's t test), but there was no correlation between lobar P carinii cluster counts and pentamidine levels. We conclude that the absence of a relationship between cluster count and pentamidine level, the similarity in regional pentamidine levels between upper and middle lobes, as well as the similarity in pentamidine levels between the PCP-positive and PCP-negative groups indicate that the regional dose of pentamidine is not the determining factor as to whether aerosolized pentamidine prophylaxis will succeed or fail.     

Shear bond strength of amalgam and gallium alloys to dentine

The purpose of this in vitro investigation was to determine the shear bond strength of admixed (Dispersalloy), irregular (Oralloy) and spherical (Lojic) amalgams, as well as an admixed gallium alloy (Galloy) to superficial, buccal, human dentine surfaces, using the Scotchbond Multi-Purpose Plus system. The bonds were stressed to failure in an Instron testing machine after 48 hours, and the following values (MPa) were obtained: Admixed = 7.74 +/- 0.7; Irregular = 9.47 +/- 1.4; Spherical = 9.82 +/- 2.4; Galloy = 11.03 +/- 2.5. Data were statistically analysed and fracture sites examined in a scanning electron microscope. Galloy demonstrated a statistical significant higher shear bond strength than to the other types of amalgams (p < 0.01).     

Early compressive strength and phase-formation of dental amalgam

The tunic cuticle of Botrylloides simodensis, a colonial ascidian, is an electrondense sheet overlaying the tunic in which zooids are embedded. When the margins of colonies were cut off and the colonies were incubated in running seawater, the tunic cuticle regenerated at the cut surface of the tunic matrix by the following process: 1) Electron-dense fibers appeared at the cut surface within a few minutes. 2) Fiber formation proceeded during the next several hours, and the number of fibers greatly increased. 3) In 12 to 24 hours, the fibers aggregated and formed a continuous layer, which was the newly regenerated cuticle. 4) Minute protrusions appeared in the new cuticle after 3 to 5 days. Fiber formation occurred even in fragments of colonial margins that were incubated in a bottle of seawater. It was inhibited under some experimental conditions including low pH and the presence of some proteases or protease inhibitors.     

Influences of matrix ductility,interfacial bonding strength,and fiber volume fraction on tensile strength of unidirectional metal matrix composite

A trial to predict the influences of ductility of matrix, interfacial bonding strength, and volume fraction of fiber on the tensile strength of unidirectional metal matrix composites was attempted by means of a Monte Carlo computer simulation method. The main results are summarized as follows. (1) The strength of strongly bonded composites increased with increasing ductility of matrix and then remained nearly constant. (2) When the matrix was ductile, the strength of composite increased with increasing interfacial bonding strength and then remained nearly constant. When the matrix was not ductile, the strength increased but then decreased with interfacial bonding strength. In this case, there was an optimum bonding strength, for which the strength of composite was highest. (3) Concerning the strength of composite as a function of volume fraction of fiber, there arose the case where it is approximately described by the rule of mixtures and also the case where it is not described by this rule, depending on the ductility of matrix, interfacial bonding strength, and scatter of strength of fiber.     

Galactans and cellulose in flax fibres: putative contributions to the tensile strength

The proton spin-spin relaxation time, T2, measured from solid-state NMR, indicates a greater rigidity for cellulose than for the adhesive matrix between the microfibrils of flax ultimate fibres. Cytochemical and biochemical analyses allow the identification of: (1) EDTA-soluble RG I-polymers in the primary walls and cell junctions of fibres; (2) long 1 --> 4-beta-D-galactan chains between primary and secondary wall layers; and (3) arabinogalactan-proteins throughout the secondary walls. These polymers in the adhesive matrix between microfibrils and/or cellulose layers ensure that cracks propagate along the matrix rather than across the fibres and play an important role in allowing flax fibres to approach the tensile strength of advanced synthetic fibres like carbon and Kevlar.     

Bond strength and interfacial morphology of adhesives to primary teeth dentin

PURPOSES: To evaluate (1) the shear bond strength to the dentin of primary teeth and failure site of hydrophilic dentin bonding agents, (2) the interfacial micromorphology of these adhesives on primary teeth. MATERIALS AND METHODS: Seventy-six primary noncarious molars stored in distilled water were obtained. The teeth were cleaned with pumice and a rubber cup. The mesio-buccal surface of the teeth was ground flat with hand pressure with a series of SiC paper ending with the 600 grit to provide a uniform surface on superficial dentin to which the adhesives and resin composite could be applied. After preparing the dentin surface, the teeth were stored in distilled water for 48 hours. They were then rinsed and dried with compressed air and divided at random into four groups of 16 specimens each: Group 1: Dentastic; Group 2: One-Step; Group 3: Prime & Bond 2.0; Group 4: Compoglass SCA. Z100 resin was used in all groups. All specimens were thermocycled (500x) and sheared in an Instron machine. After shear testing, the debonding sites of all samples were examined with a stereomicroscope and selected samples were also examined with the scanning electron microscope. Three additional samples per group were used to evaluate the resin adaptation to dentin. RESULTS: The results in MPa were: Dentastic 19.62 (4.67); One-Step 11.24 (3.67), Prime & Bond 22.38 (6.47), Compoglass SCA 18.88 (4.04). ANOVA (P < 0.0001) revealed that there was a significant difference between the groups. The Student-Newman-Keuls test (P < 0.05) showed no statistically significant difference between Dentastic, Prime & Bond and Compoglass SCA. However, these three groups were statistically significantly higher than One Step. In the Dentastic group, 14 of 16 samples revealed resin cohesive failure (resin fracture) while two of 16 displayed dentin cohesive failure (dentin fracture). In the One Step group, 15 samples failed at the resin and one sample showed dentin cohesive failure. In the Prime & Bond group, 12 specimens revealed resin cohesive failure while four displayed dentin cohesive failure. In the Compoglass SCA group, 13 samples had resin cohesive failures while three had dentin cohesive failures. All samples revealed an intimate adaptation to the dentin displaying resin tag formation.     

In vitro shear strength of bonded amalgam cores with and without pins

After ileo-pouch-anal anastomosis (IPAA) there is an increased risk of incontinence due to intraoperative damage of the anal sphincter. We present a new concept to identify a potential incontinence prior to the closure of ileostomy by clinical and anal manometrical examinations. In 11 of 121 (9.1%) patients we diagnosed a potential incontinence. By biofeedback training we could achieve in this way a sufficient continence after the closure of ileostomy. After an average of 5.0 +/- 4.3 months of training rest pressures improved from 19.3 +/- 2.1 mmHg to 33.0 +/- 3.5 mmHg and squeeze pressures from 60.5 +/- 27.7 mmHg to 93.5 +/- 17.3 mmHg. Prior to IPAA patients with potential incontinence show significantly reduced rest pressures of 51.0 +/- 18.4 mmHg.     

The effect of dentin primer on the tensile bond strength to human enamel

Four third-generation dentin bonding products (Scotchbond Multi-Purpose, Optibond, All-Bond 2, and Prisma Universal Bond 3) were tested to evaluate their tensile bond strength to enamel. Test enamel specimens were etched, primed, and polymerized according to each manufacturer's directions. Control specimens were treated identically except the primer application was eliminated. The results demonstrated that the dentin primer significantly increased the tensile bond strength of All-Bond 2, significantly decreased the tensile bond strength of Scotchbond Multi-Purpose and Optibond, and had no significant effect for Prisma Universal Bond 3. A one-way analysis of variance was run between the eight groups tested, and three significant subsets were found (P < .05). The subset with the highest mean tensile bond strengths consisted of Prisma Universal Bond 3 primed and nonprimed, All-Bond 2 primed, and Optibond nonprimed.     

Comparative clinical study of amalgam fillings

Two different types of amalgam alloys (Strafill NG2, [Ogussa] and googfill 700 [Ogussa]) were placed into 106 contralateral, homologous molar tooth-pairs of 81 patients. Scoring after two years showed significant difference in case of marginal ditching favouring the non gamma2 alloy. However significant differences were not found in case of other observed failures, such as bulk fracture, surface roughness and secondary caries.     

A computer simulation on tensile strength of surface-Damaged fibers

The strength of surface-damaged fibers was studied by means of a computer simulation experiment based on the Monte-Carlo method using a simple model which assumes that the surface flaws can be regarded as mode I notches on fiber surfaces, the strength of undamaged fibers obeys the Weibull distribution function, and the largest flaw determines the strength of damaged fibers. Normal and exponential distribution functions were taken as the flaw size distribution function. By employing the present simulation method, the effects of average flaw size, coefficient of variation of flaw size, density of flaws, and gage length on average strength and its coefficient of variation were studied. It was found that the surface-damaged fibers can retain their full strength only when the average flaw size is small, the coefficient of variation of flaw size is small, density of flaw size is low, and gage length is short. Otherwise the average strength of damaged fibers was reduced seriously. It was emphasized that the scatter of size of flaws and density of flaws strongly affect the strength of fibers as well as flaw size and gage length.     

高强IF钢的高速应变行为

利用拉伸实验装置研究了高强IF钢在高应变速率下的变形特性。结果表明：高强IF钢是应变速率敏感性材料,在应变速率10-4～103/s的范围内,应变速率对高强IF钢的应变硬化率与屈服强度的影响具有2阶段性。在第一阶段,应变速率较低,应变硬化率与屈服强度对应变速率的敏感性较小;在第二阶段,应变速率较高,随应变速率的增加,应变硬化率迅速降低,屈服强度迅速增加。     

硬质合金复合涂层的结合强度与失效机理

通过4种硬质合金基体和3种TiN/TiCN/Al<,2>O<,3>TiN复合涂层的组合,采用化学气相沉积(CVD)法制备12种涂层顾质合金样品,借助划痕试验机、扫描电镜和能谱仪测定涂层与基体的结合强度,观察划痕的形貌,测定划痕的微区成分.结果表明,基体成分和WC的晶粒度,以及涂层的成分和厚度对涂层与基体的结合强度有明显...     

Structural disorders at the insertion of the supraspinatus tendon. Relation to tensile strength

We examined macroscopically and microscopically 55 cadaver rotator-cuff tendons attached to their humeral heads to determine the distance between the edge of the articular cartilage and the tendon insertion of the supraspinatus (the width of the sulcus) and the score of regressive changes at the sulcus. In 33 specimens we measured the tensile strength. The width of the sulcus was correlated with the score of regressive changes and with the ultimate tensile strength of the supraspinatus tendon. The width of the sulcus correlated positively with the score of regressive changes (r = 0.66, p < 0.0001), but there was a negative correlation between the latter and the ultimate tensile strength (r = -0.81, p = 0.001) and between the width of the sulcus and the ultimate tensile strength (r = -0.74, p = 0.004). We believe that the width of the sulcus is a simple and useful clinical indicator of the integrity and the tensile strength of the supraspinatus tendon.     

Comparing the tensile strength of brackets adhered to laser-etched enamel vs. acid-etched enamel

This study compared the tensile bond strength of brackets adhered to laser-etched enamel with that of brackets adhered to acid-etched enamel. Forty extracted, intact bovine teeth were treated with either 37 percent phosphoric acid for 15 seconds or neodymium:yttrium-aluminumgarnet laser on black-ink-coated enamel. After thermocycling, tensile stress was applied to the bonded specimens at a 0.1 millimeter/minute orosshead speed. A t-test comparison of means showed a significant difference between the laser-etched and acid-etched teeth, with the acid-etched teeth demonstrating significantly more tensile bond strength at a 95 percent level of significance.     

Analysis of tensile properties for a whisker-reinforced metal-matrix composite

A micro-mechanical model is used to analyse the tensile properties of a ductile metal reinforced by short fibres. It is assumed that fibre alignment has been obtained during processing, and the numerical analysis for a representative unit cell also relies on the assumption of a periodic array of fibres. The special unit cell model developed here represents neighbouring fibres shifted relative to one another. Comparison of results for rigid fibres with results accounting for fibre elasticity shows that apart from the initial elastic range the overall stress-strain behaviour is dominated by matrix plasticity. The analyses focus on uniaxial tension in the fibre direction, but also the effect of stress triaxiality is investigated. Quite good agreement is obtained between the model predictions and published experimental results. The sensitivity of the overall stress-strain behaviour to the fibre volume fraction, the fibre length, and fibre spacings is studied by a number of analyses.     

Effects of aging on tensile fatigue strength of bovine dentin

The effects of aging on the tensile fatigue strength of bovine dentin were investigated. Tensile tests and tensile fatigue tests were performed in 37 degrees C water with bovine dentin specimens of two different age groups. The tensile strengths of the young group and the adult group were 74.0 MPa and 72.7 MPa, respectively; there was no significant difference between the young and the adult group. However, the tensile fatigue strength of the adult group, 46.9 MPa, was significantly weaker than that of the young group, 51.0 MPa. There was a obvious difference between the tensile fracture surface and the tensile fatigue fracture surface; a smooth surface of the peritubular dentin and an uneven surface of the intertubular dentin were clearly distinct in the fatigue fracture surface. Plugged dentinal tubules and narrower dentin tubules were commonly observed in the adult group. These morphological changes were suggested to be the reason for the decrease in the tensile fatigue strength with aging.     

Effect of disinfectants on the bond strength of composite to dentin

The article describes ultrasonographic (US), computed tomographic (CT), 99mTc-MIBI and angiographic findings of 16 cases of multiple endocrine neoplasia (MEN) confirmed by operations and pathological examinations. Hyperparathyroidism either was the first manifestation of MEN I or was diagnosed simultaneously with other tumors. Medullary thyroid carcinoma usually developed first or coincided with pheochromocytoma in MEN I. Regular US and CT screening can lead to the detection of new endocrine neoplasia. The authors consider that US and CT are the best imaging methods for MEN.