载银壳聚糖涂布液的制备及涂布纸抑菌性能的研究

以壳聚糖(CS)和AgNO3为原料,以Na BH4为还原剂,制备了载银壳聚糖(Ag-CS)涂布液,进而对纸张涂布,制得涂布纸。利用FT-IR、XRD和SEM分析其结构和形貌,研究了制备工艺对涂布纸抗张指数以及对金黄色葡萄球菌的抑菌性能的影响。结果表明,CS中的-NH2和-OH与Ag+发生配位结合,并使得结晶度下降。CS用量为1%,AgNO3用量为0.2mmol/l,Na BH4用量为0.3mmol/l,CS相对分子质量为500k Da时,涂布纸对金黄色葡萄球菌有很好的抑菌性,同时纸页的抗张指数也得到改善。涂布纸SEM分析表明,载银壳聚糖涂布液在纸页表面形成膜层。     

壳聚糖-淀粉涂布抗菌纸的制备及性能研究

以壳聚糖-淀粉混合物对纸张进行涂布处理,研究制备工艺对涂布纸抗张指数以及对金黄色葡萄球菌抗菌性能的影响。结果表明,涂布液中壳聚糖浓度为15 g/L、淀粉与壳聚糖的浓度之比为1.5∶1.0、乙酸用量为1.5%、pH值为5、壳聚糖相对分子质量为20万时,涂布量为2.02 g/m²条件下制备的涂布纸对金黄色葡萄球菌有很好的抗菌性,同时纸张的抗张指数也得到明显改善。     

壳聚糖/蒙脱土复合涂布液的制备及涂布纸保鲜性能的研究

制备了壳聚糖（C S）/蒙脱土（M MT）复合涂布液,进而对纸张涂布,制得涂布纸。利用涂布纸对圣女果进行包装,测定6d后圣女果的失重率、可滴定酸和Vc含量,考察涂布液制备条件对涂布纸保鲜性能的影响。结果表明,在C S用量1.5%、CS与MMT比例为3∶1、CS相对分子质量20万时,可获得最佳的保鲜性能。对涂布液的X-射线图谱和红外光谱分析表明,CS进入到了MMT的层间。涂布纸SEM图分析表明,CS/MMT复合涂布液在纸张表面形成了膜层。测定不同包装方式下一定时间的圣女果失重率、可滴定酸和Vc含量的变化,通过对比发现,10d后失重率为6.3%,可滴定酸下降24.31%,Vc含量下降11.23%。与对照样相比较,CS/MMT复合涂布纸有利于减少营养物质的流失,从而延长果蔬的常温贮藏期。     

载银壳聚糖涂布液的制备及其涂布纸保鲜性能的研究

以壳聚糖(CS)和AgNO3为原料,以NaBH4为还原剂,制备载银壳聚糖(Ag-CS)涂布液;然后对纸张涂布,制得涂布纸.利用FT-IR、XRD和SEM分析其结构和形貌;利用涂布纸对圣女果进行包装,测定6天后圣女果的失重率、可滴定酸和抗坏血酸(Vc)含量,考察涂布液制备条件对涂布纸保鲜性能的影响.结果表明:CS中的-NH2和-OH与Ag+发生配位结合,使得结晶度下降;涂布纸SEM的分析表明载银壳聚糖涂布液在纸页表面形成膜层;在CS用量1.5％、AgNO3用量0.2 mmol·L-1、NaBH4用量0.3 mmol·L-1、CS相对分子质量500 kDa时,可获得最佳的保鲜性能;Ag-CS涂布纸有利于减少营养物质的流失,从而延长果蔬的常温贮藏期.     

载Nisin壳聚糖淀粉涂布纸的制备与性能分析

制备一种以天然生物材料为防油抗菌涂层的新型防油抗菌纸,并测试其防油抗菌性能。将防油抗菌剂涂布于纸张表面制备防油抗菌纸,用表面排斥法测试其防油等级,用菌落法计算纸张对大肠杆菌与金黄色葡萄球菌的抑制率。结果表明:1g/100mL壳聚糖溶液与10g/100mL淀粉溶液体积比为12时,涂布纸张的防油等级达到8,防油部分成本约为0.3元/m2;Nisin的添加量达到1g/100mL时,涂布纸张对大肠杆菌以及金黄色葡萄球菌的抑制率分别为70.3%,72.8%。载Nisin壳聚糖淀粉涂布纸在保证防油性的同时,较壳聚糖涂布纸有效降低了成本,控制了黏度,且具有比淀粉涂布纸张更好的韧性与平整度,能有效抑制大肠杆菌和金黄色葡萄球菌。     

载银壳聚糖涂布纸对樱桃番茄保鲜包装效果的影响

本研究以壳聚糖(CS)和Ag NO_3为原料,以Na BH_4为还原剂,制备了载银壳聚糖(AgCS)涂布液,并用该涂布液涂布纸张,制得Ag-CS涂布纸。利用红外光谱仪(FT-IR)、X射线衍射光谱仪(XRD)、扫描电子显微镜(SEM)和X射线光电子能谱仪(XPS)分析Ag-CS复合物结构、形貌和元素组成,以其涂布纸对樱桃番茄(又称圣女果)进行包装,测定其失重率、可滴定酸和标准抗坏血酸(Vc)含量,与无包装、原纸包装、CS涂布纸包装相比较,考察测定不同包装条件对樱桃番茄品质的影响。结果表明,CS中的—NH_2和—OH首先与Ag~+发生配位结合,进而被还原成纳米银和壳聚糖配合物Ag-CS,并使其结晶度下降。SEM分析表明,Ag-CS涂布液在纸张表面形成膜层。通过对比发现,Ag-CS涂布纸包装的樱桃番茄10天后失重率为5.87%,可滴定酸含量下降23.29%,Vc含量下降13.62%。与对照样相比较,Ag-CS涂布纸有利于减少营养物质的流失,从而延长果蔬的常温贮藏期。     

氢氧化钠-尿素-氧化锌体系制备抗油抗菌纸的研究

使用氢氧化钠-尿素-氧化锌水溶液选择性溶解滤纸纤维,以制备自增强的抗油抗菌纸。探讨了处理温度和时间对纸张强度性能和抗油性能的影响,同时评价了制备的抗油抗菌纸对大肠杆菌和金黄色葡萄杆菌的抗菌性能。使用扫描电子显微镜(SEM)、傅里叶红外光谱(FT-IR)、X射线衍射仪(XRD)对纸张结构进行表征,同时使用原子吸收分光光度计(AAS)和X射线光电子能谱(XPS)测定了纸张中氧化锌的含量。结果表明,滤纸经过处理后,纸张抗张指数和耐破指数均提高2倍,在24 h内能够完全阻止油脂渗透,对金黄色葡萄球菌具有明显的抗菌效果,同时纸张中氧化锌含量符合食品安全要求的范围,此法制备的抗油抗菌高强度纸张具有作为食品包装材料的潜力。     

聚苯乙烯纳米复合物涂布包装纸的表面结构和抗菌性能

对可循环利用材料用作抗菌包装材料的可行性进行了评估。向聚苯乙烯（PS）内添加二氧化钛纳米颗粒（添加或不添加银纳米颗粒）制备PS纳米复合物。用5%或10%的PS纳米复合物对稻草浆成纸进行涂布。采用扫描电镜分别对涂布纸和未涂布纸的表面结构进行分析。采用能量色散X射线分析仪对涂布纸进行元素分析。同时对涂布纸的阻隔性能、透气度、施胶度、抗张强度以及对绿脓杆菌、金黄色葡萄球菌、念珠菌和葡萄球菌的抑菌效果进行研究。     

采用聚苯乙烯纳米复合涂料改善包装纸抗菌性能

<正>以聚苯乙烯、二氧化钛纳米颗粒以及银纳米颗粒等为原料制备聚苯乙烯纳米复合涂料,用5%或10%的聚苯乙烯纳米复合涂料对稻草浆制备的包装纸进行涂布,涂布纸的透气度、抗张强度、吸水性以及阻隔性能均得到改善;对绿脓杆菌、金黄色葡萄球菌、念珠菌等细菌有很好的抑菌效果。     

改性凹凸棒土填料在抑菌纸中的应用研究

采用硅烷偶联剂KH550对凹凸棒土(attapulgite,ATP)填料进行改性,再对改性后的ATP负载银离子制备具有抗菌活性的造纸填料。探讨改性ATP载银量的影响因素并对抑菌纸的抑菌性能和物理性能进行评价。结果表明:载银时间、载银温度、硅烷偶联剂KH550用量和硝酸银浓度均对载银量有正向影响,60 min、50℃、硅烷偶联剂用量75%和1 mol·L~(-1)的硝酸银溶液是最合适的载银条件;当填料添加量为10%时,纸张留着率为55.38%,纸张的抗张指数高于空白纸页;抑菌纸对大肠杆菌和金黄色葡萄球菌均呈现出抑菌性能。     

Reliable identification of grapevine rootstock varieties using RAPD PCR on woody samples

Since grapevine ( Vitis spp .) rootstock material is being traded increasingly as disbudded woody material a lack of distinctive morphological features on such material necessitates an alternative and reliable means of identification. Methods described here were developed for rapid and efficient extraction of DNA from woody samples rich in phenolic compounds and polysaccharides, and for subsequent identification of varieties by RAPD PCR. Using these methods, and with the application of only one selected RAPD primer, we were able to differentiate sixteen rootstock varieties, including the seven varieties most commonly used in Germany. Problems commonly encountered with reproducibility of RAPD patterns were avoided by choosing primers with a dinucleotide sequence and a high G/C content that allowed a rather high annealing temperature of 45°C. Methods described here should also be useful for other horticultural crops, especially those with woody tissues rich in phenolic compounds and polysaccharides.     

An internet compendium of analytical methods and spectroscopic information for monomers and additives used in food packaging plastics

An internet website (http://cpf.jrc.it/smt/) has been produced as a means of dissemination of methods of analysis and supporting spectroscopic information on monomers and additives used for food contact materials (principally packaging). The site which is aimed primarily at assisting food control laboratories in the European Union contains analytical information on monomers, starting substances and additives used in the manufacture of plastics materials. A searchable index is provided giving PM and CAS numbers for each of 255 substances. For each substance a data sheet gives regulatory information, chemical structures, physico-chemical information and background information on the use of the substance in particular plastics, and the food packaging applications. For monomers and starting substances (155 compounds) the infra-red and mass spectra are provided, and for additives (100 compounds); additionally proton NMR are available for about 50% of the entries. Where analytical methods have been developed for determining these substances as residual amounts in plastics or as trace amounts in food simulants these methods are also on the website. All information is provided in portable document file (PDF) format which means that high quality copies can be readily printed, using freely available Adobe Acrobat Reader software. The website will in future be maintained and up-dated by the European Commission's Joint Research Centre (JRC) as new substances are authorized for use by the European Commission (DG-ENTR formerly DGIII). Where analytical laboratories (food control or other) require reference substances these can be obtained free-ofcharge from a reference collection housed at the JRC and maintained in conjunction with this website compendium.     

Aroma characterization of various apricot varieties using headspace–solid phase microextraction combined with gas chromatography–mass spectrometry and gas chromatography–olfactometry

The characterization of the aromatic profile of several apricot cultivars with molecular tracers in order to obtain objective data concerning the aromatic quality of this fruit was undertaken using headspace–solid phase microextraction (HS–SPME). Six apricot cultivars were selected according to their organoleptic characteristics: Iranien, Orangered, Goldrich, Hargrand, Rouge du Roussillon and A4025. The aromatic intensity of these varieties measured by HS–SPME–Olfactometry were defined and classified according to the presence and the intensity of grassy, fruity and apricot like notes. In the six varieties, 23 common volatile compounds were identified by HS–SPME–GC–MS. Finally, 10 compounds, ethyl acetate, hexyl acetate, limonene, β-cyclocitral, γ-decalactone, 6-methyl-5-hepten-2-one, linalool, β-ionone, menthone and (E)-hexen-2-al were recognized by HS–SPME–GC–O as responsible of the aromatic notes involved in apricot aroma and considered as molecular tracers of apricot aromatic quality which could be utilized to discriminate apricot varieties.     

Tests of potential functional barriers for laminated multilayer food packages. Part I: Low molecular weight permeants

The advent of the functional barrier concept in food packaging has brought with it a requirement for fast tests of permeation through potential barrier materials. In such tests it would be convenient for both foodstuffs and materials below the functional barrier (sub-barrier materials) to be represented by standard simulants. By means of inverse gas chromatography, liquid paraffin spiked with appropriate permeants was considered as a potential simulant of sub-barrier materials based on polypropylene (PP) or similar polyolefins. Experiments were performed to characterize the kinetics of the permeation of low molecular weight model permeants (octene, toluene and isopropanol) from liquid paraffin, through a surrogate potential functional barrier (25 μm-thick oriented PP) into the food simulants olive oil and 3% (w/v) acetic acid. These permeation results were interpreted in terms of three permeation kinetic models regarding the solubility of a particular model permeant in the post-barrier medium (i.e. the food simulant). The results obtained justify the development and evaluation of liquid sub-barrier simulants that would allow flexible yet rigorous testing of new laminated multilayer packaging materials.     

Analysis of benzo[a]pyrene in spiked fatty foods by second derivative synchronous spectrofluorimetry after microwave-assisted treatment of samples

A simple, rapid and inexpensive method has been developed for the determination of benzo[a     

The development of reference materials for paralytic shellfish poisoning toxins in lyophilized mussel. II: Certification study

This paper describes the second part of a project undertaken to develop certified mussel reference materials for paralytic shellfish poisoning toxins. In the first part two interlaboratory studies were undertaken to investigate the performance of the analytical methodology for several PSP toxins, in particular saxitoxin and decarbamoyl-saxitoxin in lyophilized mussels, and to set criteria for the acceptance of results to be applied during the certification exercise. Fifteen laboratories participated in this certification study and were asked to measure saxitoxin and decarbamoyl-saxitoxin in rehydrated lyophilized mussel material and in a saxitoxin-enriched mussel material. The participants were allowed to use a method of their choice but with an extraction procedure to be strictly followed. The study included extra experiments to verify the detection limits for both saxitoxin and decarbamoyl-saxitoxin. Most participants (13 of 15) were able to meet all the criteria set for the certification study. Results for saxitoxin.2HCl yielded a certified mass fraction of <0.07 mg/kg in the rehydrated lyophilized mussels. Results obtained for decarbamoyl-saxitoxin.2HCl yielded a certified mass fraction of 1.59+/-0.20 mg/kg. The results for saxitoxin.2HCl in enriched blank mussel yielded a certified mass fraction of 0.48 +/- 0.06 mg/kg. These certified reference materials for paralytic shellfish poisoning toxins in lyophilized mussel material are the first available for laboratories to test their method for accuracy and performance.     

Announcing a new international peer-reviewed journal:Food Science and Human Wellness now accepting manuscript submission in English

<正>We are pleased to announce the launch of a new international peer-reviewed journal-Food Science and Human Wellness,ISSN 2213-4530,which is an open access journal,produced and hosted by Elsevier B.V.on behalf of Beijing Academy of Food Sciences.Food Science and Human Wellness is an international peer-reviewed English journal that provides a forum for the dissemination of the     

Chinese CTP Market

According to Printing and Printing Equipment Industries Association of China（PEIAC）＇s statistics to the plate manufucturer in China, in 2013, the actual offset plate production has reached 346 million square meters in China. Among them, the CTP production volume was 245 million square meters, up by 11% than that of last year; the total sales of the CTP plate was 239 million square meters, up by 13%.     

Preparatory Work of Print China 2015 is Going Smoothly

正Held at Guangdong Modern International Exhibition Center,Print China 2015 will cover 7exhibition halls,besides the original Hall No.3,4,5,6,7,the newly built F zone of Hall 3 will be used too.The total area will be140,000 square meters.Hall 3:Offset and large printing equipment,package printing equipment,post press