Novel test method for accurate characterization of intralaminar fracture toughness in CFRP laminates

A novel initial crack insertion method, “intralaminar film insertion method”, was proposed to investigate the fracture toughness of unidirectional carbon fiber reinforced plastic (CFRP) laminates when the crack propagates inside the ply and not in the interlayer resin-rich area. Here, a release film was inserted inside a single lamina during the resin impregnation process of prepreg manufacturing. Mode I intralaminar fracture toughness tests were carried out for conventional CFRP laminates and interlayer toughened CFRP laminates. For comparison, two conventional methods were used to introduce initial cracks. One is the “interlaminar film method”, where a release film is inserted between two prepreg plies during the lay-up process. The other is the “machined slit method”, where a slit notch is machined in parallel to the layer of CFRP laminates. It was demonstrated that the proposed “intralaminar film method” can correctly evaluate the intralaminar fracture toughness of both conventional CFRP laminate and interlayer toughened CFRP laminate from the initial value to the propagation value. For this range, it was also found that the intralaminar fracture toughness of interlayer toughened CFRP laminate was the same as that of conventional CFRP laminate. Thus, the intralaminar fracture toughness was not influenced by interlayer toughening.     

Acoustic emission study of fatigue crack closure of physical short and long cracks for aluminum alloy LY12CZ

Crack closure of physical short and long cracks of LY12CZ aluminum alloy during fatigue process was investigated using acoustic emission (AE) technique. Results showed that the effective fatigue crack growth curve (da/dN vs. ΔK_eff) of physical short and long cracks obtained by the AE technique was consistent with the effective fatigue crack growth curve at high stress ratio (R = 0.8), which implied that the AE technique could measure the crack closure level, especially for physical short crack. The growth rate of physical short crack was much higher than that of long crack at the same ΔK, and the lower crack closure level of short crack was the main reason.     

The influence of a thermoplastic toughening interlayer and hydrothermal conditioning on the Mode-II interlaminar fracture toughness of Carbon/Benzoxazine composites

Carbon fibre/Benzoxazine laminates with and without non-woven polyamide (PA) fibre veils at the interlaminar regions were manufactured using vacuum assisted resin transfer moulding (VARTM). The effect of the interlaminar thermoplastic veils on the Mode-II critical strain energy release rate (G_IIC), under both wet and dry conditions, was determined using two commercially available Benzoxazine resins: a toughened system and an untoughened system. In all samples the toughened system outperformed the untoughened system. The overall resistance to Mode-II crack growth was significantly improved by the inclusion of the interlaminar veils due to an increase in the thickness of the matrix-rich interlaminar region, plastic deformation of the PA fibres and a crack-pinning mechanism. Moisture caused an increase in matrix ductility, which improved the resistance to crack initiation; however, this was counteracted by a reduction in fibre/matrix interfacial strength causing a reduction in resistance to crack growth.     

Improvement of interlaminar mechanical properties of CFRP laminates using VGCF

In order to improve the interlaminar mechanical properties of CFRP laminates, hybrid CFRP/VGCF laminates have been fabricated by using a newly-developed method, i.e., powder method, where the powder of vapor grown carbon fiber (VGCF) is added at the mid-plane of [0°/0°]₁₄ CFRP laminates. Experimental results of double cantilever beam (DCB) tests indicate the improvement on the interlaminar mechanical properties of Mode-I fracture behavior with much higher critical load P_C and fracture toughness G_IC with VGCF interlayer. Crack propagation and fracture surface have also been observed to interpret this improvement mechanism. Moreover, based on experimental G_IC, numerical simulations using finite element method (FEM) with cohesive elements have been carried out to analyze the delamination propagation. The interlaminar tensile strength of hybrid CFRP/VGCF laminates, which is obtained by matching the numerical load–COD (crack opening displacement) curves to experimental ones, is higher than that of base CFRP laminates.     

Interfacial fatigue crack propagation in microscopic model composite using bifiber shear specimens

Interfacial fatigue crack growth behavior in GF/epoxy model composites was investigated using bifiber shear (BFS) specimens in a scanning electron microscope. The specimen is composed of two E-glass filaments with diameters of 23 and 40 μm, and bisphenol A type epoxy is impregnated between the filaments. The crack growth behavior under different stress ratios was investigated to clarify the fatigue crack growth mechanism. The change in the crack growth rate, da/dN, was not monotonic with crack length, suggesting a variation in the resistance to fatigue crack growth along a single filament. The resistance to fatigue crack growth of the interface is much smaller than that of composite laminates. The fatigue crack growth mechanism of the glass fiber/epoxy interface under different stress ratios is controlled by the maximum energy release rate, G_max, which is completely different from that of composite laminates.     

Failure analysis of a petrochemical plant reducing gear

This study aims to investigate the cause of failure of an 845 mm external diameter reducing gear that operated during 30 months in a petrochemical plant. The failure analysis procedure included material characterisation (microstructure, chemical composition and microhardness), fracture surface evaluation, and stress distribution by finite elements on critical regions of the gear. Fracture mechanics and fatigue crack growth were also used to develop a da/dN–ΔK curve and then determine the gear material crack growth resistance. Results indicate that the gear was not properly manufactured and failure occurred as a result of a fatigue process facilitated by a manufacturing defect.     

Transverse crack growth behavior considering free-edge effect in quasi-isotropic CFRP laminates under high-cycle fatigue loading

The high-cycle fatigue characteristics focused on the behavior of the transverse crack growth up to 10⁸ cycles were investigated using quasi-isotropic carbon fiber reinforced plastic (CFRP) laminates whose stacking sequence was [−45/0/45/90]_s. To assess the fatigue behavior in the high-cycle region, fatigue tests were conducted at a frequency of 100 Hz in addition to 5 Hz. In this study, to evaluate quantitative characteristics of the transverse crack growth in the high-cycle region, the energy release rate considering the free-edge effect was calculated. Transverse crack growth behavior was evaluated based on a modified Paris law approach. The results revealed that transverse crack growth was delayed under the test conditions of the applied stress level of σ_max/σ_b = 0.2.     

Mixed Bending-Tension (MBT) test for mode I interlaminar and intralaminar fracture

A new Mixed Bending-Tension (MBT) test is proposed for mode I fracture of laminated composites. The MBT specimen consists of a relatively small pre-cracked laminate adhesively bonded to pin-loaded steel beams. This design reduces significantly the bending stresses that prevent successful application of DCB tests to certain laminates. The MBT was here applied to carbon/epoxy unidirectional [0°]₂₆ and [90°]₂₆ laminates with starter delaminations. Interlaminar initiation G_IC values of [0°]₂₆ laminates agreed well with previous DCB test results, while [90°]₂₆ laminates exhibited 50% higher values. Significant lengths of fairly planar intralaminar crack propagation were seen in the latter laminates. The results showed a fibre bridging related R-curve, which was more pronounced in [0°]₂₆ laminates. The consistency of the present results indicates that the MBT opens new possibilities for the interlaminar and intralaminar mode I fracture.     

Fatigue crack growth acceleration due to intermittent overstressing in adhesively bonded CFRP joints

Double cantilever beam joints were used to investigate cohesive and interlaminar crack growth in bonded composite joints under constant and variable amplitude (VA) loading. Numerical crack growth integration was used to predict the VA fatigue life using constant amplitude data. This underestimated the fatigue crack growth rate for interlaminar cracks, indicating crack growth acceleration due to load interactions. This was also the case for cohesive cracks subjected to a moderate initial strain energy release rate (G_max). An unstable crack growth regime was also identified for the case of high initial G_max cohesive crack propagation. This behaviour is attributed to the development of a damage zone ahead of the crack tip.     

Structure property relation of hybrid biocomposites based on jute,viscose and polypropylene: The effect of the fibre content and the length on the fracture toughness and the fatigue properties

In the present study, the extent of jute and viscose fibre breakage during the extrusion process on the fracture toughness and the fatigue properties was investigated. The composite materials were manufactured using direct long fibre thermoplastic (D-LFT) extrusion, followed by compression moulding. The fracture toughness (K_IC) and the fracture energy (G_IC) of the PP–J30 composites were significantly improved (133% and 514%, respectively) with the addition of 10 wt% viscose fibres, indicating hindered crack propagation. The addition of viscose fibres resulted in three times higher fatigue life compared with that of the unmodified jute composites. Further, with the addition of (2 wt%) MAPP, the PP–J30–V10 resulted in a higher average viscose fibre length of 8.1 mm, and the fracture toughness and fracture energy increased from 9.1 to 10.0 MPa m^1/2 and 28.9 to 31.2 kJ/m², respectively. Similarly, the fatigue life increased 51% compared with the PP–J30–V10, thus demonstrating the increased work energy due to hindrance of the propagation of cracks.     

Experiments under pure shear and rolling contact fatigue conditions: Competition between tensile and shear mode crack growth

In the present paper, the mechanism of shear crack growth under both pure torsion and mixed mode loadings, simulating rolling contact fatigue testing conditions, has been investigated for a bearing steel and the role of the superimposed compressive stress in subsurface RCF has been clarified both numerically and experimentally. In particular a previous data set of fatigue tests on micro-notched specimens subjected to torsion and out-of-phase loads with |σ_min|/τ_max ≅ 3.5 (LP1) has been complemented with the new tests onto micro-notched specimens loads with |σ_min|/τ_max ≅ 0.7 (LP2) and a test under pure compression. The same tests have been also simulated numerically with a non-linear FE analysis of crack advance. The numerical analyses have been conducted with the aim of demonstrating that the compressive stress fully suppresses the tendency to tensile mode growth as the crack extends.Eventually, the competition between tensile and shear mode growth during a fatigue cycle has been investigated theoretically in terms of local branch SIFs. In particular, the conditions for the branch crack growth have been examined on the basis of the effective SIFs: the crack tip shielding effects due to the crack surface interference (both the mode I contribution caused by the asperity mismatch and the shear attenuation produced by the frictional stresses) have been quantified by employing a model for crack sliding interaction under pure mode III and mixed mode I + III loadings.     

Short cracks initiated in Al 6013-T6 with the focused ion beam (FIB)-technology

The fatigue crack growth behaviour of short corner cracks in the Aluminium alloy Al 6013-T6 was investigated. The aim was to determine the crack growth rates of small corner cracks at a stress ratio of R = 0.1, R = 0.7 and R = 0.8 and to find a possible way to predict these crack growth rates from fatigue crack growth curves determined for long cracks. Corner cracks were introduced into short crack specimens, similar to M(T) – specimens, at one side of a hole (Ø = 4.8 mm) by cyclic compression (R = 20). The precracks were smaller than 100 μm (notch + precrack). A completely new method was used to cut very small notches (10–50 μm) into the specimens with a focussed ion beam. The results of the fatigue crack growth tests with short corner cracks were compared with the long fatigue crack growth test data. The short cracks grew at ΔK-values below the threshold for long cracks at the same stress ratio. They also grew faster than long cracks at the same ΔK-values and the same stress ratios. A model was created on the basis of constant K_max-tests with long cracks that gives a good and conservative estimation of the short crack growth rates.     

Mode II interlaminar fracture properties of Moso bamboo

Bamboo is a kind of biological composites reinforced by unidirectional long fiber. Once there exists crack, the propagation of delamination is controlled by the interlaminar fracture toughness instead of by strength. In this paper, the end notched flexure (ENF) beam specimen was used to test the Mode II interlaminar fracture toughness G_IIC along grain of Moso bamboo internode and the fracture surface was analyzed. The results were obtained that the Mode II interlaminar fracture toughness G_IIC calculated by the experiment parameter substitution method was more accurate and the value was 1303.18 J/m² (coefficient of variation = 8.96%) which was about three times higher than the value of Mode I interlaminar fracture toughness; the crack propagation of Mode II interlaminar fracture was mainly self-similar cracking, but the fracture surface was rougher. Ground tissue in the zone of Mode II crack propagation was characterized by hackle shearing deformation. The SEM photos showed that ground tissue separated from fiber along middle lamella under shear stress and as the increasing of the dislocation of upper and lower layer, the thin-walled ground tissue would fracture transversely by tension, while to thick-walled fiber cell, only middle lamella and primary wall were torn then debonded, fragments remained.     

The fatigue crack growth rate and crack opening displacement in 18G2A-steel under tension

In the paper, the results of crack tip opening displacement (CTOD) and crack opening displacement (COD) in place of crack initiation as well as the fatigue crack growth rate in higher strength steel are presented. The investigation were carried out on flat specimens with central notch under constant amplitude tensile fatigue loading at stress ratio R = 0.2 and different value of the stress σ_max. The test results showed that with growth of crack length l grew values of the CTOD and COD. In the work, it was proposed calculation of the CTOD value on basis various dependence of plastic zone radius on crack tip.     

Defect detection in CFRP by infrared thermography with CO2 Laser excitation compared to conventional lock-in infrared thermography

This paper presents a NDT by a CO₂ Laser infrared thermography applied to defect detection in CFRP. The CO₂ Laser is an infrared laser with the wavelength of 10.6 μm. This excitation has a controllable heating beam by a geometric relation D = 0.01575·d, which allows to heat the samples at a specific position (placed at the distance “d”) and area (of a diameter “D”). The PPT interpretation principle was used to reduce the non-uniformity’s effect of the excitation causing inhomogeneous heat. The test with this excitation is much faster than the tests with conventional lock-in thermography method.     

Application of crack tip plasticity based fatigue model on high temperature alloy HAYNES® 282®

Confined crack tip plasticity model is employed to predict time independent fatigue crack growth rate (FCGR) behavior of HAYNES® 282® alloy at temperatures 1200F and 1400F. Crack growth tests were done in lab air, vacuum and steam environments at load ratios R = K_min/K_max ranging from 0.05 to 0.5. Calibrated model predicts average cyclic crack growth rate behavior of the material reasonably well. Predictions do not capture the accelerated fatigue crack growth rates observed in the data at low load levels. Such effects are believed to be caused by environmentally driven factors, which are not expected to be predicted by plasticity based models.     

Experimental investigation of R-ratio effects on fatigue crack growth of adhesively-bonded pultruded GFRP DCB joints under CA loading

A series of fatigue experiments was performed in order to investigate the effect of the R-ratio on the fatigue/fracture behavior of adhesively-bonded pultruded GFRP double cantilever beam joints. Constant amplitude fatigue experiments were carried out under displacement control with a frequency of 5 Hz in ambient laboratory conditions. Three different R-ratios were applied: R = 0.1, R = 0.5 and R = 0.8. The crack length was determined by means of crack gages and a dynamic compliance method. The dominant failure mode was a fiber-tear failure that occurred in the mat layers of the pultruded laminates. The depth of the crack location significantly affected the energy dissipated for the fracture under cyclic loading. Short-fiber and roving bridging increased the fracture resistance during crack propagation. Fatigue crack growth curves were derived for each R-ratio and each observed crack path location. The fatigue threshold and slope of the fatigue crack growth curve significantly increased with increased R-ratio.     

Cyclic fatigue delamination of carbon fiber-reinforced polymer-matrix composites: Data analysis and design considerations

Activities toward standardization of fracture mechanics tests on carbon fiber-reinforced polymer-matrix (CFRP) composites have recently focused on cyclic fatigue under mode I (tensile opening), mode II (in-plane shear) and mixed-mode I/II loading. Data from recent round robins performed by Technical Committee 4 (TC4) of the European Structural Integrity Society (ESIS) and from preliminary testing of additional CFRP epoxy laminates at the authors’ laboratories are analyzed with different approaches in attempts to reduce scatter and to identify parameters for CFRP structural design. Selected test data comparing load and displacement control for the cyclic fatigue tests are also discussed. Specifically, threshold values from Paris-law data fitting are compared with values from fitting with a modified Hartman–Schijve approach. Independent of the approach used for the analysis, mode I threshold values of selected CFRP seem to be in the range between about 30 and 100 J/m², i.e., roughly around the range of critical mode I energy release rate values (denoted by G_IC) obtained from fracture testing of neat commercial epoxy resins, but clearly below quasi-static initiation G_IC-values for unidirectional CFRP composites. Implications for CFRP structural design based on mode I fatigue fracture mechanics test data are briefly discussed.