AMARANTH GRAIN DRYING IN A FLUIDIZED BED

An empirical equation as a function of drying time and temperature was developed to calculate the moisture ratio required Tor balch fluidized bed dryers design for amaranth grain drying

The relative deviations of the moisture ratio values calculated with the proposed equation with regard to the experimental ones ranged between 0.014 and 0.095 for a drying air temperature between 60 and 100 ° C, and a grain initial moisture content between 23.5 and 16.6 % wb.     

Determination of Spray-Drying Kinetics in a Small Scale

The main aim of the study presented in this article was to develop and test a method to determine spray-drying kinetics in a laboratory scale. A special measuring tunnel to obtain evaporation rate similar to the conditions observed in a spray-drying column was designed, built and tested.

Extensive studies of drying kinetics for maltodextrin were performed for different air flow rates and air temperatures. Test runs to determine repeatability of this technique showed satisfactory agreement between subsequent measurements, which confirms accuracy of the developed measuring method.

An effect of the initial moisture content on the critical moisture content was observed which is related to a decrease of the equilibrium vapor pressure over the solution and a decrease of the driving force of evaporation and drying rate of the process.

Results of the experiments proved that the generalized drying curve obtained from small-scale experiments could be used to describe spray-drying kinetics if the critical moisture content of the material is known.     

Heating/Drying Using Particulate Medium : A Review Part II. Equipment

This paper presentS an overview of particulate medium dryers developed to evaluate the drying of grains using heated particulate media. Components of particulate medium heating and drying equipments as well as the devices employed to conduct the materials through the machine are described. How these components accomplish the basic processes involved in conduction/particulate medium heating is also explained.

To characterize the performance of these dryers based on criteria developed for farm level dryers was not possible because of the different methods employed by researchers and the various conditions the equipment were subjected to. So in order to assess the operating characteristics of each design. the dryers were compared based on their ability to remove moisture and their thermal and drying efficiency. Comparison was made on the methods utilised by each design to accomplish heating of the medium, mixing the medium with grain, the separation of the medium from grain, and the means of recirculating the medium.

Several studies conducted to evaluate the different parameters which influence drying using heated particulates are discussed. The granular media used in heating the grain and the corresponding types of grains used in the tests are also presented.     

Kinetic Study and Modeling of the Degradation of the Maize Kernels Quality During Drying in Fluidized Bed

Only a few kinetic studies have been reported in the literature on the evolution of comercial quality of maize during drying and to the best of our knowledge no model allows to predict the dynamic coupling of drying and product quality evolution. The aim of this work is to present new information on the effects of the operating conditions (harvest year, weight of maize to be dried, initial moisture content of the grain and air temperature) on the evolution of maize saline-soluble protein denaturation and the wet-milling quality during drying of maize in a batch floatation fluidized bed dryer. Also, kinetic laws are proposed for the quality criteria that will be combined with drying model already derived [1, 2].

The experimental results show that the degradation of the main components of maize (starch and proteins) is considerably affected by the temperature level and to a lesser extent by the initial moisture content of grains. Beyond 70°C, the denaturation of saline-soluble proteins occurs rapidly in the heat-up period of the grains. As for the wet-milling quality degradation, it starts only above 90°C.

Kinetic laws derived from this study express the variation of the degradation rate of proteic and wet milling quality as functions of the solubility of saline-soluble proteins or the starch-gluten separation index, the grain moisture content and temperature.     

A MATHEMATICAL MODEL FOR PARALLEL FLOW DRYER FOR SLABS WITH HIGH THERMAL DIFFUSIVITY

An analytical model for the process is developed. The thermal diffusivity of the drying slabs is assumed infinite and the moisture diffusivity constant during the entire drying process.

With specified initial and boundary conditions, the mathematical model yields a two-part solution for the diffusion equation. The first part is valid for the initial drying during which the surface moisture content exceeds the value of fiber saturation. This part of the solution is used until the surface moisture content drops to the fiber saturation value. The moisture profile at the end of this period is used as the initial condition for the second period of drying which takes place under hygroscopic conditions.

Two simplifying assumptions are adapted for the hygroscopic region: 1. The dependence between the surface temperature and the moisture content is linear. 2. Constant (average) absorption heat is used during this second drying period.

For both parts of the solution, the surface moisture gradient is proportional to the local temperature difference between the drying air and the slab surface. This temperature difference can be expressed by means of a water mass balance equation for the part of the dryer between the slab in-feed and the point considered and by using the thermodynamic properties of the humid air.     

PROCESSES RELATED TO DRYING: PART II USE OF THE SAME MODEL TO SOLVE TRANSFERS BOTH IN SATURATED AND UNSATURATED POROUS MEDIA

From the mathematical formulation presented in part I, a numerical code is developed to simulate heat and: mass transfers in porous media. The aim of this· tool is to understand and to improve each process related to drying. The association of a comprehensive set of equations with a efficient 2-D computer code allows us to predict the comportment of several porous media even if submitted to severe drying conditions. A few runs have been selected with special attention paid to the effect of internal gaseous pressure:

Convective drying of softwood at high temperature illustrate the typical two-dimensional transfers that occur in an anisotropic medium.

Microwave drying of light concrete pinpoints liquid expulsion of water which is driven by the pressure due to internal heating.

Finally, appropriate physical behaviours of a bed of glass spheres allows one to deal with simple processes for which full saturation occurs.     

VACUUM DRYING OF OAKWOOD :MOISTURE STRAINS AND DRYING PROCESS

After presenting the characteristics and the data acquired in an industrial evacuated kiln, a simplified analysis of heat and mass transfers is proposed. This analysis is based on the existence of a evaporization front determining two zones in the longitudinal direction :

-a dried zone in which moisture is less than 30 %

-a wet zone in which moisture is still at its initial value.

Such a hypothesis allows to study transfers transversally first, then longitudinally. Both equation systems ore linked by conditions of continuity for mass and energy.

This study allows to determine the shapes of the temperature and pressure curves in the longitudinal direction. The linearity of the variation of the average drying velocity versus the average moisture content of the board is also proved. Finally, the modeling of mechanical phenomena thanks to a finite element program shows the rupture zones appearing during the drying process.     

A STUDY OF CLOSED CYCLE DRYING FOR THE COATED FILM WITH ORGANIC SOLVENT ON THE CONTINUOUS SHEET MATERIALS

The conventional drying of the coated film with organic solvent on continuous sheet materials is usually performed in open or one pass drying system using air as the drying medium. The concentration of evaporated organic solvent in the drying system must be low enough to prevent explosion and large volume of off gas from dryer to solvent recovery system is required, resulting in poor heat economy for all the plant

To improve the heat economy of the plant it had been proposed to use a closed cycle drying system, where an inert gas, e.g. nitrogen, is used as the drying medium. High concentration of the organic solvent in the recycle gas mixture may then be used, which results in smaller volume of recycle gas and possibility of applying an inexpensive solvent recovery system of dehumidification. This investigation includes two important problems to realize the closed cycle drying

(1)Measurement of solvent (toluene) evaporation rate from coated film in the gas mixture of toluene andnitrogen over a wide range of toluene/nitrogen ratios (0-1.0) and drying temperature using bench scaleapparatus

(2)Development of a contactless sealing method, using an inert gas, for closed cycle drying of continuoussheet materials. The results of preliminary tests demonstrate its feasibility.     

Food Drying and Dewatering

Food drying and dewatering raises a growing interest because of increasing requirements in quality, specially in the production of ingredients and additives for food formulation. Heat and mass transfers, as well as mechanical phenomena and reactions kinetics induced by these transfers must be more and more carefully controlled during drying and storage.

This chapter relates recent advances in

- drying of solids

- spray-drying

- drum-dryine

- superheateded steam drying

- osmotice dehydration

- hot oil immersion drying     

KINETICS OF DRYING IN CYCLICALLY SHIFTED SPOUTED BED

This paper presents kinetics of batchwise drying in a spouted bed apparatus with cyclically shifted gas stream, i.e. drying medium flowrate is changed cyclically along inlet cross-section of a bed during operation time.

Such an apparatus provides advantages of both spouted and oscillating beds which include: good hydrodynamic conditions within the bed and energy savings. Two types of particulate materials, i.e. beet and wheat seeds, which differ largely in physical properties were used in experiments.

Based on the results of this investigation formulae for reduced moisture content (X^red) in dependence on drying time and air temperature were developed.     

DIFFUSION COEFFICIENTS FOR PREDICTING ROUGH RICE RE-WETTING BEHAVIOR

Thin-layer re-wetting experiments were conducted with medium grain rough rice in the temperature range of 17.8 to 45^°C and for relative humidities between 56 and 89.3%, with initial moisture contents in the range of 10.26 to 12.71% dry-basis to determine the diffusion coefficient of rough rice. Recent efforts to characterize the re-wetting characteristics of rough rice are summarized. New equation for temperature dependent liquid diffusion coefficients for medium grain rough rice are presented. The diffusion coefficient in re-wetting was lower than the drying. The results presented here, over typically five day re-wetting, will be useful in studying the longer term moisture transfer process occurring during ventilated storage.     

SOLAR GRAIN DRYING IN HUMID AND HOT-TEMPERATE CLIMATES

A natural solar drying system has been tested with wheat. Simple solar collectors give the small temperature rise needed for low temperature drying. The system, with a capacity of 35 tomes, is placed in a region of humid hot-temperate climate. It has been designed to dry all the locally produced grain (wheat, corn, soybean, sunflower, sorghum, etc.), without a supplemental heat source.

Two different types of solar collectors of the same effective area were tested, with one a storage-collector and the other a bare plate collector

Data from four field tests performed between 1981 and 1983 are given and discussed. The mean mass of water removed from the wheat per hour was of 6.54 kg, under an average air flow of 4.3 m3 /min. tonne     

SOLAR DRYING OF GRAPES

Mass losses and low quality are the most serious disadvantages of traditional grape drying methods. For the production of high quality raisins an increase in the drying rate is required and the grapes should be protected from rain, dust and insects during drying.

Under the terms of a joint German-Greek research program low-cost solar grape dryers were developed in the Institute of Agricultural Engineering of Hohenheim University and were tested in Greece in cooperation with the Crete Agricultural Research Center.

The required data basis for optimizing solar grape dryers was obtained by additional laboratory tests measuring the influence of various drying parameters on drying rate and quality.

Tests with the solar dryers have shown that it is possible to reduce the drying time and improve the quality significantly compared to the traditional drying methods. Also mass losses due to rain can be prevented.     

Determination of Moisture Diffusivity of Lentil Seed During Drying

The mechanism of drying and the diffusion of water in green (fresh), red and whole lentils (4.20-4.32 mm diameter and 2.20-2.30 mm thickness) were successfully interpreted and modelled by using Fick's law. The moisture content of fresh green lentil was 55 % and moisture content of the red and whole lentils was increased to 39-40 % and drying temperature (45-60°C) was varied, but the velocity and the humidity of the drying air was kept constant.

The effective diffusuvity was estimated from drying rate curves and expressed by an Arrhenius relation.     

Drying Characteristics of Porous Materials in a Fluidized Bed under Reduced Pressure

The drying of porous materials immersed in the fluidized bed under reduced pressure was performed, and the results were compared with those of hot air drying. The pressure in drying chamber was changed (5.0-101.3 kPa) and the effect of it was examined.

The temperature of the sample center becomes lower as the pressure in drying chamber decreases, and the temperature in fluidized-bed drying is higher than that in hot air drying at the same pressure. The effect of pressure in drying chamber on the sample temperature is significant for different temperatures of drying gas.     

COMPARISON OF SUPERHEATED STEAM AND AIR OPERATED SPRAY DRYERS USING COMPUTATIONAL FLUID DYNAMICS.

In this paper a numerical simulation of a spray dryer using the computational fluid dynamics (CFD) code Fluent is described. This simulation is based on a discrete droplet model and solve the partial differential equations of momentum, heat and mass conservation for both gas and dispersed phase.

The model is used to simulate the behaviour of a pilot scale spray dryer operated with two drying media : superheated steam and air Considering that there is no risk of powder ignition in superheated steam, we choosed a rather high inlet temperature (973 K). For the simulation, drop size spectrum is represented by 6 discrete droplets diameters, fitting to an experimental droplets size distribution and all droplets are injected at the same velocity, equal to the calculated velocity of the liquid sheet at the nozzle orifice.

It is showed that the model can evaluate the most important features of a spray dryer : temperature distribution inside the chamber, velocity of gas, droplets trajectories as well as deposits on the walls. The model predicts a fast down flowing core jet surrounded by a large recirculation zone. Using superheated steam or air as a drying medium shows only slight differences in flow patterns. Except for the recirculation which is tighter in steam.

The general behaviour of droplets in air or steam are quite the same : smallest droplets are entrained by the central core and largest ones are taken into the recirculation zone. In superheated steam, the droplets penetrate to a greater extent in the recirculation zone. Also, they evaporate faster. The contours of gas temperature reflect these differences as these two aspects are strongly coupled. In both air and steam there is a “cool” zone which is narrower in steam than in air. Finally, the panicle deposit problem seems to be more pronounced in air than in steam.

Adding to the inherent interest in using superheated steam as a drying medium, the model predicts attractive behaviour for spray drying with superheated steam. In particular. under the conditions tested with the model, a higher volumetric drying rate is obtained in superheated steam.     

THE INFLUENCE OF PRESSURE AND TEMPERATURE ON THE KINETICS OF VACUUM DRYING OF KETOPROFEN

This paper explores the influence of temperature and pressure on drying kinetics of 2-(3-benzoylphenil propionic acid) ketoprofen, in a vacuum dryer on laboratory scale, Experimentally determined relations between moisture content and drying rate vs time, were approximated with an exponential model. Model parameters were correlated with drying conditions (temperature, pressure) and defined by functions of their potentions.

From an energy balance of the process, a mathematical model for simulating dependence of sample temperature vs drying time, and moisture content of material, has been developed.

Simulation of the drying kinetics and sample temperature, by use of those functional dependencies shows good agreement with experimental results.     

Heating/Drying Using Particulate Medium : A Review Part I. General and Heat transfer parameters

This paper presents an Overview of particulate medium drying and heat treating of cereal grains. While the conventional air drying of grains is well documented, studies on the drying of grains using heated granular medium do not appear to exist. The scientific study of the different aspects of drying with a heated granular medium began in the early 1970's. Progress on the utilization of particle-to-particle heat transfer was slow as evidenced by the fact that there is no commercial dryer using the method as of today.

The first section of this paper deals with conduction heating and how it led to the use of granular medium in heating the grain. Starting with the earliest work on conduction heating reported by Kelly ( 1939), the developments in the heating of grain using granular media is discussed. For decades since Kelly's report, work in the subject area dealt mostly with the theoretical aspects of solid-to-solid heat transfer. Thus, in the succeeding section of the paper, heat transfer parameters and mechanisms involved in the process are thoroughly investigated.     

PROCESSES RELATED TO DRYING: PART I, THEORETICAL MODEL

The aim of this paper is to summarize ten years of work in order to model the drying of solids. Nowadays there is a general agreement amongst the various researchers worldwide. If the porous medium is viewed at the so-called “macroscopic” scale (that is to say when it is viewed as a continuous and homogeneous equivalent medium) a set of three partial derivative equations is derived, three state variables being necessary to thermodynamically describe the medium (temperature, moisture content and total pressure in the gaseous phase for example).

After a short historical survey of the modeling of drying, we want to obtain this set of equations drawing the readers attention to three particular points : the importance of the air mass balance, the right way to write the energy equation (and the associated boundary conditions) and the taking into account of the adsorbed water.

A second part of this article [I] will be devoted to the numerical solution of this problem and will illustrate these points.