Mechanical behaviour of glass and carbon fibre reinforced composites at varying strain rates

The choice of composite materials as a substitute for metallic materials in technological applications is becoming more pronounced especially due to the great weight savings these materials offer. In many of these practical situations, the structures are prone to high impact loads. Material and structural response vary significantly under impact loading conditions as compared to quasi-static loading. The strain rate sensitivity of both carbon fibre reinforced polymer (CFRP) and glass fibre reinforced polymer (GFRP) are studied by testing a single laminate configuration, viz. cross-ply [0°/90°] polymer matrix composites (PMC) at strain rates of 10⁻³ and 450 s⁻¹. The compressive material properties are determined by testing both laminate systems, viz. CFRP and GFRP at low to high strain rates. The laminates were fabricated from 48 layers of cross-ply carbon fibre and glass fibre epoxy. Dynamic test results were compared with static compression test carried out on specimens with the same dimensions. Preliminary compressive stress–strain vs. strain rates data obtained show that the dynamic material strength for GFRP increases with increasing strain rates. The strain to failure for both CFRP and GFRP is seen to decrease with increasing strain rate.     

Strain rate effects on the compressive property and the energy-absorbing capacity of aluminum alloy foams

The strain rate sensitivity of various relative densities, open-cell aluminum alloy foams fabricated by a powder metallurgical method is investigated under compression loading. Their response to strain rate has been tested over a wide range of strain rates, from 10⁻³ to 2600 s⁻¹ at room temperature. Within this range, the experimental results show that the yield strength and the energy absorbed increase with an increase of strain rate. However, the yield strength of higher relative density foams increases bilinearly with the logarithm of strain rate, and the yield strength of lower relative density foams shows only a linear increase. The compaction strain slightly decreases with an increase of strain rate. The higher relative density aluminum alloy foams are more sensitive to strain rate than the lower relative density foams.     

High strain rate mechanical behavior of epoxy under compressive loading: Experimental and modeling studies

Investigations on high strain rate behavior of epoxy LY 556 under compressive loading are presented. Compressive Split Hopkinson Pressure Bar (SHPB) apparatus was used for the experimental investigations. The studies are presented in the strain rate range of 683-1890 per second. It was generally observed that the compressive strength is enhanced at high strain rate loading compared with that at quasi-static loading. During SHPB testing of the specimens, it was observed that the peak force obtained from the strain gauge mounted on the transmitter bar is lower than the peak force obtained from the strain gauge mounted on the incident bar. Further, an analytical method is presented based on variable rate power law for the prediction of compressive strength at high strain rate loading for epoxy LY 556. Using the analytical method, high strain rate compressive stress-strain behavior is presented up to strain rate of 10,000 per second.     

High strain rate compression response of carbon/epoxy laminate composites

Composite materials exhibit excellent mechanical properties over metallic materials and hence are increasingly considered for high technology applications. In many practical situations, the structures are subjected to loading at very high strain rates. Material and structural response vary significantly under such loading as compared to static loading. A structure that is expected to perform under dynamic loading conditions, if designed with the static properties, might be too conservative. Hence, it is necessary to characterize the advanced composites under high strain rate loading. In the current investigations, the response of carbon/epoxy laminated composites under high strain rate compression loading is considered using a modified split Hopkinson Pressure Bar (SHPB) setup at three different strain rates of 82, 164 and 817 s⁻¹. The laminates were fabricated using 32 plies of a DA 4518 unidirectional carbon/epoxy prepreg system. Both unidirectional and cross-ply laminates were considered for the study. In the case of cross-ply laminates, the samples were tested in the thickness as well as in the in-plane direction. The unidirectional laminate samples were subjected to loading along 0° and 90° directions. Dynamic stress–strain plot was obtained for each sample and compared with the static compression test result. The results of the study indicate that the dynamic strength (with the exception of through the thickness loading of cross-ply laminates) and stiffness exhibit considerable increase as compared to the static values within the tested range of strain rates.     

Further investigation on the dynamic compressive strength enhancement of concrete-like materials based on split Hopkinson pressure bar tests. Part I: Experiments

Effects of the inertia-induced radial confinement on the dynamic increase factor (DIF) of a mortar specimen are investigated in split Hopkinson pressure bar (SHPB) tests. It is shown that axial strain acceleration is unavoidable in SHPB tests on brittle samples at high strain-rates although it can be reduced by the application of a wave shaper. By introducing proper measures of the strain-rate and axial strain acceleration, their correlations are established. In order to demonstrate the influence of inertia-induced confinement on the dynamic compressive strength of concrete-like materials, tubular mortar specimens are used to reduce the inertia-induced radial confinement in SHPB tests. It is shown that the DIF measured by SHPB tests on tubular specimens is lower than the DIF measured by SHPB tests on solid specimens. This paper offers experimental support for a previous publication [Li QM, Meng H. About the dynamic strength enhancement of concrete-like materials in a split Hopkinson pressure bar test. Int J Solids Struct 2003; 40:343–360.], which claimed that inertia-induced radial confinement makes a large contribution to the dynamic compressive strength enhancement of concrete-like materials when the strain-rate is greater than a critical transition strain-rate between 10¹ and 10² s⁻¹. It is concluded that DIF formulae for concrete-like materials measured by split Hopkinson pressure bar tests need to be corrected if they are going to be used as the unconfined uniaxial compressive strength in the design and numerical modelling of structures made from concrete-like materials to resist impact and blast loads.     

Further investigation on the dynamic compressive strength enhancement of concrete-like materials based on split Hopkinson pressure bar tests. Part II: Numerical simulations

Split Hopkinson pressure bar (SHPB) tests have been used widely to measure the dynamic compressive strength of concrete-like materials at high strain-rates between 10¹ and 10³ s⁻¹. It has been shown in companion paper (Zhang M, Wu HJ, Li QM, Huang FL. Further investigation on the dynamic compressive strength enhancement of concrete-like materials based on split Hopkinson pressure bar tests Part I: Experiments. Int J Impact Eng 2009;36(12):1327–1334) that the axial strain acceleration is normally unavoidable in an SHPB test on brittle materials. Axial strain acceleration introduces radial confinement in the SHPB specimens and consequently enhances the compressive strength of concrete-like specimens. This paper employs numerical simulation to further demonstrate that the unexpected radial confinement in an SHPB test is responsible for the increase of the dynamic compressive strength of concrete-like materials at strain-rates from 10¹ to 10³ s⁻¹. It confirms the observations in Zhang et al. (Zhang M, Wu HJ, Li QM, Huang FL. Further investigation on the dynamic compressive strength enhancement of concrete-like materials based on split Hopkinson pressure bar tests Part I: Experiments. Int J Impact Eng 2009;36(12):1327–1334) that the dynamic increase factor (DIF) measured in SHPB tests can be reduced either by using tubular SHPB specimens or by reducing the diameter of the SHPB specimen. A kinetic friction model is proposed based on kinetic friction tests and is implemented in the numerical model. It shows that it is necessary to use a kinetic friction model, rather than a constant friction model, for more accurate numerical simulation of SHPB tests.     

Dynamic mixed-mode I/II delamination fracture and energy release rate of unidirectional graphite/epoxy composites

Mixed-mode open-notch flexure (MONF), anti-symmetric loaded end-notched flexure (MENF) and center-notched flexure (MCNF) specimens were used to investigate dynamic mixed I/II mode delamination fracture using a fracturing split Hopkinson pressure bar (F-SHPB). An expression for dynamic energy release rate G_d is formulated and evaluated. The experimental results show that dynamic delamination increases linearly with mode mixing. At low input energy E_i ? 4.0 J, the dynamic (G_d) and total (G_T) energy rates are independent of mixed-mode ratio. At higher impact energy of 4.0 ? E_i ? 9.3 J, G_d decreases slowly with mixed I/II mode ratio while G_T is observed to increase more rapidly. In general, G_d increases more rapidly with increasing delamination than with increasing energy absorbed. The results show that for the impact energy of 9.3 J before fragmentation of the plate, the effect of kinetic energy is not significant and should be neglected. For the same energy-absorption level, the delamination is greatest at low mixed-mode ratios corresponding to highest Mode II contribution. The results of energy release rates from MONF were compared with mixed-mode bending (MMB) formulation and show some agreement in Mode II but differences in prediction for Mode I. Hackle (Mode II) features on SEM photographs decrease as the impact energy is increased but increase as the Mode I/II ratio decreases. For the same loading conditions, more pure Mode II features are generated on the MCNF specimen fractured surfaces than the MENF and MONF specimens.     

Dynamic compression of cellular cores: temperature and strain rate effects

Cross-linked polyvinyl chloride closed-cell foams were examined under quasi-static and high strain rate compression loading using a servo-hydraulic testing machine and a modified split Hopkinson pressure bar apparatus consisting of polycarbonate bars for strain rates up to 1900 s⁻¹. Three foam densities were examined viz. 75, 130, and 300 kg/m³. Each core density has been subjected to compressive loading at room and elevated temperatures. A reverse trend in failure modes was observed when moving from room to elevated temperatures at high strain loading, which was not found in quasi-static testing at elevated temperatures. Accordingly, post-impact tests were conducted to evaluate the residual strength of the foam cores subject to elevated temperatures and HSR. Results of the post-impact test revealed that the foam cores are still capable of taking some loading. The residual strength of cores was fairly constant regardless of temperature therefore recovery of volume does not signify an increase in residual strength of cores.     

Effect of stitching and weave architecture on the high strain rate compression response of affordable woven carbon/epoxy composites

In this study, experimental investigations on stitched and unstitched woven carbon/epoxy laminates under high strain rate compression loading are discussed. Stitched/unstitched laminates are fabricated with aerospace grade plain and satin weave fabrics with room temperature curing SC-15 epoxy resin using affordable vacuum assisted resin infusion molding process. The samples are subjected to high strain rate loading using modified compression split Hopkinson’s pressure bar at three different strain rates ranging from 320 to 1149 s⁻¹. Results are discussed in terms of unstitched/stitched configuration, fabric type and loading directions. Dynamic compression properties are compared with those of static loading. Failure mechanisms are characterized through optical and scanning microscopy.     

Through-thickness compressive strength of a carbon/epoxy composite laminate

As carbon-fiber-reinforced composite materials are increasingly used for heavy-duty self-lubricating bearings, their through-thickness compressive strength (TTCS) has become an important parameter because the TTCS depends on the weave type and stacking sequence of laminates regardless of their tribological properties.In this work, the TTCS of a carbon/epoxy composite bearing material was measured with respect to weave type, stacking sequence, and direction of cut from the laminate. The tests showed that, for unidirectional laminate, cylindrical specimens resulted in the most reliable data of TTCS. However, for woven fabric laminate, cubic specimens with the edge length greater than twice the repeating unit gave reliable results.     

Through-thickness compressive strength of carbon–phenolic woven composites

Carbon–phenolic woven composites are increasingly employed as the material for the heavy-duty journal bearings. Since the through thickness compressive strength (TTCS) is important for the heavy-duty bearing, in this paper, the effects of lay-up angles and specimen thickness of woven composites on TTCS were investigated for the efficient design of carbon–phenolic woven composite bearings. From the experiments and FEM analysis, it was found that the TTCS of the carbon–phenolic woven composite is much dependent on the stacking sequence rather than composite thickness because different stacking sequence produced much different interlaminar stresses.     

Fracture mechanisms and failure analysis of carbon fibre/toughened epoxy composites subjected to compressive loading

This study investigates the failure mechanisms of unidirectional (UD) HTS40/977-2 toughened resin composites subjected to longitudinal compressive loading. A possible sequence of failure initiation and propagation was proposed based on SEM and optical microscopy observations of failed specimens. The micrographs revealed that the misaligned fibres failed in two points upon reaching maximum micro-bending deformation and two planes of fracture were created to form a kink band. Therefore, fibre microbuckling and fibre kinking models were implemented to predict the compressive strength of UD HTS40/977-2 composite laminate. The analysis identified several parameters that were responsible for the microbuckling and kinking failure mechanisms. The effects of these parameters on the compressive strength of the UD HTS40/977-2 composite systems were discussed. The predicted compressive strength using a newly developed combined modes model showed a very good agreement to the measured value.     

Mechanical properties of ceramic fiber-reinforced concrete under quasi-static and dynamic compression

The research herein is made on the quasi-static and dynamic mechanical properties of ceramic fiber reinforced concrete (CRFRC for short) through the adoption of a hydraulically-driven testing system as well as a 100-mm-diameter split Hopkinson pressure bar (SHPB) system. As test results have turned out, such quasi-static properties as compressive strength, splitting tensile strength and flexural strength of CRFRC increase with the rise in the volume fraction of fiber. Within the strain range of 20–120 s⁻¹, the effect of the axial strain acceleration on the dynamic strength of CRFRC could be ignored. Therefore, the dynamic increase ratio (DIF) derived from SHPB tests can truly reflect the dynamic enhancement of CRFRC. The dynamic strength, critical strain and specific energy absorption (SEA) of CRFRC are sensitive to the strain rate. The addition of ceramic fiber to plain concrete can significantly improve its properties—dynamic strength, critical strain and energy absorption. And also, an analysis is conducted of the mechanism for strengthening and toughening the concrete.     

Improved interfacial properties of carbon fiber/epoxy composites through grafting polyhedral oligomeric silsesquioxane on carbon fiber surface

Carbon fibers were grafted with a layer of uniform octaglycidyldimethylsilyl POSS in an attempt to improve the interfacial properties between carbon fibers and epoxy matrix. Atomic force microscopy (AFM), X-ray photoelectron spectroscopy (XPS) and dynamic contact angle analysis were performed to characterize the carbon fibers. AFM results show that the grafting of POSS significantly increased the carbon fiber surface roughness. XPS indicates that oxygen-containing functional groups obviously increased after modification. Dynamic contact angle analysis shows that the surface energy of modified carbon fibers is much higher than that of the untreated ones. Results of the mechanical property tests show that interlaminar shear strength (ILSS) increased from 68.8 to 90.5 MPa and impact toughness simultaneously increased from 2.62 to 3.59 J.     

High strain rate compression of epoxy based nanocomposites

This work aimed to investigate the strain-rate effect (0.001–3000 s⁻¹) on compressive properties of the highly cross-linked epoxy and the epoxy sample filled with 10 wt% sol-gel-formed silica nanoparticles. As the strain rate increased, the compressive modulus and transition strength of both samples went up distinctly, the strain at break and ultimate strength decreased more or less, while the strain energy at fracture nearly did not change. Adding the sol-gel-formed silica nanoparticles can improve effectively the compressive modulus, transition strength as well as strain energy at fracture of the epoxy polymer owing to their homogeneous dispersion in epoxy matrix.     

Torsion fatigue behavior of unidirectional carbon/epoxy and glass/epoxy composites

This paper presents results of the feasibility of carbon/epoxy composites (CFRP) as a future helicopter flexbeam material. Torsional behaviors of unidirectional CFRP and glass/epoxy composites (GFRP) with the same resin matrix were investigated. The initial torsional rigidity of CFRP was almost identical to that of GFRP. The torsional rigidities calculated using finite element analyses (FEA) agreed with the experimental results: the torsional rigidities are governed mainly by the material’s shear stiffness. Torsion fatigue tests were also conducted by controlling the angle of twist of the sinusoidal wave under a constant tensile axial load. No catastrophic failure occurred with either GFRP or CFRP, although decreased amplitudes of torque and torsional rigidities were observed according to the number of cycles. Results of X-ray CT inspections and numerical calculation by FEA revealed that degradation of a torsional rigidity is caused mainly by splitting crack propagation along the fiber direction. The torsion fatigue life of CFRP was superior to that of GFRP. Consequently, results confirmed that CFRP exhibits excellent properties as a torsional element of a helicopter flexbeam in terms of torsional rigidity and tension–torsion fatigue behaviors.     

Experimental description of thermomechanical properties of carbon fiber-reinforced TiC matrix composites

Titanium carbide ceramic is a good potential material used in high temperature environment for its good strength, erosion resistance and thermal stability. Unfortunately, the low thermal shock resistance and low fracture toughness are the well-known impediments to its application as high temperature structure components. In order to extend the application of TiC ceramics at high temperature, 20 vol.% short carbon fiber was added into TiC matrix to improve the thermomechanical properties. With the incorporation of carbon fiber, the thermal expansion coefficient of TiC composites was decreased and the thermal conductivity was increased slightly below 900 °C. The flexural strength was improved from 471 MPa for monolithic TiC to 593 MPa for TiC composites, and the strengthening effect of carbon fiber became more prominent at high temperatures. The addition of fiber decreased the elastic modulus of TiC composite. The elastic modulus of the composite decreased with increasing temperature. The improvement of high temperature strength and thermal conductivity and the decrease of thermal expansion will benefit the application of TiC composites in high temperature environment where the temperature usually varies.     

Using split Hopkinson pressure bars to perform large strain compression tests on polyurea at low,intermediate and high strain rates

The strain rate sensitivity of polyurea is characterized using a modified split Hopkinson pressure bar (SHPB) system. The device is composed of a hydraulic piston along with nylon input and output bars. In combination with an advanced wave deconvolution method, the modified SHPB system provides an unlimited measurement time and thus can be used to perform experiments at low, intermediate and high strain rates. A series of compression tests of polyurea is performed using the modified SHPB system. In addition, conventional SHPB systems as well as a universal hydraulic testing machine are employed to confirm the validity of the modified SHBP technique at low and high strain rates. The analysis of the data at intermediate strain rates shows that the strain rate is not constant due to multiple wave reflections within the input and output bars. It is demonstrated that intermediate strain rate SHPB experiments require either very long bars (>20 m) or very short bars (<0.5 m) in order to achieve an approximately constant strain rate throughout the entire experiment.     

复合材料层间应变测试实验

复合材料受到应力作用层间会产生变形,应力过大层间会出现撕裂的现象。针对这一问题, 利用光纤法珀应变传感器与复合材料层间间隙尺寸相当的特点,将该传感器置入复合材料层间,在万能拉伸仪上进行复合材料应变测试实验。实验表明:利用光纤法珀应变传感器检测复合材料层间应变的方法是完全可行的。     

单壁碳纳米管无纺布/环氧树脂复合材料的电磁屏蔽性能

采用一种导电材料预制体-单壁碳纳米管(Single-wall carbon nanotube,SWCNT)无纺布与环氧树脂复合制备了电磁屏蔽复合材料,并对所制复合材料的电磁屏蔽性能进行了表征。结果表明:所制复合材料对电磁波的屏蔽效率随SWCNT无纺布厚度的增加而增加。在较低的SWCNT无纺布填加量下所制复合材料可以实现对低频电磁波较高的屏蔽效率。不同于填加粉体导电材料所制电磁屏蔽复合材料,作为导电材料预制体使用的SWCNT无纺布是一个独立的整体导电薄膜,可以直接引入到基体当中,不存在分散问题。并且通过简单的导电预制体多层叠加的方式即可实现复合材料更高的屏蔽效率。