冷轧薄板表面斑迹缺陷的控制

正在钢铁产品中,冷轧板对表面质量的要求非常严格,表面缺陷是冷轧板最主要的质量问题,一旦冷轧板出现表面缺陷,就会严重影响后续深加工的产品质量和性能。马鞍山钢铁股份有限公司第一钢轧总厂冷轧产品曾经在一段时间内饱受表面斑迹缺陷困扰,给一钢轧产品乃至马钢产品在市场的形象带     

Fe-6.5%Si钢极薄带的试制

 为了研究Fe-6.5%Si钢极薄带的制备工艺,并获得良好的产品磁性能,以薄带铸轧试验机制备的6.5%Si钢铸带为原料,分别采用一次温轧法、二次温轧法和基于应变诱导无序(DID)原理的高硅钢室温冷轧3种工艺制备出厚度为0.1 mm的Fe-6.5%Si钢。分析结果显示,一次温轧法退火后以高强度γ织构为主,由于压下率达到90%,形变储能高,晶粒尺寸最大,铁损最低,同时磁感也最低;二次温轧的退火板除了γ织构外,还有较强的η织构,故其磁感值高于一次温轧法,该方法得到的6.5%Si钢薄带综合磁性能最优,但生产成本高,效率低;基于DID原理,对6.5%Si钢热轧板在温度为300～450 ℃、压下率为45%～65%的条件下进行温轧,实现了6.5%Si钢软化,随后可将6.5%Si钢室温冷轧至0.1 mm,此时温轧板和冷轧板内部有序相消失,基体变成无序态;室温冷轧板退火后晶粒更细,铁损略有升高。此外,室温冷轧可促进{111}<112>形变晶粒在冷轧剪切带中形核形成有利织构,因此磁感值得到更大提升;采用DID原理进行室温冷轧,效率较高,后续可通过优化退火工艺使其进一步降低铁损,该方法为薄带铸轧工艺批量生产磁性能优异的6.5%Si钢极薄带提供技术参考。     

冷轧薄板表面斑迹缺陷的控制

正在钢铁产品中,冷轧板对表面质量的要求非常严格,表面缺陷是冷轧板最主要的质量问题,一旦冷轧板出现表面缺陷,就会严重影响后续深加工的产品质量和性能。马鞍山钢铁股份有限公司第一钢轧总厂冷轧产品曾经在一段时间内饱受表面斑迹缺陷困扰,给一钢轧产品乃至马钢产品在市场的形象带来极为不利的影响,并且造成巨大经济损失。仅2011年6月至2012年4月,一钢轧冷轧成品就因质量问题赔付21 417 t,其中表面斑迹缺陷质量问题占总的质量问题的近三分之一,成为一个亟待解决的     

TC1钛合金宽幅薄板轧制工艺研究

对比分析了包覆叠轧和冷轧两种工艺制备TC1钛合金宽幅薄板表面质量、组织形貌和力学性能,并研究了成品退火温度对冷轧板材力学性能和组织的影响。结果表明:这两种工艺生产的TC1钛合金薄板力学性能均可满足GJB 2505A—2008要求,冷轧工艺生产的TC1钛合金成品板材表面质量良好,性能稳定,晶粒更为细小;冷轧板材成品退火温度控制在550~580℃较为适宜。     

轧制方式对SUS430铁素体不锈钢组织和性能的影响

 采用X射线衍射技术和光学显微分析等方法,研究了同步和异步冷轧方式对SUS430铁素体不锈钢微观组织、织构演变以及力学和成形性能的影响。结果表明,与同步冷轧相比,由于异步轧制剪切变形的引入,可使异步冷轧板材的平均晶粒尺寸减小。在同步冷轧过程中,其二次冷轧再结晶织构为完整的γ纤维织构,导致铁素体不锈钢的最终性能优于同步一次冷轧;而在异步冷轧过程中,异步一次冷轧再结晶织构为强点{111}<[1][1]2>的γ纤维织构,异步二次冷轧再结晶织构属于随机取向织构,其结果是异步一次冷轧板材的性能优于异步二次冷轧。综合分析表明,与异步二次冷轧方式相比,同步二次冷轧方式有利于铁素体不锈钢性能的提高。     

冷轧工艺对00Cr21MoNbTi铁素体不锈钢组织、织构与成形性能的影响

利用电子背散射衍射技术(EBSD)研究了冷轧轧程和冷轧压下率对00Cr21MoNbTi铁素体不锈钢的组织、织构与成形性能的影响.结果表明:随轧程数的增加,再结晶晶粒尺寸变化不大,但材料的平均r值相应提高;相同两轧程条件下,随累计压下率增大,材料的再结晶晶粒尺寸细化,平均r值以及{111}织构组分含量提高.再结晶织构峰值...     

一次轧程高硬度酒精罐用镀铬板的开发

某生产厂此前采用二次冷轧轧程生产镀铬用二次冷轧材,为降低生产成本,提高产线效率,推荐客户选取适宜原材料进行试验。通过优化冷轧、退火、平整工艺后,成功开发DR8酒精罐用镀铬板,产品性能满足要求。达到了采用一次轧程代替二次轧程生产的目的,生产效率提高一倍,成材率提高了1%,生产成本大幅度降低。     

再结晶晶粒取向分布对铁索体不锈钢起皱的影响

针对铁素体不锈钢拉伸后的表面起皱现象,研究了再结晶晶粒取向分布对起皱程度的影响.将厚度3mm的430铁素体不锈钢热轧退火板,经2种工艺(一次冷轧、多次冷轧)轧制和再结晶退火后得到最终厚度均为0.1mm的冷轧板,分析了再结晶晶粒取向、轴向拉伸后表面起皱程度以及二者的相关性.结果表明,{211)〈011〉和{100}〈011〉取向晶粒的存在是引起表面起皱的内因;铁素体不锈钢中各个晶粒取向均匀分布,削弱了塑性各向异性,从而抑制起皱的产生.铁素体不锈钢在拉伸变形后,相近取向的相邻晶粒表面呈现单滑移痕迹,这是形成起皱的主要原因.多次冷轧-中间退火为减轻铁素体不锈钢表面起皱提供了一种新途径.     

受热不均匀对低碳钢SAE1010板材组织及成形性能的影响

为了研究退火过程受热不均匀对板材组织及成形性能的影响规律,对热轧态SAE1010低碳钢板进行冷轧及连续退火,分析热轧态、冷硬态及退火态钢板边部和芯部的显微组织,分别对退火态钢板边部和芯部试样进行拉伸和折弯试验。结果表明,热轧态试样少量岛状珠光体分布在铁素体晶界处,边部组织晶粒尺寸小于芯部,珠光体中部分片层渗碳体退化为球状。冷硬态板材组织沿轧制方向呈现明显的晶粒破碎特征,退火态边部组织存在较多的大晶粒和粒状渗碳体团,芯部组织较为均匀细小。退火态板材芯部材料伸长率高于边部而强度低于边部,经180°折弯后芯部钢板无开裂而边部出现裂纹。退火温度均匀性对于SAE1010低碳钢板组织和性能具有重要的影响。     

20CrMnTiH圆钢精轧后控冷过程温度场有限元分析

通过对20CrMnTiH圆钢精轧后控制冷却过程温度场进行有限元模拟以及现场温度实测,得出了Φ35 mm规格圆钢芯部、1/2半径处和表层温度的分布曲线。分析说明,轧后水冷却过程圆钢表层温度急速下降,而芯部温度下降缓慢,水冷时圆钢芯部与表面的最大温差约为115℃;水冷后的空冷过程使得圆钢芯部和表层温度逐渐一致。20CrMnTiH圆钢精轧后采用快速水冷并配合空冷工艺,有利于抑制奥氏体晶粒长大并获得均匀细小的轧材组织。     

Evolution of Through-Thickness Texture in Ultra Purified 17%Cr Ferritic Stainless Steels

 Texture inhomogeneity usually takes place in ferritic stainless steels due to the lack of phase transformation and recrystallization during hot strip rolling, which can deteriorate the formability of final sheets. In order to work out the way of weakening texture inhomogeneity, conventional hot rolling and warm rolling processes have been carried out with an ultra purified ferritic stainless steel. The results showed that the evolution of through-thickness texture is closely dependent on rolling process, especially for the texture in the center layer. For both conventional and warm rolling processes, shear texture components were formed in the surface layers after hot rolling and annealing; sharp α-fiber and weak γ-fiber with the major component at {111}<110> were developed in both cold rolled sheet surfaces, leading to the formation of inhomogeneous γ-fiber dominated by {111}<112> after recrystallization annealing. In the center layer of conventional rolled and annealed bands, strong α-fiber and weak γ-fiber textures were formed; the cold rolled textures were comprised of sharp α-fiber and weak γ-fiber with the major component at {111}<110>, and inhomogeneous γ-fiber dominated by {111}<112> was formed after recrystallization annealing. By contrast, in the centre layer of warm rolled bands, the texture was comprised of weak α-fiber and sharp γ-fiber, and γ-fiber became the only component after annealing. The cold rolled texture displayed a sharp γ-fiber with the major component at {111}<112> and the intensity of γ-fiber close to that of α-fiber, resulting in the formation of a nearly homogeneous γ-fiber recrystallization texture in the center layer of the final sheet.     

摩擦对IF钢铁素体区热轧和退火织构的影响

采用X射线衍射仪分析IF钢铁素体区热轧织构以及退火织构的演化,在实验室热轧机上进行了IF钢的铁素体区热轧,研究了摩擦对IF钢铁素体区热轧、退火织构的影响。结果表明：无润滑轧制时,钢板表层形成强高斯织构组分{110}〈001〉,弱γ纤维织构,导致再结晶织构中高斯组分强度高,γ纤维织构强度低;润滑轧制时,钢板表层高斯织构组分强度降低,{100}〈011〉、γ纤维织构强度提高,退火后γ纤维织构强度提高。钢板中心受摩擦作用影响较小,轧制过程中发展为较强的α和γ纤维织构,退火后γ纤维织构成为主要织构组分。     

Effects of Rolling Parameters on Texture and Formability of High Strength Ultra-Low Carbon BH Steel

 The effects of hot rolling and cold rolling parameters on texture and r (plastic strain ratio) value of high strength ultra low carbon bake hardening (ULC-BH) steels are studied with orientation distribution function (ODF) structural analysis method. After hot rolling, the high strength ULC-BH steel sheet has weak γ-fiber with uniform orientation distributions, and weak α-fiber, of which {445}<110> component forms a high intensity peak at coiling temperature of 750 ℃. After cold rolling, both {111}<110>-{111}<112> intensity on the γ-fiber and {111}-{112}<110> intensity on the α-fiber enhanced. As a result of substitutional solute elements Mn and P being added to the steel, strong {112}<110> deformation texture component is observed on α-fiber, especially at 80% cold rolling reduction, and this leads to the strong {111}<112> recrystallization texture after annealing. The increase of cold rolling reduction shifts the maximum intensity on the γ-fiber from {111}<112> to {111}<113>. After annealing, a very strong γ-fiber is obtained, with intensity peak at {111}<112> component when cold rolling reduction reaches 80%. Increasing coiling temperature and cold rolling reduction improve γ-fiber intensity and r value, resulting in good deep drawability.     

CSP流程试制50W270高牌号无取向硅钢织构的演变

研究了CSP流程试制50W270高牌号无取向硅钢热轧→常化→冷轧→退火过程中织构的演变.利用电子背散射衍射技术对全流程织构进行测量和分析.发现热轧板织构在厚度方向上存在较大差异,表层主要为铜型、黄铜和高斯织构,1/4层存在微弱的高斯织构和旋转立方织构,中心层以γ纤维织构和旋转立方织构为主,还含有较弱的α纤维织构.与热轧板相比,常化板表层和1/4层织构变化不大,中心层旋转立方织构和α纤维织构增强.冷轧板各层均具有α纤维织构和γ纤维织构.与冷轧板相比,成品板各层中α纤维织构基本消失,还出现了立方织构和高斯织构.      

铌对低温取向硅钢初次再结晶行为的影响

以含铌取向硅钢铸坯低温加热制备高磁感取向硅钢为研究目标,通过研究铌对低温取向硅钢初次再结晶行为的影响,达到获得有利于二次再结晶发展的初次再结晶组织目的,采用OM和EBSD技术主要对比了 0.055％铌和不含铌对低温取向硅钢中间退火板的初次再结晶组织、织构和晶界特征的影响.结果表明,铌的加入,使硅钢基体中形成了细小弥散的...     

中温含铜取向硅钢的形变和再结晶织构特征

通过对比中温含铜取向硅钢与普通取向硅钢和高磁感取向硅钢的组织和织构特征,分析中温含铜取向硅钢独特的织构演变规律及其对二次再结晶行为的影响.结果表明,为了获得有利于高斯晶粒长大的强γ取向线织构,中温含铜钢需经过回复退火处理和高温退火阶段慢速升温.回复过程中γ取向线晶粒储能降低,同时慢速升温有利于γ取向线晶粒的形核和再结晶.中温含铜钢的二次再结晶开始温度超过1000℃,由于初次再结晶晶粒组织以γ织构为主且非γ取向线晶粒较少,导致最终二次晶粒尺寸超大且晶界圆滑,二次再结晶机理以择优长大为主导,超大的二次晶粒尺寸导致最终成品的铁损升高,但通过激光刻痕处理后,整体铁损的降低效果比二次晶粒较小的高磁感取向硅钢更加显著.      

Microtexture Evolution and Grain Boundary Character Distribution of Interstitial-Free Steels With Moderate Levels of Cold Rolling Reductions

High-strength interstitial-free steel sheets have very good deep drawability when processed to have {111} recrystallization texture. The microtexture evolution and grain boundary character distribution of interstitial-free steels as a function of moderate levels of cold rolling reductions were investigated by the metallographic microscopy and electron backscatter diffraction technique. The results showed that there was a close relationship between microtexture and grain boundary character distribution for interstitial-free steel, especially the distribution and features of some specific types of coincident-site lattice boundaries. In addition, α-fiber texture was weakened to vanish while γ-fiber texture strengthened gradually as cold rolling reduction was increased from 20% to 75% for cold rolled and annealed samples. Accordingly, increasing the rolling reduction from 20% to 75% would lead to a significant increase in the proportion of Σ3 boundaries. Also, it was found that the microtexture of 20% cold rolled sample would induce a high frequency of Σ11 grain boundaries, but the microtexture of 75% cold rolled sample would produce more Σ7 and Σ17 grain boundaries. It was suggested that texture played a significant role in the formation of grain boundary character distribution.     

Recrystallization and grain growth of cold-rolled gold sheet

Recrystallization and grain growth of a cold-rolled gold sheet with 98 pct reduction in area (RA) were investigated with electron backscatter diffraction (EBSD) and X-ray diffraction (XRD). Gold with some dopants (Be, Ca, and La) was used in this research and its recrystallization temperature was 320 °C. Isothermal annealing experiments at 400 °C, 500 °C, and 600 °C were carried out for the cold-rolled gold sheet, and recrystallization texture was examined. In the cold-rolled gold sheet, α- and β-fibers were measured mainly and some shear texture components were found on the surface. Shear texture components remained on the surface for 2 hours at 400 °C and were consumed by other recrystallized grains after 24 hours at 400 °C. Microstructure and texture evolution during in-situ annealing at 400 °C were investigated from the cold-rolled state to the fully recrystallized state using EBSD. Most of the newly, recrystallized grains came from the deformed β-fiber regions and consisted of β-fiber, cube, and other random orientations.