Boiling of water and FC-72 in microchannels enhanced with novel features

A microchannel test section comprised of parallel square microchannels with a 25 × 25 μm and 50 × 50 μm cross section was manufactured. Boiling of perfluorinated dielectric fluid FC-72 and water in microchannels was studied. Troublesome occurrences associated with flow boiling in microchannels were reduced or eliminated with inlet/outlet restrictors, inlet/outlet manifolds and potential nucleation cavities incorporated in the array of microchannels. The gradual reduction of channel cross section in the manifolds ensured a uniform distribution of the working fluid among the microchannels. The flow restrictors provided a higher upstream pressure drop in comparison with the downstream pressure drop which favors vapor flow in the downstream direction and consequentially suppresses the vapor backflow present in flow boiling. The superheat of the microchannel wall necessary for the onset of boiling was decreased significantly with the incorporation of properly sized artificial cavities. Experimental results confirmed the benefits of the etched features, as there was (i) an even working fluid distribution (ii) without dominating backflows of vapor (iii) at a low temperature of the onset of boiling. Bubble growths as well as other events in the microchannels were visualized with a high-speed imaging system which captured images at over 87,000 frames per second. Results exhibit boiling hysteresis dependence of the working fluid and its mass flux through the microchannels. The temperature of the onset of boiling is highly dependent on the working fluid, microchannel size and its roughness.     

Microchannel size effects on local flow boiling heat transfer to a dielectric fluid

Heat transfer with liquid–vapor phase change in microchannels can support very high heat fluxes for use in applications such as the thermal management of high-performance electronics. However, the effects of channel cross-sectional dimensions on the two-phase heat transfer coefficient and pressure drop have not been investigated extensively. In the present work, experiments are conducted to investigate the local flow boiling heat transfer of a dielectric fluid, Fluorinert FC-77, in microchannel heat sinks. Experiments are performed for mass fluxes ranging from 250 to 1600 kg/m² s. Seven different test pieces made from silicon and consisting of parallel microchannels with nominal widths ranging from 100 to 5850 μm, all with a nominal depth of 400 μm, are considered. An array of temperature sensors on the substrate allows for resolution of local temperatures and heat transfer coefficients. The results of this study show that for microchannels of width 400 μm and greater, the heat transfer coefficients corresponding to a fixed wall heat flux as well as the boiling curves are independent of channel size. Also, heat transfer coefficients and boiling curves are independent of mass flux in the nucleate boiling region for a fixed channel size, but are affected by mass flux as convective boiling dominates. A strong dependence of pressure drop on both channel size and mass flux is observed. The experimental results are compared to predictions from a number of existing correlations for both pool boiling and flow boiling heat transfer.     

Correlation of critical heat flux and two-phase friction factor for subcooled convective boiling in structured surface microchannels

Critical heat flux (CHF) and pressure drop of subcooled flow boiling are measured for a microchannel heat sink containing 75 parallel 100 μm × 200 μm structured surface channels. The heated surface is made of a Cu metal sheet with/without 2 μm thickness diamond film. Tests and measurements are conducted with de-ionized water, de-ionized water +1 vol.% MCNT additive solution, and FC-72 fluids over a mass velocity range of 820–1600 kg/m² s, with inlet temperatures of 15(8.6)°C, 25(13.6)°C, 44(24.6)°C, and 64(36.6)°C for DI water (FC-72), and heat fluxes up to 600 W/cm². The CHF of subcooled flow boiling of the test fluids in the microchannels is measured parametrically. The two-phase pressure drop is also measured. Both CHF and the two-phase friction factor correlation for one-side heating with two other side-structured surface microchannels are proposed and developed in terms of the relevant parameters.     

Local heat transfer distribution and effect of instabilities during flow boiling in a silicon microchannel heat sink

Flow boiling of the perfluorinated dielectric fluid FC-77 in a silicon microchannel heat sink is investigated. The heat sink contains 60 parallel microchannels each of 100 μm width and 389 μm depth. Twenty-five evenly distributed temperature sensors in the substrate yield local heat transfer coefficients. The pressure drop across the channels is also measured. Experiments are conducted at five flow rates through the heat sink in the range of 20–80 ml/min with the inlet subcooling held at 26 K in all the tests. At each flow rate, the uniform heat input to the substrate is increased in steps so that the fluid experiences flow regimes from single-phase liquid flow to the occurrence of critical heat flux (CHF). In the upstream region of the channels, the flow develops from single-phase liquid flow at low heat fluxes to pulsating two-phase flow at high heat fluxes during flow instability that commences at a threshold heat flux in the range of 30.5–62.3 W/cm² depending on the flow rate. In the downstream region, progressive flow patterns from bubbly flow, slug flow, elongated bubbles or annular flow, alternating wispy-annular and churn flow, and wall dryout at highest heat fluxes are observed. As a result, the heat transfer coefficients in the downstream region experience substantial variations over the entire heat flux range, based on which five distinct boiling regimes are identified. In contrast, the heat transfer coefficient midway along the channels remains relatively constant over the heat flux range tested. Due to changes in flow patterns during flow instability, the heat transfer is enhanced both in the downstream region (prior to extended wall dryout) and in the upstream region. A previous study by the authors found no effect of instabilities during flow boiling in a heat sink with larger microchannels (each 300 μm wide and 389 μm deep); it appears therefore that the effect of instabilities on heat transfer is amplified in smaller-sized channels. While CHF increases with increasing flow rate, the pressure drop across the channels has only a minimal dependence on flow rate once boiling is initiated in the microchannels, and varies almost linearly with increasing heat flux.     

Unstable and stable flow boiling in parallel microchannels and in a single microchannel

A simultaneous visualization and measurement study have been carried out to investigate flow boiling instabilities of water in microchannels at various heat fluxes and mass fluxes. Two separate flow boiling experiments were conducted in eight parallel silicon microchannels (with flow interaction from neighboring channels at headers) and in a single microchannel (without flow interaction), respectively. These microchannels, at a length of 30 mm, had an identical trapezoidal cross-section with a hydraulic diameter of 186 μm. At a given heat flux and inlet water temperature, it was found that stable and unstable flow boiling regimes existed, depending on the mass flux. A flow boiling map, in terms of heat flux vs mass flux, showing stable flow boiling regime and unstable flow boiling regime is presented for parallel microchannels as well as for a single microchannel, respectively, at an inlet water temperature of 35 °C. In the stable flow boiling regime, isolated bubbles were generated and were pushed away by the incoming subcooled liquid. Two unstable flow boiling regimes, with long-period oscillation (more than 1 s) and short-period oscillation (less than 0.1 s) in temperature and pressure, were identified. The former was due to the expansion of vapor bubble from downstream while the latter was owing to the flow pattern transition from annular to mist flow. A comparison of results of flow boiling in parallel microchannels and in a single microchannel shows that flow interaction effects from neighboring channels at the headers are significant.     

Flow pattern transition instability during flow boiling in a single microchannel

We studied the unique characteristics of flow boiling in a single microchannel, including the periodic pressure drop, mass flow rate, and temperature fluctuations, in terms of a long time period. Experiments were conducted using a single horizontal microchannel and deionized water to study boiling instabilities at very small mass and heat flow rate conditions. A Polydimethylsiloxane (PDMS) rectangular single microchannel had a hydraulic diameter of 103.5 μm and a length of 40 mm. A series of piecewise serpentine platinum microheaters were fabricated on the inner bottom wall of the rectangular microchannel to supply thermal energy to the test fluid. Real-time flow visualizations of the flow pattern inside the microchannel were performed simultaneously with measurements of the experimental parameters. Tests were performed for mass fluxes of 170 and 360 kg/m² s and heat fluxes of 200–530 kW/m². The test results showed that the heated wall temperature, pressure drop, and mass flux all fluctuated with a long period and large amplitude. These periodic fluctuations exactly matched the transition of two alternating flow patterns inside the microchannel: a bubbly/slug flow and an elongated slug/semi-annular flow. Therefore, the flow pattern transition instability in the single microchannel caused a cyclic behavior of the wall temperature, pressure drop, and mass flux, and this behavior had a very long period (100–200 s) and large amplitude.     

Adiabatic two-phase flow in rectangular microchannels with different aspect ratios: Part I – Flow pattern,pressure drop and void fraction

An aspect ratio is an important parameter for two-phase flow in a rectangular microchannel. To study the aspect ratio effect on the flow pattern, pressure drop and void fraction, experiments of adiabatic liquid water and nitrogen gas two-phase flow in rectangular microchannels were conducted. The widths and heights of rectangular microchannels are 510 μm × 470 μm, 608 μm × 410 μm, 501 μm × 237 μm and 503 μm × 85 μm. Therefore, the aspect ratios of the rectangular microchannels are 0.92, 0.67, 0.47 and 0.16; and the hydraulic diameters of the rectangular microchannels were 490, 490, 322 and 143 μm, respectively. Experimental ranges were liquid superficial velocities of 0.06–1.0 m/s and gas superficial velocities of 0.06–71 m/s. Visible rectangular microchannels were fabricated using a photosensitive glass. And pressure drop in microchannels was directly measured through embedded ports. The visualization of the flow pattern was carried out with a high-speed camera and a long distance microscope. Typical flow patterns in the rectangular microchannels observed in this study were bubble flow, transitional flow (multiple flow) and liquid ring flow. As the aspect ratio decreased, the bubble flow regime became dominant due to the confinement effect and the thickness of liquid film in corner was decreased. A void fraction in the rectangular microchannels has a linear relation with the volumetric quality. And the two-phase flow becomes homogeneous with decreasing aspect ratio owing to the reduction of the liquid film thickness. Like Zhang et al.’s [19] correlation, as the confinement number increased, the C-value in Lockhart and Martinelli correlation decreased. And a frictional pressure drop in the rectangular microchannels was highly related with the flow pattern.     

Hydrodynamics and heat transfer during flow boiling instabilities in a single microchannel

Boiling in microchannels is widely considered as one of the front runners in process intensification heat removal. Flow boiling heat transfer in microchannel geometry and the associated flow instabilities are not well understood, further research is necessary into the flow instabilities adverse effect on heat transfer.Boiling is induced in microchannel geometry (hydraulic diameter 727 μm) to investigate several flow instabilities. A transparent, metallic, conductive deposit has been developed on the exterior of rectangular microchannels, allowing simultaneous heating and visualisation.Presented in this paper is data for a particular case with a uniform heat flux of 4.26 kW/m² applied to the microchannel and inlet liquid mass flowrate, held constant at 1.13 × 10^?5 kg/s. In conjunction with obtaining high-speed images, a sensitive infrared camera is used to record the temperature profiles on the exterior wall of the microchannel, and a data acquisition system is used to record the pressure fluctuations over time. Various phenomena are apparent during the flow instabilities; these can be characterised into timescales occurring at 100’s seconds, 10’s seconds, several seconds and finally milliseconds. Correlation of pressure oscillations with temperature fluctuations as a function of the heat flux applied to the microchannel is possible.From analysis of our results, images and video sequences with the corresponding physical data obtained, it is possible to follow simultaneously particular flow, pressure and temperature conditions leading to nucleate boiling, flow instabilities and transition regimes during flow boiling in a microchannel. The investigation allowed us to quantify and characterise the timescales of various observed instabilities during flow boiling in a microchannel. High speed imaging revealed some of the controlling physical mechanisms responsible for the observed instabilities.     

Fluid flow and convective heat transfer in flat microchannels

This study investigates the design, construction and instrumentation of an experimental microchannel, with a rectangular cross-section and large aspect ratio, that allows characterization of the flow and convective heat transfer under well defined and precise conditions and makes it possible to vary the hydraulic diameter of the microchannel. The flow friction coefficient is estimated by direct pressure drop measurements inside the microchannel in a zone where the flow is fully developed. Since the wall thermal conditions inside the microchannel can not be measured directly, their estimation requires temperature measurements in the wall thickness and an inverse heat conduction method. The thermal and hydrodynamic results obtained by varying the hydraulic diameter between 1 mm and 100 μm do not deviate from the theory or empirical correlations for large-scale channels. These results let us confirm that for smooth walls the continuum mechanics laws for convection and fluid mechanics remain valid in microchannels of hydraulic diameter greater than or equal to 100 μm.     

Experimental investigation and flow visualization to determine the optimum dimension range of microgap heat sinks

The rapid increase of heat flux in high performance electronic devices has necessitated the development of high capacity thermal management techniques that can support extremely high heat transfer rates. Flow boiling in microgap is very promising for this purpose due to its high heat transfer rate and ease of fabrication. However, the effects of microgap dimension on heat transfer and pressure drop characteristics along with flow visualization have not been investigated extensively. This paper focuses on flow boiling experiments of deionized water in silicon microgap heat sink for ten different microgap dimensions from a range of 80 μm–1000 μm to determine the most effective and efficient range of microgap dimensions based on heat transfer and pressure drop performance. High speed flow visualization is conducted simultaneously along with experiments to illustrate the bubble characteristics in the boiling flow in microgap. The results of this study show that confinement in flow boiling occurs for microgap sizes 500 μm and below and confined slug/annular flow is the main dominant regime whereas physical confinement does not occur for microgap sizes 700 μm and above and bubbly flow is the dominant flow regime. The microgap is ineffective below 100 μm as partial dryout strikes very early and the wall temperature is much higher for a fixed heat flux as microgap size increases above 500 μm. In addition, results show that pressure drop and pressure fluctuation decrease with the increases of gap size whereas wall temperature and wall temperature fluctuation increase with the increases of gap size. A strong dependence of heat transfer coefficient on microgap sizes is observed for microgap sizes 500 μm and below. However, the heat transfer coefficient is independent of microgap size for microgap sizes 700 μm and above.     

Nanofluid stabilizes and enhances convective boiling heat transfer in a single microchannel

The flow boiling heat transfer in a single microchannel was investigated with pure water and nanofluid as the working fluids. The microchannel had a size of 7500 × 100 × 250 μm, which was formed by two pyrex glasses and a silicon wafer. A platinum film with a length of 3500 μm and a width of 80 μm was deposited at the bottom channel surface, acting as the heater and temperature sensor. The nanofluid had a low weight concentration of 0.2%, consisting of de-ionized water and 40 nm Al₂O₃ nanoparticles. The nanoparticle deposition phenomenon was not observed. The boiling flow displays chaotic behavior due to the random bubble coalescence and breakup in the milliseconds timescale at moderate heat fluxes for pure water. The flow instability with large oscillation amplitudes and long cycle periods was observed with further increases in heat fluxes. The flow patterns are switched between the elongated bubbles and isolated miniature bubbles in the timescale of 100 s. It is found that nanofluid significantly mitigate the flow instability without nanoparticle deposition effect. The boiling flow is always stable or quasi-stable with significantly reduced pressure drop and enhanced heat transfer. Miniature bubbles are the major flow pattern in the microchannel. Elongated bubbles temporarily appear in the milliseconds timescale but isolated miniature bubbles will occupy the channel shortly. The decreased surface tension force acting on the bubble accounts for the smaller bubble size before the bubble departure. The inhibition of the dry patch development by the structural disjoining pressure, and the enlarged percentage of liquid film evaporation heat transfer region with nanoparticles, may account for the heat transfer enhancement compared to pure water.     

An experimental investigation on pressure drop of steam condensing in silicon microchannels

Experiments are carried out to study the two-phase pressure drop for water vapor condensation in four smooth trapezoidal silicon microchannels having hydraulic diameters of 109 μm, 142 μm, 151 μm, and 259 μm, respectively. It is found that two-phase frictional pressure drops in the microchannels are greatly influenced by the hydraulic diameter, mass flux and vapor quality. The two-phase pressure drop data in microchannels are compared with existing correlations for macro- and mini-channels based on the homogenous model and the separated flow model to determine their applicability to condensing flows in microchannels. A modified correlation for the Matinelli–Chisholm constant, taking into consideration of surface tension and diameter effects, is developed in the form of the Lockhart–Martinelli correlation for the pressure drop in steam condensation in microchannels. The resulting condensation pressure drop correlation equation is within ±15% of the experimental data.     

A four-zone model for saturated flow boiling in a microchannel of rectangular cross-section

A four-zone flow boiling model is presented to describe saturated flow boiling heat transfer mechanisms in a microchannel of rectangular cross-section. The boiling process in the microchannel is assumed to be a cyclic passage of four zones: (i) liquid-slug zone, (ii) elongated bubble zone, (iii) partially-dryout zone, and (iv) fully-dryout zone. The existence of the partially-dryout zone in this model is proposed to take into consideration of corner effects on boiling heat transfer in the microchannel. To verify this new model, an experimental study was carried out to investigate flow boiling heat transfer of water in a microchannel having a rectangular cross-section with a hydraulic diameter of 137 μm (202 μm in width and 104 μm in depth) with a length of 30 mm under three-side heating condition. The data for bubble nucleation frequency was correlated in terms of the Boiling number, which was used to determine the heat transfer coefficient. It is found that the present four-zone flow boiling model successfully predicts trends of boiling heat transfer data in a microchannel with a rectangular cross-section, having a sharp peak at low vapor quality depending on the mass flow rate. The predictions of flow boiling heat transfer coefficient in the microchannel are found in good agreement with experimental data with a MAE of 13.9%.     

Visualization of convective boiling heat transfer in single microchannels with different shaped cross-sections

Convective boiling in transparent single microchannels with similar hydraulic diameters but different shaped cross-sections was visualized, along with simultaneous measurement of the local heat transfer coefficient. Two types of microchannels were tested: a circular Pyrex glass microtube (210 μm inner diameter) and a square Pyrex glass microchannel (214 μm hydraulic diameter). A 100-nm-thick semi-transparent ITO/Ag thin film sputtered on the outer wall of the microchannel was used for direct joule heating of the microchannel.The flow field visualization showed semi-periodic variation in the flow patterns in both the square and circular microchannels. Such variation was because the confined space limited the bubble growth in the radial direction.In the square microchannel, both the number of nucleation bubbles and the local heat transfer coefficient increased with decreasing vapor quality. The corners acted as active nucleation cavities, leading to the higher local heat transfer coefficient. In contrast, lack of cavities in the smooth glass circular microchannel yielded a relatively smaller heat transfer coefficient at lower vapor quality. Finally, the heat transfer coefficient was higher for the square microchannel because corners in the square microchannel acted as effective active nucleation sites.     

Visualization of flow patterns and bubble behavior during flow boiling in open microchannels

Flow boiling in microchannels is favored by the heat transfer community due to the high heat transfer rates that can be obtained with lower mass flow rates. However, the heat transfer rates for flow boiling in microchannels are impacted by flow reversals and flow instabilities. An open microchannel structure was recently proposed to reduce the impact of the flow boiling instabilities. Subcooled flow boiling experiments were conducted in open microchannels using deionized water. The open microchannels had 6 parallel channels with a 0.3 mm uniform thickness gap above them The channels were fabricated on a 6 mm × 40 mm copper block. The channels were 0.5 mm wide and 0.3 mm deep with 0.43 mm wide fins between them. Flow visualizations were performed with a high-speed CCD camera with the results showing that the flow regimes in the open microchannels differ from those in closed microchannels with stratified flow and no flow instability. Two types of confined bubbles were observed with characterizations of the effects of the bubbles on each other. The heat transfer mechanisms for flow boiling in open microchannels are also described.     

Friction factor and heat transfer in multiple microchannels with uniform flow distribution

Predictions of flow and heat transfer in microchannels are ongoing issues in microfludics. This work focused on laminar flow (69 < Re < 800) within rectangular microchannel with hydraulic diameter from 106 μm to 307 μm for single-phase liquid flow. The friction factors obtained by experiments on the microchannels showed that conventional theory for fully-developed flow is applicable within the range of our experiments. A manifold configuration which ensured uniform flow through the microchannel array is thought to contribute to the improvement of accuracy. The average Nusselt number for the microchannel array was also evaluated experimentally in the condition of constant heat transfer rate. We found that there were deviations between the experimental and theoretical values of heat transfer rate in the microchannels. In order to predict heat transfer rate accurately, we proposed an empirical correlation in terms of Nu/(Re^0.62 Pr^0.33) and Brinkman number confined to the experimental range. The correlation is expected to be useful to design the microchannel devices related to heat transfer.     

High heat flux flow boiling in silicon multi-microchannels – Part III: Saturated critical heat flux of R236fa and two-phase pressure drops

New experimental critical heat flux results for saturated boiling conditions have been obtained for R236fa flowing in a silicon multi-microchannel heat sink composed of 67 parallel channels, 223 μm wide, 680 μm high and with 80 μm thick fins separating the channels. The microchannel length was 20 mm. The footprint critical heat fluxes measured varied from 112 to 250 W/cm² and the wall critical heat fluxes from 21.9 to 52.2 W/cm² for mass velocities from 276 to 992 kg/m²s. When increasing the mass velocity, the wall critical heat flux was observed to increase. The inlet saturation temperatures (20.31 ? T_sat,in ? 34.27 °C) and the inlet subcoolings (0.4 ? Δ T_sub ? 15.3 K) were found to have a negligible influence on the saturated CHF. The best methods for predicting the data were those of Wojtan et al. [L. Wojtan, R. Revellin, J. R. Thome, Investigation of critical heat flux in single, uniformly heated microchannels, Exp. Therm. Fluid Sci. 30 (2006) 765–774] and Revellin and Thome [R. Revellin, J. R. Thome, A theoretical model for the prediction of the critical heat flux in heated microchannels, Int. J. Heat Mass Transfer 50 (in press)]. They both predict the experimental CHF results with a mean absolute error of around 9%. Using the critical vapour quality, an annular-to-dryout transition is also proposed as a limit in a diabatic microscale flow pattern map. Pressure drop measurements were measured and analysed, showing that the homogeneous model could correctly predict the observed trends.     

Pressure effects on flow boiling instabilities in parallel microchannels

The effects of pressure on flow boiling instabilities in microchannels were experimentally studied. Experiments were conducted using water in 223 μm hydraulic diameter microchannels with mass fluxes ranging from 86 to 520 kg/m² s and pressures ranging from 50 to 205 kPa. Onset of flow oscillation, critical heat flux (CHF) conditions, local transient temperature measurements along with flow boiling visualization were obtained and studied. System pressure was found to significantly affect flow instabilities. For high pressure, it was observed that boiling instabilities were significantly delayed and CHF was extended to high mass qualities. Local temperature measurements also revealed lower magnitudes and higher frequencies of oscillations at high system pressures.     

Experimental investigation of fluid flow and heat transfer in a single-phase liquid flow micro-heat exchanger

This work presents an experimental analysis of the hydrodynamic and thermal performance of micro-heat exchangers. Two micro-heat exchangers, characterized by microchannels of 100 × 100 and 200 × 200 μm square cross-sections, were designed for that purpose. The fluid used was deionized water and there was no phase change along the fluid circuit. The fluid pressure drop along the heat exchanger and the heat transfer were measured and corrections were made to isolate the contribution of the microchannels. The results were compared with the predictions of the classical viscous flow and heat transfer theory. The main conclusions show that the experimental results fit well with these theories. No effects of heat transfer enhancement or pressure drop increase were observed as a consequence of the small scale of the microchannels.     

Boiling flow characteristics in microchannels with very hydrophobic surface to super-hydrophilic surface

Boiling flow process plays a very important role to affect the heat transfer in a microchannel. Different boiling flow modes have been found in the past which leads to different oscillations in temperatures and pressures. However, a very important issue, i.e. the surface wettability effects on the boiling flow modes, has never been discussed. The current experiments fabricated three different microchannels with identical sizes at 105 × 1000 × 30000 μm but at different wettability. The microchannels were made by plasma etching a trench on a silicon wafer. The surface made by the plasma etch process is hydrophilic and has a contact angle of 36° when measured by dipping a water droplet on the surface. The surface can be made hydrophobic by coating a thin layer of low surface energy material and has a contact angle of 103° after the coating. In addition, a vapor–liquid–solid growth process was adopted to grow nanowire arrays on the wafer so that the surface becomes super-hydrophilic with a contact angle close to 0°. Different boiling flow patterns on a surface with different wettability were found, which leads to large difference in temperature oscillations. Periodic oscillation in temperatures was not found in both the hydrophobic and the super-hydrophilic surface. During the experiments, the heat flux imposed on the wall varies from 230 to 354.9 kW/m² and the flow of mass flux into the channel from 50 to 583 kg/m²s. Detailed flow regimes in terms of heat flux versus mass flux are also obtained.