钛镍丝材切削性能改进

研究了生产工艺对形状记忆合金TiN i丝材切削性能的影响,结果表明:通过改变丝材的拉拔温度、矫直温度、矫直力等工艺参数,TiN i丝材的硬度及屈服强度、抗拉强度、延伸率等力学性能均发生改变,从而使得丝材的切削性能得到明显改善。     

冷连轧对TC16钛合金丝材组织性能的影响

冷轧加工不仅可以实现小规格丝材尺寸的高精度控制,也可以满足对组织和性能有特殊要求的丝材加工。通过对比分析冷连轧和热拉拔两种加工方式制备出的TC16钛合金丝材的性能和组织,研究了冷连轧工艺对TC16钛合金丝材退火态和固溶时效态性能的影响。结果表明,冷连轧获得的TC16钛合金丝材经退火后的抗拉强度比热拉拔加工丝材低,但是塑性较高,更有利于后续TC16钛合金紧固件的冷镦制成形;经过热处理强化后,冷连轧获得的TC16钛合金丝材强化效果明显,抗拉强度提高和塑性降低程度更为显著。相比热拉拔加工,冷连轧可有效破碎纵向长条α相并储存更多的加工畸变能,是获得优良退火态塑性和增强热处理强化作用的主要原因。     

退火工艺对WRe20热电偶丝材机械性能的影响

研究了退火工艺(退火方式,退火温度,速度,时间)对WRe20热电偶丝材机械性能的影响。发现在1 350℃,保温45min退火获得的0.4mm粗丝具有最佳的抗弯折性能;而0.104 mm细丝采用连续退火工艺,在1 100℃环境下以18 m/s的速度退火,其抗拉强度和延伸率最好,同时随退火温度的升高,丝材的抗拉强度下降而延伸率升高;对于退火条件相同而直径不同的丝材,其延伸率随丝径的减小而减小。研究结果表明合理的退火工艺,可以显著改善加工性能,利于丝材的进一步加工,提高成品率。     

退火工艺在钨铼热电偶丝材的应用

钨铼丝材在加工过程中易出现断裂、开劈等现象,为了提高材料塑性和热电稳定性,可通过退火处理来改善性能。文章详细阐述了钨铼丝材生产过程中各阶段的退火工艺和作用,通过退火处理,丝材的塑性和热电稳定性得到明显提高。     

矫直方式对3J58合金性能的影响

对现有丝材盘园矫直机进行改造后,发现用矫直方式矫直后的3J58丝材,具有较低的Δf/f(?)-T曲线的斜率和较高的 Q 值.认为这是由于改变了丝材表层的变形状态所致。     

钽丝的织构和再结晶行为研究

研究了变形钽丝在不同温度下退火后的织构演变和再结晶行为，发现1360℃退火后钽丝初次再结晶基本完成；1500℃退火后，钽丝中发生了二次再结晶，晶粒异常粗大。提出了拉拔钽丝的再结晶织构模型。     

40Cr磨光材端面及心部缺陷分析

某钢铁厂生产的40Cr磨光材在退火矫直车皮后的成品检查时发现,部分磨光材端面存在严重向内凹陷并伴有心部孔洞的缺陷。采用低倍检验、金相检验、扫描电镜观察和能谱分析等方法对缺陷形成的原因进行了分析。结果表明:40Cr磨光材端面及心部缺陷是在退火后的矫直过程中产生的,是由于受到了棒材内部的拉应力作用而形成的;同时试样轴向中心处的夹杂物细长且相对集中,也有可能成为产生心部孔洞的诱因。     

在线退火温度对TiNi合金组织和性能的影响

通过对试样微观组织及力学性能进行实验,研究了在线退火温度对TiNi合金丝材组织和性能的影响。实验表明,TiNi合金丝材经过(750~830℃)×2.3min在线退火处理后,丝材抗拉强度均大于960MPa,屈服强度均大于460MPa,延伸率均大于24.5%,断面收缩率均达到25%以上,830℃×2.3min在线退火处理后延伸率和断面收缩率最高,分别为54.5%和64.0%;说明经过830℃×2.3min在线退火处理后丝材塑性得到改善,达到最优。随着在线退火温度的升高,丝材的显微硬度逐渐降低。由微观组织可以看出,830℃×2.3min在线退火处理后丝材晶粒得到了细化。     

眼镜架用Ti-22V-4Al合金丝制备工艺研究

Ti-422(Ti-22V-4A1)合金具有优越的综合性能,特别具有很好的冷加工成形性,因此,用于制作高端眼镜架极具潜力.为了获得规模化生产Ti-422合金眼镜丝材的最佳工艺,对该合金冷加工丝材的变形程度和热处理工艺同力学性能和组织结构的关系进行了研究.结果得出,采用φ10 mm热轧坯料,辊模拉拨到φ5.0mm,退火后按55%～70%变形再辊模拉伸制得不同直径的丝材料,经780℃,30 min退火处理,其组织均匀,延伸率达20%以上.然后经520℃,4 h时效处理,维氏硬度达到2800 MPa,完全达到眼镜架用丝材对材料硬度2700 MPa＜Hv＜3000 MPa的技术要求.     

变形镁合金丝成形工艺的研究现状与展望

综述了镁合金的塑性成形工艺性能、镁合金丝成形工艺方法的研究现状和镁合金丝成形工艺的发展趋势。形变温度、载荷形式和晶粒尺寸对镁合金的塑性变形能力影响很大;通过升高温度和使镁合金处于三向压应力状态可以显著提高镁合金的塑性,因此热挤压是一种可行的镁合金丝塑性成形方法;拉拔成形过程中的应力状态对镁合金的塑性发挥不利,但在镁合金丝拉拔过程中引入电磁场、电脉冲等外场可以使镁合金的温度快速升高、晶粒细化,从而大幅提高镁合金的塑性,外场作用下生产效率极高的拉拔成形新技术是未来镁合金丝成形工艺的研究与发展方向。     

Improved shape memory composites combined with TiNi wire and shape memory epoxy

In order to develop high functionality of shape memory materials, the shape memory composites combined with TiNi wire and shape memory epoxy were fabricated, and the mechanical and thermomechanical properties were studied. The results showed that TiNi wire can compensate for the stiffness decrease of SMPs at elevated temperature, and the strength of interface and strength of interface matrix were important to further increase elevated temperature mechanical properties. The recovery stress of composites could be adjusted by changing the pre-strain, and the maximum recovery stress was obtained at 8% which was TiNi wire maximum recoverable strain. The addition of 1 vol% TiNi wire could increase the maximum recovery stress from 1.36 MPa to 4.04 MPa, which was almost 3 times of the matrix and at the same time maintained the rates of shape fixity and shape recovery close to 100%.     

Pass schedule of wire drawing process to prevent delamination for high strength steel cord wire

The high-speed drawing of high carbon content steel wires is usually conducted at room temperature employing a number of passes or reductions through several dies. In the multipass drawing process, the temperature rise at each pass affects the mechanical properties of the final product (such as its bending and torsion properties, and its tensile strength). This temperature rise during deformation encourages delamination in the wire, which has a deleterious influence on the torsional properties and durability of the wire. In this study, we investigated the delamination of wires using torsion tests and evaluated the wire temperature during drawing. Our data shows that one of the main reasons for delamination was an excessive rise in wire temperature. Based on our experimental results, in order to prevent delamination due to an excessive rise in wire temperature, a new isothermal pass schedule that could control the wire temperature was designed. The pass redesign for the conventional high carbon (0.75 wt%C) steel cord wire drawing process with delamination was carried out by using the isothermal pass schedule to control the wire temperature. In order to verify the effectiveness of the proposed method, wire drawing and torsion test were conducted. From the results of experiments, it was possible to produce high carbon steel cord wire without delamination.     

TiNi超弹丝的传感及驱动功能研究

测试了TiNi超弹丝在恒温拉伸、卸载过程中的电阻－应力－应变关系曲线，分析了力学及电阻特性的变化机理。结果表明，在恒温拉伸过程中TiNi超弹丝的电阻变化率与温度呈近似线性关系，在卸载过程中TiNi超弹丝表现出较大的屈服应力。可得出TiNi超弹丝具有力传感与驱动功能的结论，为构建以TiNi超弹丝为组元的智能材料结构提供了理论依据。     

SPS制备TiNi增强镁合金复合材料的微观结构及力学性能

以AZ31镁合金为基体,TiNi形状记忆合金丝为增强体,利用放电等离子烧结法（SPS）制备了TiNi/Mg复合材料,用OM、SEM、EDS对其微观形貌进行表征,并用XRD及DSC研究TiNi丝的相变,同时对该复合材料进行准静态拉伸实验,对其室温及高温力学性能进行研究。结果表明,所制备的TiNi/Mg复合材料中界面处存在Mg、Ti、Ni元素的互扩散现象,并形成宽度约为2 μm的互扩散层;所制备的TiNi/Mg复合材料的高温力学性能高于室温,其中其屈服强度、抗拉强度及弹性模量在100℃时（分别为157 MPa,292 MPa,22 GPa）较室温分别提高了12%、33%和29%,150℃时（分别为143 MPa,251 MPa,20 GPa）较室温分别提高了2%、14%和18%。     

拔丝模孔形计算机视觉检测技术

拔丝模是拔丝工业中的重要零件，是控制拔丝精度的关键，目前一般用显微镜或投晾影仪检测孔形质量，检测精度低，速度慢，文中论述了用计算机视觉检测技术实现拔丝模孔形全自动测量的方法，作者依此完成了“拔丝模孔形自动测量仪”的研制与开发，研制出的仪器已交付天津市金刚石工具厂实际使用，实际应用结果表明，用视觉检测技术开发的“拔丝模孔形自动测量仪”测量精度满足实际要求，速度快，使用方便。     

高强焊丝用H10Mn2SiNiMoTi盘条拉拔横裂分析

某高强焊丝用盘条在拉拔过程中出现很多横向断裂裂纹,采用扫描电镜、金相显微镜、直读光谱仪、显微硬度计等设备对断裂试样进行检测分析,结果表明,断裂的盘条化学成分和金相组织正常,夹杂物不严重,引起横裂产生的主要原因是边部的马氏体组织。焊丝在拉拔过速或者拉拔时润滑条件差的情况下,焊丝圆周与模具的接触位置摩擦生热,在高温下发生奥氏体相变,后续冷却又形成了马氏体组织。马氏体组织硬度高、脆性大,在焊丝拉拔轴向拉应力的作用下产生了横向开裂。     

Mechanical behavior of nanocrystalline TiNi alloy produced by severe plastic deformation

Nanocrystalline (NC) Ti₄₉₄Ni_50:6 alloy with a different mean grain size in a range of 20–100 nm has been successfully produced using severe plastic deformation by high pressure torsion and further annealing at various temperatures. The features of microstructure and martensitic transformation of the NC TiNi have been studied. During tensile tests the effects of the grain size on mechanical properties at room and elevated temperatures are studied and discussed. The NC TiNi exhibits an unusual increased strength but low ductility at room temperature. However, it demonstrates enhanced strength and ductility at higher temperatures.     

The effect of stacking fault energy on the microstructural development during room temperature wire drawing in Cu,Al and their dilute alloys

The effect of stacking fault energy (SFE) on the evolution of microstructures during wire drawing at room temperature has been studied in pure aluminium, pure copper and Cu-2.2% Al andCu-4.5% Al alloys which covers a range of SFE values from 4 to 166 mJ m^–2. The compositions are expressed in atomic parts per million by weight. The microstructures have been characterized from samples obtained by deforming rods of these materials to true wire drawing strain values of up to 1.47. A decrease in the SFE value changes the deformation mechanisms from the formation of cell structure and their size refinement in a high SFE material to the formation of deformation bands and deformation twins in a low SFE materials. The Cu-2.2% Al alloy deforms by deformation bands at low true strain values while deformation twins within the bands control the deformation mechanisms at higher true strain values. The alloy, Cu-4.5% Al, with the lowest SFE value deforms only by deformation twins even at low true strain values and the presence of overlapping and intersecting deformation twins are the dominating features as the rods are drawn to higher true wire drawing strains.     

The Manufacture of Resorbable Suture Material from Magnesium – Drawing and Stranding of Thin Wires

With the aid of multiple wire drawing passes, the magnesium alloys ZEK100, MgCa0.8, and AL36 were reduced to monofilament wires possessing diameters between 0.5 and 0.1 mm. These filaments were subsequently twisted into poly‐filament suture material using stranding. In order to analyze the microstructural constituents and the mechanical‐tribological properties, metallographic specimens were prepared and tensile tests were performed on both monofilament as well as poly‐filament wire strands. Appropriate parameters were ascertained for the wire drawing process with regard to forming rate, temperature, and heat treatment. During the investigations, the alloy ZEK100 exhibited particularly interesting mechanical properties which, owing to its high tensile strengths (up to 550 MPa for monofilament) and fracture strains (up to 30% for poly‐filament), are comparable to those of conventional polymer‐based suture materials. In addition to this, integrating a core (internal, individual wire) into the poly‐filament mesh of wire strands represents an interesting alternative for future research in which structures composed of different materials, and the advantages of combining their properties are brought into particular focus.