An estimation of maximum pressure for a thick-walled tube subjected to internal pressure

The plastic deformation of a thick-walled tube subjected to internal pressure is investigated by an incremental finite element method and the maximum bearing pressure is estimated. The results are compared with some approximate solutions proposed by MacGregor and others. A useful design formula is derived in order to estimate the maximum pressure and it is shown that better estimation can be made by this formula than by others proposed previously.     

Creep damage in small punch creep specimens of Type 304 stainless steel

Small punch creep tests on Type 304 stainless steel have been performed at 650 °C. Based on these tests, a finite element model, with modified Kachanov–Rabotnov creep damage constitutive equations, was established. The variation of central deflection and creep strain with time and the evolution of creep damage under constant loads were analysed by using the finite element model. The central creep deflection curves in the specimens were obtained at different loads in both tests and simulations and have three different stages, similar to conventional creep tests. There is good agreement between experimental results and simulation data. The creep damage at the central part is high, and localization of damage is obvious. Initial failure occurs at the bottom surface, about 0.8 mm away from the centre which agrees well with the finite element mode observation.     

Influence of machining-induced martensite on hydrogen-assisted fracture of AISI type 304 austenitic stainless steel

Hydrogen-assisted fracture of AISI type 304 steel has been evaluated with a special focus on the strain-induced martensite that is produced below the specimen surface during standard turning operation. Two different surface conditions were investigated: one containing martensite, resulting from the machining process, and a martensite-free state which is obtained after a proper heat treatment. Additionally, chemical composition and thickness of oxide layers, occurring in both studied cases, were analyzed by secondary ion mass spectrometry. These two different conditions were tested at room temperature in air (ambient pressure) and in hydrogen gas (40 MPa) atmosphere, respectively. Experimental results reveal a detrimental effect of machining-induced martensite on AISI type 304 steel performance in hydrogen, leading to major differences in relative reduction of area (RRA) between the as-machined and the heat-treated state for the same material. In this context, an operating mechanism based on hydrogen diffusion is discussed.     

304不锈钢在太阳能热水器行业的应用

从不锈钢材料及太阳能热水器内胆加工两方面,阐述了不锈钢内胆翻孔开裂及腐蚀失效的预防措施。     

Estimating structural integrity,using the TPFC approach,of annealed type 304 stainless steel plate and pipes containing surface defects

Test results and an evaluation of the two-parameter fracture criterion (TPFC) are presented. The tests were conducted at room temperature with annealed Type 304 stainless steel flat-plate tensile specimens containing triangular-, ellipsoidal- or rectangular-shaped surface flaws, and pressurised pipe specimens with internal or external triangular-shaped surface defects. Generally accepted analytical techniques are not available for these and other very ductile materials used in many nuclear reactor components and an accurate assessment of the influence of defects on structural component integrity is needed.The TPFC approach was used in conjunction with the initial defect size and the loads required for the initiation of subcritical crack growth, for penetration through the wall thickness and for instability. Generally, the test results obtained from the flat specimens could be used to predict, from a conservative point of view, the behaviour of pipe specimens. Since $\text{K}{}_{\mathrm{<mtext>F</mtext>}}$ is thickness dependent, it is recommended that tests be conducted for the specific thickness of concern using specimens containing surface defects. The TPFC approach can provide an accurate means for predicting structural integrity.     

Measurement and simulation of residual stress in type 304 weld overlay stainless steel pipe

Repair by welding overlay is a commonly used method mainly employed to rebuild piping systems suffering from intergranular stress corrosion cracking (IGSCC). It is desirable that the overlay welding technique, by attaching an overlay weld to the pipe and sustaining a heat sink of flowing water inside the pipe, induces a compressive residual stress at the inner surface of the welded pipe for prevention of IGSCC. A better understanding of the effect of a welding overlay repair on the residual stresses at the inner and outer surfaces of weld overlay is thus required. To obtain this understanding, it is necessary to investigate the distribution of residual stresses on the welded pipe.

In this study, the hole-drilling strain-gauge method was adopted to determine the residual stresses at the inner and outer surfaces of the weld overlay pipe. The incremental drilling technique was used on pipes with outside diameters of 267 mm. In addition, the Weld 3 code was applied to simulate the residual stress distribution for comparison and verification with the measured results.

The results obtained from the experimental and from the computational methods are in good agreement. The residual stress at the inner surface of the pipe is compressive with a magnitude approaching the yield stress of the material; that at the outer surface is tensile, also with a magnitude close to yield stress but smaller than the compressive stress. The experimental residual stress magnitude is generally greater than that from computation. This observation can be attributed to several factors including applied mechanics, temperature distribution, original residual stress, strain gauge location, mechanical grinding and the oxidation layer.     

Temperature distribution and residual stresses due to multipass welding in type 304 stainless steel and low carbon steel weld pads

Welding is a reliable and efficient metal-joining process widely used in industry. Due to the intense concentration of heat in the heat source of welding, the regions near the weld line undergo severe thermal cycles, thereby generating inhomogeneous plastic deformation and residual stresses in the weldment. Plates of different thickness are used in industry and these plates are normally joined by multipass welding. In a multipass welding operation, the residual stress pattern developed in the material changes with each weld pass. In the present experimental work, thermal cycles and transverse residual stresses due to each pass of welding have been measured in the weld pads of AISI type 304 stainless steel and low carbon steel with 6, 8 and 12 mm thickness. X-ray diffraction method was used for residual stress measurements. The welding process used was the Manual Metal Arc Welding (MMAW) process. In this paper, the peak temperatures attained at different points during deposition of weld beads in stainless steel and low carbon steel weld pads are compared. The residual stress patterns developed, the change in the peak tensile stress with the deposition of weld beads, and the relation between the peak temperatures and the residual stresses in the weld pads are discussed.     

Effect of alloying elements on hydrogen environment embrittlement of AISI type 304 austenitic stainless steel

The chemical composition of an AISI type 304 austenitic stainless was systematically modified in order to evaluate the influence of the elements Mo, Ni, Si, S, Cr and Mn on the material’s susceptibility to hydrogen environment embrittlement (HEE). Mechanical properties were evaluated by tensile testing at room temperature in air at ambient pressure and in a 40 MPa hydrogen gas atmosphere. For every chemical composition, the corresponding austenite stability was evaluated by magnetic response measurements and thermodynamic calculations based on the Calphad method. Tensile test results show that yield and tensile strength are negligibly affected by the presence of hydrogen, whereas measurements of elongation to rupture and reduction of area indicate an increasing ductility loss with decreasing austenite stability. Concerning modifications of alloy composition, an increase in Si, Mn and Cr content showed a significant improvement of material’s ductility compared to other alloying elements.     

Dependence of hydrogen embrittlement on hydrogen in the surface layer in type 304 stainless steel

Hydrogen embrittlement (HE) together with the hydrogen transport behavior in hydrogen-charged type 304 stainless steel was investigated by combined tension and outgassing experiments. The hydrogen release rate and HE of hydrogen-charged 304 specimens increase with the hydrogen pressure for hydrogen-charging (or hydrogen content) and almost no HE is observed below the hydrogen content of 8.5 mass ppm. Baking at 433 K for 48 h can eliminate HE of the hydrogen-charged 304 specimen, while removing the surface layer will restore HE, which indicates that hydrogen in the surface layer plays the primary role in HE. Scanning electron microscopy (SEM) and scanning tunnel microscopy (STM) observations show that particles attributed to the strain-induced α′ martensite formation break away from the matrix and the small holes form during deformation on the specimen surface. With increasing strain, the connection among small holes along {111} slip planes of austenite will cause crack initiation on the surface, and then the hydrogen induced crack propagates from the surface to interior.     

Simulation of the impact of internal pressure on the integrity of a hydrogen-charged Type-316L stainless steel during slow strain rate tensile test

A hydrogen-charged Type-316L austenitic stainless steel represents a slight loss of tensile ductility and cup-and-cone fracture accompanied by small-sized dimple. The reduction in the dimple size is interpreted to be attributed to void sheets caused by localized slip deformations by hydrogen. This paper aims to clarify the contribution of an internal pressure to the characteristic void growth of a hydrogen-charged Type-316L stainless steel during slow strain rate tensile (SSRT) test in air at room temperature. The internal pressure of pre-existing voids in the specimen charged by 100 MPa hydrogen gas at 270 °C for 200 h was simulated by diffusion-desorption analysis of hydrogen with the finite differential method (FDM). The subsequent impact of the internal pressure on the void growth was simulated by fracture-mechanics approach with the finite element method (FEM). The simulations performed under various void morphologies and fracture toughness suggested that the internal pressure in the voids was significantly low, hardly affecting the void growth.     

Analyses of hydrogen distribution around fatigue crack on type 304 stainless steel using secondary ion mass spectrometry

Secondary Ion Mass Spectrometry (SIMS) analyses were carried out on type 304 austenitic stainless steel. On annealed specimen exposed to hydrogen (10 MPa, 358  K), Element Depth Profiles SIMS mode was able to describe quantitatively the hydrogen profile content computed by the Fick’s law. Based on SIMS analyses on the wake of a fatigue crack (propagation in hydrogen gas at 0.6 MPa and RT), it was possible to compute an apparent diffusivity and solubility in the crack tip region. The apparent solubility and diffusivity in the deformed regions were two times and five orders of magnitude higher than the ones on annealed material, respectively. High hydrogen content was found around the crack tip, where the plastic deformation was well developed (pronounced slip activity). The high apparent diffusivity is presumed to result from enhanced hydrogen transport induced by cyclic plastic activity at the crack tip.     

Acoustic emission study of deformation behaviour of sensitised 304 stainless steel

Abstract

A systematic study has been undertaken to correlate the changes in acoustic emissions during tensile deformation of sensitised AISI type 304 stainless steel. Samples of a typical 304 stainless steel were sensitised at 700°C for 4, 14 and 24 h after being austenised at 1050°C for 30 min. AE signals were recorded during tensile test by using two sensors with 125 kHz resonant frequency. The results showed significant change in generation of AE during tensile deformation of sensitised AISI 304 stainless steel in compare to solution annealed material. This type of behaviour could be attributed to the microstructural changes in the sensitised specimens especially formation of continuous Cr₂₃C₆ carbides on grain boundaries which lead to increase in shearing by dislocations.     

Corrosion protection of type 304 stainless steel bipolar plates of proton-exchange membrane fuel cells by doped polyaniline coating

Polyaniline coating doped with dodecylbenzesulfonate anions is electrodeposited galvanostatically on type 304 stainless steel used as bipolar plates of proton-exchange membrane fuel cell from a basic solution of 0.3 M aniline monomer solution containing sodium dodecylbenzesulfonate as a supporting electrolyte. Electrochemical measurements in 1 M H₂SO₄ and in 0.3 M HCl show that the polyaniline coating increases the free corrosion potential of the steel by more than 300 mV and 450 mV, respectively, with a corrosion rate more than two orders of magnitude lower than that of the uncoated steel. Long-term exposure studies show that the coating is highly stable and inhibits the corrosion of the steel effectively.     

Using an equation based on flow stress to estimate structural integrity of annealed Type 304 stainless steel plate and pipes containing surface defects

An accurate assessment of the influence of defects on structural component integrity is needed. Generally accepted analytical techniques are not available for the very ductile materials used in many nuclear reactor components. This paper presents some results from a test programme to obtain data by which to evaluate proposed models. Plate and pipe specimens containing surface flaws were fabricated from annealed Type 304 stainless steel and tested at room temperature. An evaluation of an empirical equation based on flow stress is presented. In essentially all instances the flow stress is not a constant but varies as a function of the size of the surface flaw.     

In-plane instability tests of bellows subjected to internal pressure and deformation load

The in-plane instability of U-shaped bellows is analyzed. The in-plane instability critical pressure of bellows which are subjected to zero, tensile and compressive deformation are measured experimentally. The in-plane instability critical pressure of bellows under compressive deformation is apparently lower than that under zero deformation, and the in-plane instability critical pressure of bellows under tensile deformation is higher than that under zero deformation.     

Creep life assessment of an overheated 9Cr-1Mo steel tube

Crude oil heater 9Cr–1Mo steel tubes from a refinery plant were studied, after 24 years of service at nominally 650 °C and 27 MPa, to predict their remanent lives. The investigation included dimensional, hardness and tensile measurements in addition to accelerated stress rupture tests between 650 °C and 700 °C and microstructural examination. Tube specimens were taken from two sections, the overheated side and the side which only saw the nominal operating temperature. The method employed involved the prediction of the increase in temperature with increasing sediment deposition during the operating life times using an FEM model. In addition the predicted temperatures are used to derive appropriate creep properties at relevant temperatures in a 3D pipe FEM creep analysis to predict the pipe deformation rate. All compare well with the actual service exposed pipe measurements and layer deposition. The overheated side revealed a small loss of creep strength in a stress rupture test. A layer of sediment (appr. 10 mm thickness) consisting basically of sintered carbon (coke) spread over the inside of the tube was acting as a thermal barrier causing the temperature to rise above 650 °C. Analysis for the overheated side predicted an upper bound temperature of ≈800 °C and a life of about 50 h suggesting that failure by creep rupture could occur rapidly in the sediment region.     

Fracture toughness and fatigue crack growth properties of the base metal and weld metal of a type 304 stainless steel pipeline for LNG transmission

The fatigue crack growth rate and CTOD tests on type 304 stainless steel and weld metal were studied over the temperature range −162°C to room temperature. The girth weld metal specimens were fabricated using a combination of gas-tungsten-arc-welding and shielded-metal-arc-welding. The seam weld joint was made by submerged arc welding. Fracture toughness was evaluated through CTOD tests with three point bend specimens. The fatigue crack growth rate tests were conducted using compact tension specimens in accordance with ASTM E647. The CTOD values were affected by crack orientation with respect to the rolling direction, but orientation had no influence on the fatigue crack growth rates. The fatigue crack growth rates and the CTOD values decreased with decreasing test temperature.     

Hydrogen compatibility of austenitic stainless steel tubing and orbital tube welds

Refueling infrastructure for use in gaseous hydrogen powered vehicles requires extensive manifolding for delivering the hydrogen from the stationary fuel storage at the refueling station to the vehicle as well as from the mobile storage on the vehicle to the fuel cell or combustion engine. Manifolds for gas handling often use welded construction (as opposed to compression fittings) to minimize gas leaks. Therefore, it is important to understand the effects of hydrogen on tubing and tubing welds. This paper provides a brief overview of on-going studies on the effects of hydrogen precharging on the tensile properties of austenitic stainless tubing and orbital tube welds.     

Anisotropy of cold-worked Type-304 austenitic stainless steel: Focus on the hydrogen diffusivity

Anisotropic nature of effective hydrogen diffusivity was investigated on a cold-worked (CW) Type-304 stainless steel. The material was characterized by using disk-shaped specimens sampled from two directions of steel plates with various rolling ratio. The thickness direction of the disks was parallel to the rolling direction for SL specimens and perpendicular for LT ones. Electromagnetic induction (EMI) and electron backscatter diffraction (EBSD) clarified the content and distribution of strain-induced martensite (SIM). The effective diffusivities and solubilities were jointly determined by desorption method and thermal desorption analysis (TDA) in H-charged specimens with high-pressure gas. The increase of SIM with CW ratio and the differences of SIM distribution observed between LT and SL specimens could justify the anisotropic effective diffusivities. Finite element method (FEM) was used to simulate permeation tests based on multiple EBSD maps. Simulations supported the experimental findings: at the CW ratio of 60%, the CW process increased the diffusivity by twenty and the diffusivity was five time greater in the SL specimen than the LT one. The inhomogeneous SIM distribution justified the modifications of diffusion properties by CW in both specimens.