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以CE(氰酸酯)树脂为基体,以硅烷偶联剂(KH-560)表面处理过的纳米二氧化硅(nano-SiO2)为改性剂,采用高速均质剪切法制备CE/nano-SiO2复合材料;然后以该复合材料体系的黏度、凝胶化时间、弯曲强度和玻璃化转变温度(Tg)为考核指标,采用单因素试验法优选出满足树脂传递模塑(RTM)工艺用复合材料体系的最佳工艺条件。结果表明:当w(nano-SiO2)=3%、工作温度为(90±10)℃、工作时间≤10 h、固化温度为110~200℃和后处理工艺条件为220℃/4 h时,复合材料在低温时具有良好的稳定性,在高温时具有良好的反应性,完全满足RTM工艺的基本要求。 相似文献
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在多浇口和带嵌件注塑制品的成型过程中必然存在熔体的熔接过程,从而形成熔接线。熔接线沿厚度方向的熔接过程是影响该区域的力学强度以及纤维取向等制品性能的重要因素。本文采用有限元法针对注塑制品的典型截面建立数学模型,采用T6P3单元(速度二次插值,压力线性插值),数值模拟了注塑制品熔接线的截面熔接过程。通过等厚度截面和非等厚度截面两个算例,给出了两股熔体熔接过程中的截面速度场和压力场分布。讨论了熔接线区域的壁厚均匀程度对熔接过程的影响。该计算结果可以为制品力学性能以及纤维取向等数值模拟提供数据支持。 相似文献
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主要研究局部区域纤维体积密度改变对树脂流动前沿的影响。利用RTM-Worx模拟仿真软件,分析局部渗透率对流动前沿的变化及对填充该区域所用时间的影响规律。在模拟仿真的基础上,通过添加不同厚度垫片改变局部区域纤维体积密度,以对模拟仿真结果进行实验验证。仿真与实验结果表明:当局部纤维体积密度增大到一定值之后,该局部区域流动前沿出现包络现象,并且树脂填充该局部区域所用时间也开始急剧增加;当纤维体积密度继续增大时,该区域会出现树脂填充不完整的现象,最终导致制件出现干斑缺陷。 相似文献
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气辅成型技术能够有效地改善产品力学性能、提高产品的质量,因此在注射成型生产中应用广泛,与之相应的气辅成型CAE技术也得到了快速发展。当前的气辅成型CAE技术中假定空气为不可压缩流体,忽略了空气的可压缩性,因此研究气辅成型过程中可压缩空气的流动行为具有一定的实际意义。针对气辅成型过程中可压缩空气流动的复杂行为,基于假设将复杂的三维(3D)流动问题转化为二维(2D)。采用 CBS方法建立2D瞬态可压缩空气流动的有限元分析模型,求解算法采用预共轭梯度法,并用VC++完成了算法编制,实现了可压缩空气流动过程的数值模拟,其压力结果可作为充填流动分析的基础数据。 相似文献
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Injection molding of fiber‐reinforced polymeric composites is increasing with demands of geometrically complex products possessing superior mechanical properties of high specific strength, high specific stiffness, and high impact resistance. Complex state of fiber orientation exists in injection molding of short fiber reinforced polymers. The orientation of fibers vary significantly across the thickness of injection‐molded part and can become a key feature of the finished product. Improving the mechanical properties of molded parts by managing the orientation of fibers during the process of injection molding is the basic motivation of this study. As a first step in this direction, the present results reveal the importance of packing pressure in orienting the fibers. In this study, the effects of pressure distribution and viscosity of a compressible polymeric composite melt on the state of fiber orientation after complete filling of a cavity is considered experimentally and compared with the simulation results of Moldflow analysis. POLYM. COMPOS. 28:214–223, 2007. © 2007 Society of Plastics Engineers 相似文献
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应用Hele-Shaw物理模型和改进的Cross流变模型对辅助射成型过程中充填区域内熔体的流动进行数值模拟,采用控制体积法对充模过程中的熔体前沿、熔体-气体边界进行跟踪,运用有限元/有限差分混合数值方法求解气体注射阶段的速度场、压力场、温度场,以图表的形式列举了不同时刻压力场的分布和充模过程中的流线图。在计算过程中,采用压力场和温度场耦合的方法。 相似文献
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注塑成型过程中,熔体在型腔中的流动和传热对制品质量性能有重要的影响.为了预测注塑制品的收缩、翘曲和力学性能,精确预测充填过程的流动及传热历史是十分必要的.本文考虑熔体的可压缩性及相变的影响,将充填过程中熔体的流动视为非牛顿可压流体在非等温状态下的广义Hele-Shaw流动.采用有限元/有限差分混合方法求解压力场和温度场,采用控制体积法跟踪熔体流动前沿,并应用Visual C++实现了注塑充填过程的可压缩流动分析.为了保证能量方程各项在单元内边界的连续性,结点能量方程各项由单元形心处的离散值加权平均获得,因而,能量方程在计算区域内整体求解.对两个算例进行了分析,模拟结果与实验结果的对比,验证了本文数值算法及程序. 相似文献
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在Hele-Shaw流动数值模拟中,速度是压力的后处理结果。如果是点浇口,则浇口附近速度会随单元尺寸缩小而趋于无穷大,导致能量方程作为一个整体求解时,时间步长必须非常小,否则会产生很大误差;而根据热对流物理意义分步求解,则需追踪当前物质在上一时刻位置,当单元速度很高、逆向搜索需穿透多个单元时,搜索可能会失败。鉴于此,基于分步求解法,研究提出一种变长度子时间步长方法处理对流项,确保搜索路径局限在当前单元内,并采用二分法确定子时间步数量,使算法简洁有效。算例表明,该方法在保证计算精度和求解稳定性的同时,可以明显减少计算时间,提高计算效率。 相似文献
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High speed injection has been widely used in resin transfer molding (RTM), which improves manufacturing efficiency. This sometimes leads to excessive pressure within the mold, resulting in fiber destruction and mold deformation. Heating the mold and injection resin reduces the viscosity of resin, leading to influence on mold internal pressure. Selection of optimal mold and injection temperature for effective reduction of mold internal pressure has become a source of concern in the polymer industry. This article presents an outlook relationship between mold temperature, injection temperature, and mold internal pressure. It also showcases a temperature selection method angle to addressing this issue. The “FLUENT” software has been secondarily developed that gives an insight in using the three-dimensional nonisothermal RTM simulation. © 2019 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2019 , 136, 47492. 相似文献
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《Ceramics International》2017,43(6):4785-4793
The quality of ceramics parts made by powder injection molding (PIM) method is influenced by a range of factors such as powder and binder characteristics, rheological behavior of feedstock, molding parameters and debinding and sintering conditions. In this study, to optimize the molding parameters, the effect of injection temperature and pressure on the properties of alumina ceramics in the LPIM process were thoroughly studied. Experimental tests were conducted on alumina feedstock with 60 vol% powder. Injection molding was carried out at temperatures and pressures of 70–100 °C and 0.1–0.6 MPa respectively. Results showed that increase in injection temperature and pressure and the resulting increase in flow rate leads to the formation of void which impairs the properties of molded parts. The SEM studies showed that injection at temperature of 100 °C results in evaporation of binder components. From the processing point of view, the temperature of 80 °C and pressure of 0.6 MPa seems to be the most suitable condition for injection molding. In addition, the effects of sintering conditions (temperature and time) on the microstructure and mechanical properties are discussed. The best final properties were found using injection molding under the above stated conditions, thermal debinding and sintering at 1700 °C during 3 h. 相似文献
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Marangoni效应广泛存在于液液、气液相际传质过程中,通常会对传质速率产生重要影响。对Marangoni效应的实验及理论研究有助于增进对微观传质机理的理解,是强化相间传质过程效率的重要因素。重点介绍了液液体系中单液滴萃取的实验和模拟研究,对液液体系中Marangoni效应不稳定性的判据,对气液体系有效传质面积的影响,以及两种体系中利用表面活性剂进行传质调控的研究等方面的进展进行了综述,还探讨了传质过程中Marangoni效应应用研究的方向。 相似文献
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A simplified chemorheological model of viscosity evolution for solvent containing resol resin in RTM process 下载免费PDF全文
The solvent content‐dependent chemorheology of the solvent containing resol resin for resin transfer molding (RTM) was investigated. The curing behavior of the resol resin was studied by in situ Fourier transform infrared spectroscopy together with rheology tests. The chemorheological behavior of resol resins with a series of solvent contents was measured under isothermal conditions. The four parameters of empirical dual‐Arrhenius equation regarding isothermal resin viscosity and reaction rate constant were found to be functions of the solvent content. A simplified chemorheological model involving only three parameters of curing temperature, time, and solvent content was first established to facilely describe the viscosity during precuring process. The simulated viscosity results during isothermal curing process agreed well with the experimental data which shows the simplified chemorheological model can be utilized to describe the viscosity evolution and offer guidance for optimizing the injection process and improving the design flexibility of RTM process. © 2017 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2017 , 134, 45282. 相似文献
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《Journal of the European Ceramic Society》2021,41(14):6915-6924
In recent years, widespread use of advanced ceramics in vast areas of the industries such as medical technology and automotive industries has led to the growth of the advanced ceramics market. Due to the difficult machining processes and the difficulty of forming complex parts, manufacturing of ceramic components has been restricted. Powder injection molding can be used to overcome these restrictions. In this paper, SiC feedstock was injected at various temperatures and flow rates. Numerical and experimental results of injection step and imbalance filling were studied. As well as the separation of powder and binder was simulated and verified by experimental tests. Thermogravimetric analyzer and rotational rheometer were employed to evaluate the separation in the green parts and rheological properties of the prepared feedstocks, respectively. 相似文献