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1.
Thermomechanical processing simulations were performed using a hot-torsion machine, in order to develop a comprehensive understanding of the effect of severe deformation in the recrystallized and nonrecrystallized austenite regions on the microstructural evolution and mechanical properties of the 0.2 wt pct C-1.55 wt pct Mn-1.5 wt pct Si transformation-induced plasticity (TRIP) steel. The deformation schedule affected all constituents (polygonal ferrite, bainite in different morphologies, retained austenite, and martensite) of the multiphased TRIP steel microstructure. The complex relationships between the volume fraction of the retained austenite, the morphology and distribution of all phases present in the microstructure, and the mechanical properties of TRIP steel were revealed. The bainite morphology had a more pronounced effect on the mechanical behavior than the refinement of the microstructure. The improvement of the mechanical properties of TRIP steel was achieved by variation of the volume fraction of the retained austenite rather than the overall refinement of the microstructure.  相似文献   

2.
The present study was carried out on four steels containing 0.1 pct C-1.5 pct Mn-0.003 pct B* in common, with additions of 1 pct Cr, 0.5 pct Mo, 0.25 pct Mo + 1 pct Cr, 0.2 pct Ti + 1 pct Cr. They were designated, accordingly, as Cr, Mo, Mo-Cr, and Cr-Ti steels. All the steels exhibited a complete lath martensite microstructure with thin interlaths of retained austenite (≈0.05 pct) in the quenched condition. The normalized microstructures, granular bainite, contained massive areas of ferrite and granules of bainite laths. Both microconstituents contained a fine dispersion of cementite particles (size ≈50 Å) together with high dislocation densities. A mechanism explaining their for-mation has been given. The Cr steel, due to its low hardenability, showed in addition polygonal ferrite in the neighborhood of the so-called M-A constituent (twinned martensite and/or austenite). The annealed microstructure (using a cooling rate of 0.033 °C s?1) of the Cr steel consisted of coarse ferrite-pearlite. Addition of 0.2 pct Ti to the Cr steel markedly refined the structure, whereas an addition of 0.25 pct Mo altered the microstructure to ferrite-lower bainite. In the 0.5 pct Mo steel, polygonal ferrite was found to be completely missing. The mechanical properties of the four steels after quenching, normalizing, and annealing were investigatedvia hardness and tensile test mea-surements. An empirical equation, relating the ultimate tensile strength to the steel composition, for steels that had granular bainite microstructures in the normalized condition, was proposed. The fracture surfaces exhibited cleavage and variable-size dimples depending on the microstructure and steel composition.  相似文献   

3.
Dual-phase and transformation-induced plasticity (TRIP)-assisted multiphase steels are related families of high-strength formable steels exhibiting excellent mechanical characteristics. This study shows how a ferrite-bainite-martensite microstructure containing retained austenite can improve the mechanical properties of a cold-rolled low-carbon, low-silicon steel. Such a multiphased microstructure is obtained by a heat treatment involving intercritical annealing followed by a bainite transformation tempering. Depending on the heat-treatment parameters, the samples present a variety of microstructures. Due to the presence of retained austenite, some samples exhibit a TRIP effect not anticipated with such a low silicon content. A composite strengthening effect also results from the simultaneous presence of a ductile ferrite matrix with bainite and martensite as hard second phases. A true stress at maximum load of 800 MPa and a true uniform strain of 0.18 can be obtained by forming a ferrite-bainite-martensite microstructure containing up to 10 pct of retained austenite. These properties correspond to a favorable evolution of work hardening during plastic deformation.  相似文献   

4.
 为了实现低硅含铝热轧TRIP钢的工业应用,以低硅含铝热轧TRIP钢为研究对象,采用扫描电子显微镜、透射电子显微镜、拉伸试验和X射线衍射等试验方法,研究了不同等温时间对试验钢显微组织和力学性能的影响。结果表明,试验钢的显微组织主要由多边形铁素体、贝氏体铁素体和残余奥氏体组成,随着等温时间的增加,板条贝氏体的体积分数升高,粒状贝氏体的体积分数降低;当等温时间为20 min时,试验钢的综合力学性能最佳,抗拉强度为732.25 MPa,断后伸长率为36%,强塑积为26.36 GPa·%;残余奥氏体的体积分数和碳含量先升高后降低,等温时间为20 min时试验钢表现出较强的加工硬化行为。  相似文献   

5.
The effect of additions of Nb, Al and Mo to Fe‐C‐Mn‐Si TRIP steel on the final microstructure and mechanical properties after simulated thermomechanical processing (TMP) has been studied. The laboratory simulations of discontinuous cooling during TMP were performed using a hot rolling mill. All samples were characterised using optical microscopy and image analysis. The volume fraction of retained austenite was ascertained using a heat tinting technique and X‐ray diffraction measurements. Room temperature mechanical properties were determined by a tensile test. From this a comprehensive understanding of the structural aspect of the bainite transformation in these types of TRIP steels has been developed. The results have shown that the final microstructures of thermomechanically processed TRIP steels comprise ~ 50 % of polygonal ferrite, 7 ‐12 % of retained austenite, non‐carbide bainitic structure and martensite. All steels exhibited a good combination of ultimate tensile strength and total elongation. The microstructure‐property examination revealed the relationship between the composition of TRIP steels and their mechanical properties. It has been shown that the addition of Mo to the C‐Si‐Mn‐Nb TRIP steel increases the ultimate tensile strength up to 1020 MPa. The stability of the retained austenite of the Nb‐Mo steel was degraded, which led to a decrease in the elongation (24 %). The results have demonstrated that the addition of Al to C‐Si‐Mn‐Nb steel leads to a good combination of strength (~ 940 MPa) and elongation (~ 30 %) due to the formation of refined acicular ferrite and granular bainite structure with ~7 8 % of stable retained austenite. Furthermore, it has been found that the addition of Al increases the volume fraction of bainitic ferrite laths. The investigations have shown an interesting result that, in the Nb‐Mo‐Al steel, Al has a more pronounced effect on the microstructure in comparison with Mo. It has been found that the bainitic structure of the Nb‐Mo‐Al steel appears to be more granular than in the Nb‐Mo steel. Moreover, the volume fraction of the retained austenite increased (12 %) with decreasing bainitic ferrite content. The results have demonstrated that this steel has the best mechanical properties (1100 MPa and 28 % elongation). It has been concluded that the combined effect of Nb, Mo, and Al addition on the dispersion of the bainite, martensite and retained austenite in the ferrite matrix and the morphology of these phases is different than effect of Nb, Mo and Al, separately.  相似文献   

6.
The effect of phosphorus and silicon on the formation of retained austenite has been investigated in a low-carbon steel cold rolled, intercritically annealed, and isothermally held in a temperature range of bainitic transformation followed by air cooling. The steel sheet containing phosphorus after final heat-treatment consisted of ferrite, retained austenite, and bainite or martensite. Phosphorus, especially in the presence of silicon, in steel was useful to assist the formation of retained austenite. Mechanical properties, such as tensile strength, uniform elongation, and the combination of tensile strength/ductility, were improved when phosphorus was increased up to 0.07 pct in 0.5 pct Si steel. This could be attributed to the strain-induced transformation of retained austenite during tensile deformation. Furthermore, two types of retained austenite were observed in P-containing steel. One is larger than about 1 μm in size and usually exists adjacent to bainite; the other one is of submicron size and usually exists in a ferrite matrix. High phosphorus content promotes the formation of stable (small size) austenites which are considered to be stabilized mainly by their small size effect and have a different formation mechanism from the coarser retained austenite in the lower P steels. The retained austenites of submicron size showed mechanical stability even after 10 pct deformation, suggesting that these small austenites have little effect on ductility. The 0.07 pct P-0.5 pct Si-1.5 pct Mn-0.12 pct C steel showed a high strength of 730 MPa and a total elongation of 36 pct.  相似文献   

7.
It is well known that a significant amount of retained austenite can be obtained in steels containing high additions (>1 pct) of Si, where bainite is the predominant microconstituent. Furthermore, retained austenite with optimum characteristics (volume fraction, composition, morphology, size, and distribution), when present in ferrite plus bainite microstructures, can potentially increase strength and ductility, such that formability and final properties are greatly improved. These beneficial properties can be obtained largely by transformation-induced plasticity (TRIP). In this work, the effect of a microalloy addition (0.035 pct Nb) in a 0.22 pct C-1.55 pct Si-1.55 pct Mn TRIP steel was investigated. Niobium was added to enable the steel to be processed by a variety of thermomechanical processing (TMP) routes, thus allowing the effects of prior austenite grain size, austenite recrystallization temperature, Nb in austenite solid solution, and Nb as a precipitate to be studied. The results, which were compared with those of the same steel without Nb, indicate that the retained austenite volume fraction is strongly influenced by both prior austenite grain size and the state of Nb in austenite. Promoting Nb(CN) precipitation by the change in TMP conditions resulted in a decrease in the V RA . These findings are rationalized by considering the effects of changes in the TMP conditions on the subsequent transformation characteristics of the parent austenite.  相似文献   

8.
利用扫描电子显微镜(SEM)、透射电子显微镜(TEM)、电子探针(EPMA)、X射线衍射仪(XRD)、室温拉伸等手段, 通过两相区保温-淬火(IQ)、两相区形变后保温-淬火(DIQ)、两相区保温-淬火-配分-贝氏体区等温(IQ&PB)及两相区形变后保温-淬火-配分-贝氏体区等温(DIQ&PB)热处理工艺, 研究高温形变对室温组织、性能、残余奥氏体稳定性的综合影响作用.结果表明, 经15%的压缩形变后铁素体中位错密度由0.290×1014增加至1.286×1014 m-2, 马氏体(原奥氏体)中C、Cu元素富集浓度提高, 高温形变产生位错增殖对元素配分有明显促进作用.DIQ&PB工艺下, 形变后贝氏体板条尺寸变短且宽度增加0.1 μm左右, 贝氏体转变量较未变形时增加14%, 多边形铁素体尺寸明显减小.力学性能方面, 两相区形变热处理后抗拉强度增加132.85 MPa, 断后伸长率增加7%, 强塑积可达25435 MPa·%.形变后残余奥氏体体积分数由7.8%提高到8.99%, 残余奥氏体中碳质量分数由1.05%提高到1.31%.   相似文献   

9.
Microstructures in X80 line pipe were classified by SEM analysis.The experimental results showed that the microstructures in X 80 line pipe steels were complicated consisting of polygonal ferrite,bainite and acicular ferrite.Orientation relation within acicular ferrite was investigated systematically by means of EBSD-OIM.The sub-structures were observed maximum in acicular ferrite which gives high strength and high toughness to line pipe steels.The K-S orientation relation was generally observed between acicular ferrite and austenite during phase transformation.The low energy CSL boundary characterized by Σ3 orientation relation according to Brandon criterion appeared with higher probability,which was benefit to improve the mechanical properties of line pipe steels.The orientations or texture of initial austenite grains could be deduced based on the Σ3 orientation relationship of acicular ferrite variants.  相似文献   

10.
Different thermomechanical treatments were applied to a high strength low carbon steel with a novel chemical composition. As a result, three different microstructures were produced with dissimilar mechanical and corrosion properties. Subsequently, a tempering heat treatment was applied to redistribute the phases in the steel. Microstructure A with 56 pct martensite and 32 pct bainite presented high strength but medium ductility; microstructure C with 95 pct ferrite and 3 pct martensite/austenite resulted in low strength and high ductility, and finally microstructure B with 98 pct bainite and 2 pct martensite/austenite resulted in high strength and ductility. Alternatively the corrosion behavior obtained by polarization curves was characterized in 0.1 M H2SO4, 3 M H2SO4, 3.5 wt pct NaCl, and NS4 solutions resulting in similar magnitudes, while the corrosion behavior acquired by electrochemical impedance spectroscopy had slightly differences in 3 M H2SO4.  相似文献   

11.
In this study, medium Mn transformation-induced plasticity steel with the composition Fe-0.08 pct C-6.15 pct Mn-1.5 pct Si-2.0 pct Al-0.08 pct V was investigated. After intercritical annealing at 1013 K (740 °C), the steel contained coarse-grained ferrite and two ultrafine-grained (UFG) phases: ferrite and retained austenite. The material did not deform by localized Lüders band propagation: it did not suffer from this major problem as most UFG steels do. Localization of plastic flow was shown to be suppressed because of a combination of factors, including a bimodal grain size distribution, a multiphase microstructure, the presence of nanosized vanadium carbide precipitates, and the occurrence of the deformation-induced martensitic transformation of retained austenite. A constitutive model incorporating these effects was developed. The model was used to identify the factors which can lead to a further improvement of the mechanical properties of the UFG medium Mn TRIP steels.  相似文献   

12.
 The influence of hot-rolled process on microstructure in TRIP steel and the heredity characteristic from the hot-rolled microstructure to annealed microstructure are investigated. The results show there are two kind of hot-rolled microstructures under different coiling temperatures. One is composed of coarse grains of ferrite, pearlite and bainite, and the other is composed of small grains of ferrite, bainite and austenite. After annealing, the first kind of hot-rolled microstructure is greatly refined, and volume fraction, carbon content of austenite increase significantly. However, it have little changes in grain size, volume fraction and carbon content of austenite after the second kind of hot-rolled sheet is annealed. There are also differences in distribution of retained austenite between the two annealed microstructures observed by EBSD and TEM technology. Retained austenite in the first annealed microstructure distributes mainly inside of the polygonal ferrite in the form of spot, only little retained austenite on bainte ferrite boundary, however retained austenite in the second annealing microstructure allocates several places, such as inside of polygonal ferrite, on polygonal ferrite boundary, on bainte ferrite boundary.  相似文献   

13.
A ferrite-bainite-martensite (F-B-M) microstructure was produced in a medium-carbon microalloyed (MA) steel through two routes, namely, low-temperature finish forging and rolling, followed by a two-step cooling (TSC) and annealing. Transmission electron microscopy (TEM) was employed to study the microstructural evolution in control forged and rolled material after TSC followed by annealing (TSCA). A TEM investigation was also carried out on samples low-cycle fatigue (LCF) tested at low and high total strain amplitudes of 0.4 and 0.7 pct in case of the forged steel (F-B-M(F)TSCA) and 0.55 and 0.8 pct for the rolled steel (F-B-M(R)TSCA), respectively. Microstructural changes accompanying the LCF testing were identified. The two-step cooled microstructure processed through forging (F-B-M(F)TSC) as well as rolling (F-B-M(R)TSC) revealed a complex multiphase microstructure, along with films and blocks of retained austenite. In both microstructural conditions, vanadium carbide precipitates were too fine to be identified after the TSC treatment. Annealing after TSC produced a stress-free microstructure. The F-B-M(F)TSCA microstructure predominantly consisted of granular/lower bainite, lath martensite, and polygonal ferrite with interlath films as well as blocks of retained austenite, while the F-B-M(R)TSCA microstructure predominantly consisted of lath martensite, granular/lower bainite, and polygonal ferrite with interlath strips/films of retained austenite. Lath martensite content was higher in the F-B-M(R)TSCA condition than in the F-B-M(R)TSCA condition. In both conditions, vanadium carbide precipitates could be seen after annealing. Fatigue-tested F-B-M(F)TSCA microstructure up to a total strain amplitude of 0.4 pct and F-B-M(F)TSCA microstructure up to a total strain amplitude of 0.55 pct were stable. Lath martensite did not undergo deformation and in both microstructural conditions dislocation cell structures were not observed in the ferrite or bainite regions. The interlath retained austenite strips/films played a significant role in preventing the softening during fatigue loading. First, it was stable up to a total strain amplitude of 0.4 and 0.55 pct in the respective microstructures. Second, it underwent heavy deformation during fatigue loading at high total strain amplitudes, thereby accommodating the strain. Fatigue-tested F-B-M(F)TSCA microstructure at a total strain amplitude of 0.7 pct and F-B-M(R)TSCA microstructure at a total strain amplitude of 0.8 pct revealed deformed bainite/martensite laths, dislocation cells, and slip bands in the ferrite regions, which are characteristic features of cyclic softening. The retained austenite transformed to martensite through a strain-induced transformation mechanism and, at that stage, the microstructure contained in addition dislocation-rich bainite and ferrite.  相似文献   

14.
 Warm deformation tests were performed using a kind of tubby heater. The microstructures and mechanical properties of an Fe-C-Mn-Si multiphase steel resulting from different warm deformation temperatures were investigated by using LOM (light optical microscopy), SEM and XRD. The results indicated that the microstructure containing polygonal ferrite, granular bainite and a significant amount of the stable retained austenite can be obtained through hot deformation and subsequent austempering. Warm deformation temperature affects the mechanical properties of the hot rolled TRIP steels. Ultimate tensile strength balance reached maximum (881 MPa) when the specimen was deformed at 250 ℃, and the total elongation and strength-ductility reached maximum (38% and 28614 MPa·%, respectively) at deforming temperature of 100 ℃. Martensite could nucleate when austenite was deformed above Ms, because mechanical driving force compensates the decrease of chemical driving force. The TRIP effect occurs in the Fe-C-Mn-Si multiphase steel at deforming temperature ranging from 15 to 350 ℃. The results of the effects of warm deformation on the mechanical properties of the Fe-C-Mn-Si multiphase steel can provide theoretical basis for the applications and the warm working of the hot rolled TRIP sheet steels in industrial manufacturing.  相似文献   

15.
The main emphasis of this study has been placed on understanding the effects of manganese and silicon additions and of heat-treatment (intercritical annealing and isothermal treatment) conditions on the microstructures and mechanical properties of 0.15 wt pct C transformation-induced plasticity (TRIP)-aided cold-rolled steel sheets. The steel sheets were intercritically annealed and isothermally treated at the bainitic region. Microstructural observation and tensile tests were conducted, and volume fractions of retained austenite were measured. Steels having a high manganese content had higher retained austenite fractions than the steels having a low manganese content, but showed characteristics of a dual-phase steel such as continuous yielding behavior, high tensile strength over 1000 MPa, and a low elongation of about 20 pct. The retained austenite fractions and mechanical properties varied with the heat-treatment conditions. In particular, the retained austenite fractions increased with decreasing intercritical annealing and isothermal treatment temperatures, thereby resulting in the improvement of the elongation and strength-ductility balance without a serious decrease in the yield or tensile strength. These findings suggested that the intercritical annealing and isothermal treatment conditions should be established in consideration of the stability of austenite and the solubility of alloying elements in the austenite formed during the intercritical annealing.  相似文献   

16.
Transformation-induced plasticity (TRIP) steels have excellent strain hardening exponents and resistibility against tensile necking using the strain-induced martensite formation that occurs as a result of the plastic deformation and strain on the retained austenite phase. Detailed studies on the microstructures and local mechanical properties, as well as global mechanical properties, are necessary in order to thoroughly understand the properties of TRIP steels with multiple phases of ferrite, bainite, retained austenite, and martensite. However, methods for investigating the local properties of the various phases of the TRIP steel are limited due to the very complicated and fine microstructures present in TRIP steel. In this study, the experimental and numerical methods, i.e., the experimental nanoindenting results and the theoretical finite element analyses, were combined in order to extract the local stress–strain curves of each phase. The local stress–strain curves were in good agreement with the values presented in the literature. In particular, the global plastic stress–strain behavior of the TRIP steel was predicted using the multiple phase unit cell finite element analysis, and this demonstrated the validity of the obtained properties of each local phase. The method of extracting the local stress–strain curves from the nanoindenting curves and predicting the global stress–strain behavior assists in clarifying the smart design of multi-phase steels.  相似文献   

17.
Continuous cooling transformation diagrams were determined for molybdenum-boron steels containing 0.24, 0.4, and 0.66 pct Mo with 0.1 pct C, and also 0.4 pct Mo with 0.2 pct C, after thermomechanically working by compressive deformation to 12, 25, and 50 pct reduction at 830°C (1525°F), as well as for the steels in the underformed condition. In underformed specimens, higher carbon or molybdenum decreased the limiting cooling rate for the avoidance of polygonal ferrite formation. The same was true for deformed specimens, although increased deformation raised the limiting cooling rates of all compositions. The limiting cooling rate for polygonal ferrite formation increased exponentially with austenite, deformation, as measured by true strain. Thermomechanical working also raised bainite start temperatures at fast cooling rates and caused small increases in martensite start temperatures.  相似文献   

18.
The microstructure and mechanical properties of cold rolled TRIP steel containing C 0.2, Si 0.5, Mn 1.5, A1 1.3, and Nb-kV 0.13 (mass%) with annealed martensite (TAM steel) were investigated using optical microscopy, field emission gun scanning electronic microscope (FEG SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), and mechanical testing. The mierostructure of the TAM steel mainly consisted of polygonal ferrite, bainite, annealed martensite and retained austenite. The martensite after annealing did not spheroidize, which consisted of annealed lath martensite structure and interlath second phase. Compared with the traditional TRIP steel with polygonal ferrite matrix (TPF steel), the TAM steel has more excellent elongation rate over 32%. The TAM steel also has better strain hardening behavior than the TPF steel. The excellent elongation and strain harden- ing behavior of TAM steel result from high retained austenite stability of the TAM steel, which is attributed to its fine distribution and medium strength ratio of second phase to matrix.  相似文献   

19.
Dual phase steels are characterized by a microstructure consisting of ferrite, martensite, retained austenite, and/or lower bainite. This microstructure can be altered by tempering with accompanying changes in mechanical properties. This paper examines such changes produced in a vanadium bearing dual phase steel upon tempering below 500 °C. The steel mechanical properties were minimally affected on tempering below 200 °C; however, a simultaneous reduction in uniform elongation and tensile strength occurred upon tempering above 400 °C. The large amount of retained austenite (≅10 vol pct) observed in the as-received steel was found to be essentially stable to tempering below 300 °C. On tempering above 400 °C, most of the retained austenite decomposed to either upper bainite (at 400 °C) or a mixture of upper bainite and ferrite-carbide aggregate formed by an interphase precipitation mechanism (at 500 °C). In addition, tempering at 400 °C led to fine precipitation in the retained ferrite. The observed mechanical properties were correlated with these microstructural changes. It was concluded that the observed decrease in uniform elongation upon tempering above 400 °C is primarily the consequence of the decomposition of retained austenite and the resulting loss of transformation induced plasticity (TRIP) as a contributing mechanism to the strain hardening of the steel. B. V. N. RAO, formerly Senior Research Engineer, Analytical Chemistry Department, General Motors Research Laboratories  相似文献   

20.
Mechanical Behavior of Carbide-free Medium Carbon Bainitic Steels   总被引:1,自引:0,他引:1  
The effect of bainitic transformation time on the microstructure and mechanical properties was investigated in a steel containing 0.4 pct C-2.8 pct Mn-1.8 pct Si. The microstructure was characterized using optical and transmission electron microscopy; it consisted of bainitic ferrite, martensite, and retained austenite. The volume fraction of bainite increased from 0.4 for the shortest bainitic transformation time (30 minutes) to 0.9 at the longest time (120 minutes). The above microstructures exhibited an extended elasto-plastic transition leading to very high initial work-hardening rates. The work-hardening behavior was investigated in detail using strain-path reversals to measure the back stresses. These measurements point to a substantial kinematic hardening due to the mechanical contrast between the microstructural constituents. The onset of necking coincided with the saturation of kinematic hardening. Examination of the fracture surfaces indicated that the prior austenite grain boundaries play an important role in the fracture process.  相似文献   

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