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1.
The purpose of this study was to evaluate the effect of etching and silane priming on bond strength to a feldspathic porcelain (VMK 68) of a composite resin (Clearfil APX). Two hydrofluoric acid etchants (2.5% and 5%) and seven different etching times (0, 30, 60, 90, 120, 150, and 180 seconds) were used to etch the porcelain specimens respectively. A self-curing bonding agent containing a silane coupler (Clearfil Porcelain Bond) was used on both etched and unetched porcelain surfaces. Etched relief patterns were observed by means of a scanning electron microscope, and the bond strengths between the photocured composite resin and the porcelain were determined. Scanning electron micrographs revealed complicated etching patterns with increased etching time periods. Shear testing results showed that the bond strength to the unetched porcelain of the composite resin was very low, and that etching periods for more than 30 seconds effectively enhanced the bond strength. Of the two etching agents applied to the unsilanated porcelain, the buffered 2.5% etchant produced higher bond strengths than the 5% etchant for all etching time periods except for 180 seconds. Silane priming was effective and critical for improving bond strength to the porcelain. Application of the silane bonding agent to the porcelain after hydrofluoric acid etching appeared to be suitable for achieving consistent bonding between the composite resin and the porcelain.  相似文献   

2.
This study compared the effects of different dentin surface treatments on the shear bond strengths of three adhesive systems. The adhesive systems included a resin-modified glass ionomer, Fuji II LC, and two dentin bonding systems, One Step and Scotchbond Multi-Purpose Plus. The surface treatments compared for each adhesive system were as follows: 1) the controls, which were conditioned, 2) air abrasion at 120 psi without conditioning, 3) air abrasion at 160 psi without conditioning, 4) air abrasion at 120 psi with conditioning, and 5) air abrasion at 160 psi with conditioning. The KCP 1000 Whisperjet was used for all air-abrasive specimens. Controls for each adhesive material (Fuji II LC, One Step, Scotchbond Multi-Purpose Plus) were bonded using manufacturers' recommendations. Results showed that air abrasion significantly lowered bond strength of the resin-modified glass ionomer, conditioned or nonconditioned (P < 0.01). Air abrasion alone significantly lowered bond strengths of the dentin bonding agent systems (P < 0.01). However, air abrasion plus conditioning of the dentin surface resulted in bond strengths that were similar to the conditioned-only specimens (P < 0.01).  相似文献   

3.
In this study failures of composite resin/ porcelain interfaces under shear loading were examined. Porcelain firing were made onto metal cylinders and porcelain surfaces were roughened with burrs or treated with hydrofloric acid gel and/ or sandblasted with a Microetcher. Two silane coupling agents were used in five groups, each of which had 22 samples. All of the treated samples were restored with a hybrid-type composite resin. Then each group was divided into two subgroups according to storage times of 24 h and 30 days. After thermocyling the samples which were stored for 30 days, all of the groups were subjected to shear force at the composite resin/porcelain interface until fracture occurred. The results showed that there were differences both in the 24-h and 30-day storage period bond strengths between the various surface treatment methods. The samples treated with all three of the Microetcher, hydrofloric acid and silane exhibited the highest shear bond values after 24 h storage, followed by the microetched/silane and the hydrofluoric acid/silane groups (F: 570.31, P: 0.00). After 30 days, the highest mean shear bond strength values were again with samples treated by all three processes. The storage period and thermocycling decreased the bond strength of samples, however, there was a significant difference among groups (F: 1388-55, P: 0.00). Silane pre-treatment of porcelain was important as the mean bond strength of sandblasted/etched specimens were significantly lower than the other groups which were treated mechanically, in 24 h. Sandblasting seems to have little effect on the bonding. The comparison of 24-h and 30-day samples have also significant difference (F: 91.4376, P: 0.00).  相似文献   

4.
Clinically, orthodontists are often faced with the difficulties of bonding to porcelain crowns, veneers, or bridges. Traditional methods of dealing with this are often time-consuming and generally esthetically unacceptable to patients. Current interest involves the use of organosilane primers with or without NTG-GMA and BPDM resins to aid in chemically bonding porcelain with traditional orthodontic adhesives. This study compared the bond strength of three types of adhesion promoters: Ormco Porcelain Primer (OR) (Ormco Corp., Glendora, Calif.), All-Bond2 (AB2) (Bisco Dental Products, Inc., Itasca, Ill.), and Scotchprime Ceramic Primer (SP) (3M, St. Paul, Minn.) with two orthodontic adhesives: Phase II (Reliance, Inc., Itasca, Ill.) and Rely-a-bond (Reliance, Inc., Itasca, Ill.). Eighty ceramometal samples were fabricated and hydrated for 1 week in distilled water before bonding. Next, the samples were etched with 2.5 % HF acid for 90 seconds, rinsed and upper central incisor metal orthodontic brackets were bonded with the various primers and adhesives. After 24 hours they were sheared off with an MTS machine at at rate of 0.5 mm/min, and the bond strength was measured. The mean shear bond strengths (MPa) with Phase II were as follows; Control 0.44 (sigma = 0.22), AB2 8.40 (sigma = 3.61), OR 13.31 (sigma = 5.79), SP 13.53 (sigma = 3.34). With Rely-a-bond, the shear bond strengths were Control 0.41 (sigma = 0.67), AB2 4.34 (sigma = 1.88), OR 9.73 (sigma = 4.58), and SP 12.40 (sigma = 3.05).(ABSTRACT TRUNCATED AT 250 WORDS)  相似文献   

5.
Carbon dioxide (CO2) lasers are capable of producing surface irregularities in human enamel which resemble those resulting from etching of enamel with orthophosphoric acid. This report presents the results of a laboratory study which examined the effect of selected tooth-related variables on shear bond strength between a current generation bonding agent (Scotchbond MultiPurpose) and acid-etched or laser-conditioned human enamel. There were no significant differences in shear bond strength between human maxillary central incisor teeth, first premolars, and third molars in either the acid etch or laser-conditioned groups. Polishing of enamel to give a flat surface increased the shear bond strength obtained with acid etching, but did not alter significantly bond strengths achieved with laser conditioning. There was a tendency for a higher bond strength with acid etching, but not with laser conditioning, in porcine molar enamel compared with human molar and bovine incisor enamel. In terms of the mode of operation of the laser, the repetitively pulsed mode resulted in a two-fold improvement in shear bond strength compared with the single pulse mode. These results indicate that shear bond strengths in the order of 10 MPa can be obtained reliably on human teeth using laser conditioning with pulsed modes in the absence of any other preparation of the natural enamel surface.  相似文献   

6.
The aim of the present study was to evaluate the effect of primers on the polymerization of bonding agent. We measured the degree of conversion (radical production) and mechanical properties (surface hardness and direct tensile strength) of various adhesives/primers mixed at different ratios and the effect of varying the visible-light curing time. With and without primer treatment, the tensile bond strength of adhesive resin to micacious glass ceramic and human enamel was measured. After the tensile bond test, using the Image Capture System, the failure patterns of adhesive resin bonded to micacious glass-ceramic were analysed. The results show that the mixtures containing the higher amounts of primer yielded a lower degree of conversion and inferior mechanical properties when compared with the mixtures containing a lower proportion of primer, except in the experimental bonding system. The adhesive/primer mixtures inhibited free radical polymerization. The value for the Knoop hardness number and the direct tensile strength of the adhesive/primer mixtures were significantly decreased compared with those of the adhesive bonding agent alone with no primer added. The tensile bond strength of adhesive resin bonded to micacious glass-ceramic or human enamel without primer treatment was significantly greater than that of adhesive resin with primer treatment in certain cases. Most of the fractures of ceramic surfaces were cohesive (within resins) and/or interface (at the ceramic surface) failure.  相似文献   

7.
PURPOSE: Polishing and glazing porcelain surfaces of restorations is thought to help reduce the wear on the opposing occlusion because of reduced roughness. MATERIALS AND METHODS: To test this theory, samples of a variety of dental porcelains were prepared and subjected to various polishing and self-glazing treatments commonly used in dentistry and then viewed using scanning electron microscope (SEM). Fine cracks were discovered in the surface of the samples that had been polished and then self-glazed. These cracks were typically greater than 50 microns in length with submicron surface openings and crack depths less than 20 microns. To establish the treatments responsible for the formation of these cracks, a more controlled study was performed. Samples of Vita VMK 68 no. 559 incisal porcelain (Vita Zahnfabrik, Bad S?chingen, Germany) were prepared and subjected to six treatments (sample size = 3): treatment no. 1, as-fired condition; treatment no. 2, self-glazed (32 degrees C per minute to 960 degrees C, then cooled); treatments no. 3 and 4, wet ground followed by 1 micron diamond polish (no. 4 was then self-glazed); treatments no. 5 and 6, ground and polished using a Shofu porcelain adjustment kit (Shofu Inc, Kyoto, Japan) (no. 6 was then self-glazed). The samples were observed using SEM. RESULTS: Treatments no. 1, 2, 3, and 5 showed no cracking; however, treatments no. 4 and 6 showed cracking in all specimens (approximate levels 5,100 microns/mm2 and 3,600 microns/mm2, respectively). CONCLUSIONS: Polishing followed by self-glazing produces fine surface cracks. The rougher surface resulting from the surface cracks and subsequent porcelain chipping may cause wear of opposing occlusal surfaces.  相似文献   

8.
This study evaluated the interaction of five clinical application techniques and the shear bond strength of four DBAs (OptiBond FL, Clearfil SE Bond, PQ1 and Prime & Bond NT). A hybrid resin composite (Herculite XRV restorative resin) was attached to human dentin surfaces using five application techniques: Group A--adhesive spread with a 3M brush for 30 seconds, followed by compressed air 0.5 cm from the surface for one second to remove the excess adhesive. Group B--adhesive spread with a 3M brush for 30 seconds, followed by compressed air 0.5 cm from the surface for three seconds to remove the excess adhesive. Group C--adhesive spread with 3M brush for 30 seconds, excess adhesive removed with a clean brush, two strokes side by side, no compressed air. Group D--adhesive spread with a Micro-applicator brush for 30 seconds followed by compressed air 0.5 cm from the surface for one second to remove the excess adhesive. Group E--adhesive spread with a Micro-applicator brush for 30 seconds, the excess adhesive removed with a clean brush, two strokes side by side and no compressed air. The specimens were stored in distilled water at 37 degrees C for 24 hours, followed by thermocycling between 5 degrees C and 55 degrees C for 1,000 cycles. The shear bond strengths were determined on a universal testing machine operating with a crosshead speed of 5 mm/minute. The fracture sites were examined by 20x stereo microscope to determine the type of failure that occurred during the debonding procedure. Bond strength data were compared with analysis of variance at a significance level of p<0.05. Post hoc comparisons of means were performed with t-tests with p-values adjusted for multiple comparisons. This in vitro study concluded that there was an interaction between the application technique and bonding agent tested. All DBAs utilized the one-second compressed air technique, which yielded the highest bond strengths.  相似文献   

9.
PURPOSE: To measure and compare the in vitro shear bond strength (SBS) of the following three pairs of multi- and simplified-step dentin bonding systems: OptiBond vs. OptiBond FL, All-Bond 2 vs. One-Step, and Tenure vs. Tenure Quik. MATERIALS AND METHODS: 60 extracted human mandibular molars were sectioned perpendicular to the long axis 1 mm above the CEJ to expose the dentin bonding surface. After being wet-ground to 600 grit with SiC abrasive papers, rinsed and dried, the teeth were individually mounted in phenolic rings with epoxy resin, and randomly assigned into six equal groups of 10 each. The dentin surfaces were treated with the above mentioned dentin bonding systems, and a gelatin cylinder filled with resin composite (Pertac-Hybrid) was directly bonded to each pretreated surface. After 7-day storage in 37 degrees C water followed by thermocycling, the specimens were shear tested to failure on an Instron machine. Data were analyzed by independent t-tests, one-way ANOVA, and Duncan's Multiple Comparison tests at alpha = 0.05. RESULTS: Except for the pair Tenure/Tenure Quik, the differences between the pairs All-Bond 2/One-Step and OptiBond/OptiBond FL were statistically significant with All-Bond 2 and OptiBond FL yielding higher shear bond strength (P < 0.05). Findings of this study indicated that OptiBond FL was the only simplified-step system showing improved bond strength.  相似文献   

10.
环境障涂层体系中粘结层与基体的结合性能是评价其质量的重要指标之一。本文针对环境障涂层中硅粘结层与硅基陶瓷材料结合性能不理想的问题,采用Na2CO3和Na2SO4熔盐作为蚀刻剂对SiC陶瓷表面进行粗糙化处理,研究了SiC陶瓷表面熔盐处理后的显微形貌、粗糙度以及物相组成。采用真空等离子喷涂技术制备了Si涂层,采用划痕法、压痕法以及拉伸结合强度测试法表征了涂层-基体界面的性能,发现采用高温熔盐处理方法可以显著提高Si涂层与SiC陶瓷之间的界面结合性能。本工作初步验证了高温熔盐处理方法是一种有效的陶瓷表面粗糙化处理技术。  相似文献   

11.
To understand the role of NMAA in the bonding of composite resin to a dentin surface, we investigated the effects of N-methacryloyl amino acid (NMAA) application on the expansion of aggregated collagen fibers, formation of a hybrid layer, and the tensile bond strength between composite resin and dentin. Four NMAA derivatives--N-methacryloyl-alpha-glycine (NMGly), N-methacryloyl-gamma-amino n-butyric acid (NMBu), N-methacryloyl-alpha-hydroxyproline (NMHPro), and N-methacryloyl-alpha-glutamic acid (NMGlu)--were prepared and applied to dentin surfaces which had been etched with 40% by mass H3PO4 and air-blown. The shrunken collagenous layer expanded by approximately 50% to 70% by volume of the original collagenous layer thickness after application of the NMAA primers. Application of the bonding agent and composite resin after NMAA treatment resulted in the formation of a hybrid layer. The thickness of the hybrid layer was somewhat smaller than the collagenous layer formed by the NMAA treatment only, regardless of the type of NMAA used. The thickness of the hybrid layer was approximately ten times larger than that formed without NMAA treatment. Although all NMAA primers formed hybrid layers of similar thickness, higher tensile bond strengths, from 13 to 15 MPa, were obtained when etched and air-blown dentin was treated with NMBu, NMGly, or NMGlu. NMHPro gave only 6.6 MPa, a value similar to that obtained when no NMAA was used. We concluded, therefore, that formation of the hybrid layer is a necessary but insufficient condition for high bond strength.  相似文献   

12.
PURPOSE: To compare bond strengths of fresh resin composites to previously polymerized ("aged") composites following various surface treatments. MATERIALS AND METHODS: Eighty Pertac Hybrid (PH) and an equal number of Silux Plux (SLX) specimens were fabricated and stored for 1 week prior to surface treatment. The specimens were then polished and stored for an additional 24 hours prior to final surface treatment. The surface treatments included use of one of the following: (1) diamond bur (DB), (2) microetcher with 50 microns Al2O3@80 psi pressure (ME), (3) high-pressure air abrasion with 27 microns Al2O3@psi, (KCP), or (4) low-pressure silicate ceramic deposition using 30 microns particles@34 psi (CJ-S) with a microetcher. Half of the samples were treated with a silanating agent. Fresh resin composite (same type as used for the aged specimen) was bonded to the treated surfaces, and specimens were then stored 24 h and thermocycled 300 x at 5 degrees and 55 degrees C prior to testing for shear bond strength. Two-way ANOVA was used to determine significant differences between mean shear bond strengths for both composite materials. RESULTS: Significant differences were found between the groups for both surface treatment and silane use (P < 0.05). The interaction between the two main effects was also significant (P < 0.05). Overall, the highest bond strengths were found when the low-pressure silicate ceramic deposition system (CJ-S) was used, with or without silane.  相似文献   

13.
PURPOSE: The retention forces of a newly developed compomer cement (Dyract Cem), a glass ionomer cement (Ketac Cem Aplicap), and a resin cement (F21) were examined. MATERIAL AND METHODS: Cemented cast gold crowns were removed along the path of insertion with a Zwick universal testing device. The impact of both a cured and a noncured additional bonding layer that were applied to the inner surface of the crowns was examined across the Dyract Cem group. RESULTS: The mean adhesive strength was measured at 2.36 +/- 0.69 N/mm2 in the Ketac Cem group, at 0.60 +/- 0.28 N/mm2 in the F21 group, and at 1.85 +/- 0.94 N/mm2 in the Dyract Cem group, respectively. The application of an additional bonding layer to the inner surface of the crowns did not significantly improve the retentive strength of Dyract Cem; the respective mean strengths were observed at 1.46 +/-0.33 N/mm2 for the uncured and at 1.70 +/- 0.76 N/mm2 for the cured bonding layers. CONCLUSIONS: Dyract Cem and Ketac Cem showed significantly higher retentive strengths than F21 (p < 0.001, Wilcoxon test, 5% level). No significant difference was found in bond strength between Ketac Cem and Dyract Cem.  相似文献   

14.
The normalization process and high- temperature temper process were used to investigate the effect of heat treatments on the microstructure and mechanical properties of bond interfaces. The SEM and EDS were used to discuss the microstructure and element diffusion after heat treatment. And the interfacial bond strength was obtained by compression shear test on the testing machine. With the fractured surface morphology analysis, the composition of phases at the bond interface was analyzed by XRD. The experimental results show that a small quantity of brittle intermetallic compound Fe2Nb phases are observed at the bonding interface of the Q235- Nb bonds after heat treatment, and needle structure is formed at Nb- Ti interface after normalization treatment. The compression shear strength of normalized specimens(171MPa) at 900?? is slightly higher than that of the high- temperature tempered specimens(162MPa) processed at 650??. Observation of fracture surfaces demonstrations that the failure takes place through the bonding interface of the Q235- Nb bonds during all the shear tests, the compression shear strength is lower at Q235- Nb interface than at Nb- Ti interface.  相似文献   

15.
Researchers have carried out a variety of investigations to determine the properties of available dentin bonding systems. The test methods and variables used in 50 published investigations of bond strength were analyzed. Among the studies analyzed, shear tests predominated, being used in 80% of the studies; dentin from human molar teeth was used most often (in 88% of investigations); and the most prevalent time of testing was 24 hours postcuring. However, a number of potential variables were not recorded in a high proportion of articles, among these the film thickness, the type of dentin tested, and the surface condition (moist or dry). The mode of failure was recorded in only 42% of the investigations assessed. It was found that there is little standardization of test methods in studies of dentin bond strength and that a number of variables are often either not recorded or reported.  相似文献   

16.
This study compared the tensile bond strengths of soft lining materials polymerized by using conventional water bath methods and microwave energy. The soft lining materials used in this investigation were heat temperature vulcanizing (H.T.V.) silicon material Molloplast-B, and room temperature vulcanizing (R.T.V) acrylic material Getz Soft Oryl. The H.T.V. specimens were prepared with retention, additional retention and without retention, and the R.T.V. specimens were prepared by using bonding agent and bonding agent plus retention. All were cured by both conventional water bath and microwave energy. Results showed that the mean bond strength of H.T.V. specimens ranged from 9.6 to 13.12 kg/cm2, while the mean bond strength of R.T.V. specimens ranged from 0.36 to 1.75 kg/cm2. In both conventional and microwave groups, the specimens prepared with retention, additional retention and without retention or using bonding agent and bonding agent plus retention did not show any significant difference when they were compared separately. But the difference between conventional and microwave groups was found significant in both H.T.V. and R.T.V. specimens. It showed that conventional water bath technique is better than microwave technique.  相似文献   

17.
Spin-bonding is a novel tube cladding method for fabrication of bilayer tubes based on flow-forming process. The bimetal Al/St tubular components have extensive application in different industries. In this paper, an Al/St bimetal tube was successfully produced at different thickness reductions from 35 to 65% and mechanical and metallurgical aspects of the joint were investigated. Peeling tests were done to investigate the strength of the bond. The results showed that an increase in the thickness reduction led to a significant increase in the bond strength. Besides, the bonding mechanism between Al as inner tube to St as an outer one resulting from spin-bonding process was investigated. The results showed that an excellent bonding of Al and St tubes could be achieved from this process. The results showed that the bonding process consisted of three stages. First, removal of surface layers resulting in contact between the virgin metals of two bond surfaces and then an unstable bond was formed that stabilized as deformation proceeded. Finally the bond strengthening occurred. The SEM micrographs of the peeled surfaces showed that removing surface films in aluminum and steel in the first stage was based on different mechanisms. Also, SEM back-scatter images of bond interface showed that no intermetallic phases were formed.  相似文献   

18.
Structural repair and strengthening have long been dynamic and challenging activities in construction work. One of the most commonly used methods for such repairs is the application of fiber-reinforced polymer (FRP) sheets to strengthen RC or even steel structure members. A major issue of concern in flexural strengthening of RC beams with FRP laminates is the debonding of the concrete substrate, which leads to premature failure of the structural member thus strengthened. One reason for this premature rupture may be the lack of proper preparation of the concrete surface in contact with the FRP sheet. Surface preparation is typically associated with such constraints as adverse environmental impacts, economic losses due to stoppage of activities, repair costs, or even inaccessibility of the member(s) to be strengthened. This study aims to investigate surface preparation for application of FRP sheets in an attempt to develop substitute methods for conventional surface preparation methods. The experimental specimens used for the purposes of this study included a minimum of 100 prism specimens of dimensions 100×100×500?mm subjected to four-point flexural loading. The specimens were divided into the two control and experimental groups. The control group lacked FRP sheets, while the experimental one had FRP sheets tested for their ultimate failure strength as a result of both surface preparation and transverse, longitudinal, and diagonal grooves as substitutes for surface preparation. The results indicated that surface preparation prior to bonding of FRP sheets increased ultimate rupture strength. It was also found that the substitute preparation methods greatly compensated for the lack of conventional surface preparation such that they changed, in some cases, the ultimate failure behavior of the member.  相似文献   

19.
In this paper, we evaluated performance-enhancing modifications of the coating surface for a diesel engine piston. Thermal barrier coatings were applied to insulate the substrate from higher operating temperatures. A top coat (0.4 mm thick) and bond coat (0.1 mm thick) were applied to the aluminum alloy piston crown for analysis. Yttria-stabilized zirconia was used for the top coat and NiCrAl alloy was used for the bond coat. A static thermal analysis was performed to determine the temperature distribution at the top and substrate surface. Holes (2, 3, 4 and 5 mm in diameter) were created on the surface of the coating and the temperature distribution was analyzed. Comparison of the results with those of an uncoated piston revealed that the temperature of the substrate was decreased while temperature of the top surface was increased. Decreasing the temperature of the substrate reduced thermal fatigue while increasing the temperature of the top surface reduced fuel consumption thus leading to an overall improvement in performance. The lowest substrate temperature obtained was for a coated surface with 2 mm diameter holes, whereas the highest top surface temperature obtained was for a coated surface with 5 mm diameter holes.  相似文献   

20.
Previous studies have demonstrated the ability of the argon laser to polymerize light-activated materials and improve enamel shear bond strengths. This study was conducted to evaluate the effects of the argon laser on dentin shear bond strengths of current dentin bonding systems. Argon laser (HGM Model 8) at 231 and 280 mW, 5 sec bonding agent, 10 sec composite, and a conventional curing light (Translux EC/Kulzer) at 10 sec bonding agent, 20 sec composite were used to polymerize samples of dentin bonding systems [Scotchbond Multi-Purpose Plus (3M) and Prime Bond (Dentsply/Caulk), both with TPH (Dentsply/Caulk) composite]. A flat dentin bonding site (600 grit) was prepared on the buccal surface of extracted human teeth. Twelve samples were made for each set of parameters for both laser and conventional light totaling 48 samples. Samples were stored in distilled water in light-proof containers for 24 h at 37 degrees C. Shear bond strengths (MPa) were determined for each sample on the Instron testing machine. Mean values were calculated for each set of data and ANOVA with Fisher PLSD were used for statistical analysis. The argon laser provided bond strengths that were 21-24% greater than those of the conventional curing light system.  相似文献   

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