Microstructure feature of friction stir butt-welded ferritic ductile iron

This study conducted friction stir welding (FSW) by using the butt welding process to join ferritic ductile iron plates and investigated the variations of microsturcture in the joined region formed after welding. No defects appeared in the resulting experimental weld, which was formed using a 3-mm thick ductile iron plate and tungsten carbide alloy stir rod to conduct FSW at a rotational speed of 982 rpm and traveling speed of 72 mm/min. The welding region was composed of deformed graphite, martensite phase, and dynamically recrystallized ferrite structures. In the surface region and on the advancing side (AS), the graphite displayed a striped configuration and the ferritic matrix transformed into martensite. On the retreating side (RS), the graphite surrounded by martensite remained as individual granules and the matrix primarily comprised dynamically recrystallized ferrite. After welding, diffusion increased the carbon content of the austenite around the deformed graphite nodules, which transformed into martensite during the subsequent cooling process. A micro Vickers hardness test showed that the maximum hardness value of the martensite structures in the weld was approximately 800 HV. An analysis using an electron probe X-ray microanalyzer (EPMA) indicated that its carbon content was approximately 0.7–1.4%. The peak temperature on the RS, 8 mm from the center of the weld, measured 630 °C by the thermocouple. Overall, increased severity of plastic deformation and process temperature near the upper stir zone (SZ) resulted in distinct phase transformation. Furthermore, the degree of plastic deformation on the AS was significantly greater than that on the RS, and relatively complete graphite granules and the fine ferrite grains resulting from dynamic recrystallization were observed on the RS.     

Effect of backplate diffusivity on microstructure and mechanical properties of friction stir welded joints

Series of welds were made by friction stir welding (FSW) with various backplates made out of materials ranging from low diffusivity granite to high diffusivity copper in order to reveal the effect of backplate diffusivity on the joint microstructure and properties. The temperature, microstructure, microhardness and tensile properties of joints were compared and discussed. Results show that the backplate with high diffusivity effectively decreases the heat input to the workpiece during FSW. With decreasing the backplate diffusivity the sizes of equiaxed recrystallized grains in the nugget zone increase obviously, while the hardness of the nugget zone also increases a little. The interface between the thermo-mechanically affected zone and nugget zone at the retreating side disappears under the granite backplate. Moreover, the ductility of the joint is more excellent under the copper backplate, but under the granite backplate the failure has mixed fracture characteristics of quasi-cleavage and dimples.     

Force response characteristics and mechanical properties of friction stir welded AA2024 sheets

Process force and tensile properties in friction stir welding of AA2024 sheets were studied. Results show that the forces present a periodic variation with the same periodicity which is nearly equal to the time of one tool rotation, and thus it only depends on rotation speed. With increasing welding speed the forces increase gradually, while with increasing rotation speed the forces first decrease and then increase. Joints with superior strength-ductility synergy are produced at 900?rev?min^?1–300?mm?min^?1 and 1000?rev?min^?1–350?mm?min^?1. These joints experience nearly the same peak temperature and axial force. As heat input increases the failure initiates from the interface between nugget zone (NZ) and thermo-mechanically affected zone to heat-affected zone continuing to NZ.     

Friction stir welding of aluminium hollow extrusion: weld formation and mechanical properties

Novel friction stir welding (FSW) technique, characterised by big concave upper and small convex lower shoulders, for aluminium hollow extrusion was studied. Assisted with the lower shoulder, root flaws due to the lack of tool penetration have been eliminated. The tensile strength increased with increasing welding speed. As the welding speed increases from 50 to 200 mm min^?1, the width of the welding nugget zone (WNZ) decreases, and the ductile fractured location occurred at WNZ instead of heat affected zone (HAZ) adjacent to thermomechanically affected zone (TMAZ). The interface between the TMAZ and HAZ exhibited the lowest microhardness. The results indicated that the novel FSW method has the potential to join tubular structures and hollow profiles widely used in transportation industries.     

Friction stir welding of mild steel: tool durability and steel microstructure

Abstract

In previous work, we have established a scheme that exploits a three-dimensional heat and mass flow model to assess tool durability and define the domains of satisfactory tool life in the context of welding difficult aluminium alloys. We now apply this scheme to the friction stir welding of steel and extend the calculations to cover consequences on the microstructure of the steel while optimising tool life. This is the first published model that covers both the processing parameters and the consequences on the physical metallurgy of the steel.     

Mechanical properties and microstructure of friction stir welded tailor-made blanks

This paper studies the microstructural features and mechanical properties of friction stir welds with dissimilar alloys and different thicknesses. The welds are produced in five different thickness/material combinations from 2024-T3 and 7075-T6 sheets with different thicknesses. A parametric study is conducted to optimize the welding parameters such that the different configurations can be compared. The paper is divided into two chapters: microstructural features and mechanical properties. In the first chapter, a study of the chemical composition and microstructure of the welds shows that a narrow chemical mixing zone is present in the dissimilar-alloy welds and that the stirring zone embodies the union rings and exhibits heterogeneous texture for most configurations. Study of the hardness, tensile properties and fracture surfaces in the second chapter shows that an asymmetric softened region, which is harder at the advancing side and extends more into the retreating side, is formed in the stirring zone and that the mechanical properties decrease as the thickness ratio increases. The fracture was partially ductile and partially brittle for all configurations.     

Influence of tool geometry and rotational speed on mechanical properties and defect formation in friction stir lap welded 5456 aluminum alloy sheets

Friction stir welding of AA5456 aluminum alloy in lap joint configuration is with two different tempers, T321 and O, and different thicknesses, 5 mm and 2.5 mm was investigated. The influences of tool geometry and various rotational speeds on macrostructure, microstructure and joint strength are presented. Specifically, four different tool pin profiles (a conical thread pin, a cylindrical–conical thread pin, a stepped conical thread pin and Flared Triflute pin tool) and two rotational speeds, 600 and 800 rpm, were used. The results indicated that, tool geometry influences significantly material flow in the nugget zone and accordingly control the weld mechanical properties. Of particular interest is the stepped conical threaded pin, which is introduced for the first time in the present investigation. Scanning electron microscopy investigation of the fracture location of samples was carried out and the findings correlated with tool geometry features and their influences on material flow and tension test results. The optimum microstructure and mechanical properties were obtained for the joints produced with the stepped conical thread pin profile and rotational speed of 600 rpm. The characteristics of the nugget zone microstructure, hooking height, and fracture location of the weld joints were used as criteria to quantify the influence of processing conditions on joint performance and integrity. The results are interpreted in the framework of physical metallurgy properties and compared with published literature.     

Achieving ultra-high strength friction stir welded joints of high nitrogen stainless steel by forced water cooling

The microstructure and properties of water-cooled and air-cooled friction stir welded (FSW) ultra-high strength high nitrogen stainless steel joints were comparatively studied. With additional rapid cooling by flowing water, the peak temperature and duration at elevated temperature during FSW were significantly reduced. Compared to those in the air-cooled joint, nugget zone with finer grains (900 nm) and heat affected zone with higher dislocation density were successfully obtained in the water-cooled joint, leading to significantly improved mechanical properties. The wear of the welding tool was significantly reduced with water cooling, resulting in better corrosion resistance during the immersion corrosion test.     

Influences of joint geometry on defects and mechanical properties of friction stir welded AA6061-T4 T-joints

In this paper, AA6061-T4 T-joints with three different joint geometries of T-lap/T-butt-lap/T-butt were fabricated successfully by friction stir welding. The distributions and formation mechanisms of defects in friction stir welded (FSWed) T-joints were discussed through macro and micro-observations, respectively. Hardness profiles of the as-welded samples were also measured to evaluate the softening effect during the process. What’s more, influences of joint geometry and the traverse speed on the tensile properties of FSWed T-joints were investigated. All the experimental results indicate that tunnel defects and kissing bond are easily formed and vary significantly in T-joints of the three joint geometries. Defects are moderated to a large extent with decreasing the traverse speed, but the specific relationship to tensile properties is complicated. T-lap joints present the superior tensile properties along the skin direction among the three geometries, the same as T-butt joints along the stringer direction. All the as-welded samples almost fractured in the locations of softening zones and bonding surfaces.     

Microstructure,microhardness and corrosion susceptibility of friction stir welded AlMgSiCu alloy

Microstructure, microhardness and corrosion susceptibility of friction stir welded joint in an AlMgSiCu alloy were investigated. It was found that the joint exhibits different corrosion susceptibility among the microstructural zones. The base material is the most susceptible to intergranular corrosion because of the presence of continuous cathodic precipitates (Si and Q phases) at grain boundaries and the precipitate free zone along the grain boundaries. The coarsening of intergranular precipitates and the precipitation of Q′ phases in the grain bodies reduce intergranular corrosion susceptibility but introduce pitting corrosion in the heat-affected zone. The significant elimination of intergranular corrosion both in nugget zone and thermo-mechanically affected zone is related to the low volume fraction of intergranular precipitate. Microhardness variations depend on the evolution of intragranular precipitates. The dissolution and/or coarsening of the strengthening precipitates result in the softening within the welded zone.     

Effects of peening on mechanical properties in friction stir welded 2195 aluminum alloy joints

The effects of surface treatment techniques like laser and shot peening on the mechanical properties were investigated for friction stir welded 2195 aluminum alloy joints. The loading in the tensile specimens was applied in a direction perpendicular to the weld direction. The peening effects on the local mechanical properties through the different regions of the weld were characterized using a digital image correlation technique assuming an iso-stress condition. This assumption implies that the stress is uniform over the cross-section and is equal to the average stress. The surface strain and average stress were used giving an average stress–strain curve over the region of interest. The extension of the iso-stress assumption to calculate local stress–strain curves in surface treated regions is a novel approach and will help to understand and improve the local behavior at various regions across the weld resulting in a sound welding process. The surface and through-thickness residual stresses were also assessed using the X-ray diffraction and the contour methods. The laser peened samples displayed approximately 60% increase in the yield strength of the material. In contrast, shot peening exhibited only modest improvement to the tensile properties when compared to the unpeened FSW specimens. The result that laser peening is superior to shot peening because of the depth of penetration is original since this superiority has not been presented before regarding mechanical properties performance.     

Contribution of ultrasonic to microstructure and mechanical properties of tilt probe penetrating friction stir welded joint

Tilt probe penetrating friction stir welding(PFSW)was an innovative technology proposed in recent years to avoid the formation of kissing bond in the root of joint.However,with the heat input decreasing,"S"line or zigzag line was easily introduced in the PFSW joint.In this study,ultrasonic enhanced tilt probe penetrating friction stir welding(U-PFSW)was developed to solve this problem and achieve improved joint mechanical properties.The experimental results confirmed that U-PFSW was a potent technology to completely clear the original butt surface,providing a crucial prerequisite for the achievement of high-strength joint.The application of ultrasonic improves the joint tensile strength and fracture elongation from 336 MPa and 4.3％to 359 MPa and 6.8％,respectively.Furthermore,the strength of stir zone was also increased from 391 MPa in PFSW to 420 MPa in U-PFSW.Analyses of texture and precipitate indi-cated that the dynamic recrystallization(DRX)and precipitation strengthening were both enhanced by the ultrasonic.Ultrasonic-enhanced DRX enabled a complete elimination of the"S"line;the enhanced precipitation strengthening by vacancy-induced mechanism in U-PFSW was the intrinsic reason for the significantly improved mechanical properties.     

Friction stir based welding and processing technologies - processes,parameters, microstructures and applications: A review

Friction stir welding (FSW) has achieved remarkable success in the joining and processing of aluminium alloys and other softer structural alloys. Conventional FSW, however, has not been entirely successful in the joining, processing and manufacturing of different desired materials essential to meet the sophisticated green globe requirements. Through the efforts of improving the process and transferring the existing friction stir knowledge base to other advanced applications, several friction stir based daughter technologies have emerged over the timeline. A few among these technologies are well developed while others are under the process of emergence. Beginning with a broad classification of the scattered frictions stir based technologies into two categories, welding and processing, it appears now time to know, compile and review these to enable their rapid access for reference and academia. In this review article, the friction stir based technologies classified under the category of welding are those applied for joining of materials while the remnant are labeled as friction stir processing (FSP) technologies. This review article presents an overview of four general aspects of both the developed and the developing friction stir based technologies, their associated process parameters, metallurgical features of their products and their feasibility and application to various materials. The lesser known and emerging technologies have been emphasized.     

Modification of mechanical properties of friction stir welded Cu joint by additional liquid CO2 cooling

A notable effect of the retained heat after the fiction stir welding (FSW) of Cu was studied by the application of additional liquid CO₂ cooling. The adjustment of the welding parameters made it possible to conduct the FSW processes, but the cooling rate of the joint was not sufficiently changed due to the existence of the post-annealing effect. However, the accelerated cooling can reduce the post-annealing effect and provide an ultrafine grain structure with a high dislocation density in the stir zone, and a joint with mechanical properties better than the base metal level was achieved.     

Microstructure at friction stir lap joint interface of pure titanium and steel

A commercially pure titanium plate was lap joined to a structural steel plate via friction stir welding, and the microstructures at the lap joint interface were intensively examined by means of electron backscatter diffraction analysis and transmission electron microscopy. Swirling-like macro- and micro-intermixing zones of titanium and steel are formed along the interface, where tiny Fe-Ti intermetallic particles are dispersed and mixed with β titanium in layers. The lap joint has high shear tensile strength, which is supposed to result from the dispersion of tiny Fe-Ti intermetallic particles and the formation of β titanium at the joint interface.     

Friction stir spot welding of SPCC low carbon steel plates at extremely low welding temperature

Friction stir spot welding(FSSW) was applied to 2.0 mm thick steel plate cold-rolled commercial(SPCC)low carbon steel plates at a very low rotation speed that ranged from 5 to 50 rpm, which was much lower than that generally used for the conventional FSSW technique. Due to the very low heat input, the welding processes could therefore be completed at a peak welding temperature below 160℃. As a result,a significantly refined microstructure with an average grain size of about 0.41 μm was formed in the stir zone of the joints and the J1{0–11}-211 and J2{1–10}-1–12 shear textures were the dominant components, which are different from the D1{11–2}111 and D2{-1–12}111 shear textures formed in the conventional FSSW joints. In addition, no heat affected zone could be detected along the crosssectional plane of the joints. Although a few void-like non-bonded areas were still observed along the interface between the upper and lower steel plates, the shear tensile loads of the joints increased to about 10.0 kN when welded at a condition of 8 t, 20 rpm and 30s, and the joints fractured through the plug failure mode.     

Process optimisation and mechanical properties of friction stir lap welds of 7075-T6 stringers on 2024-T3 skin

This paper focuses on the results of process optimisation and mechanical tests that were used to ascertain the feasibility of using friction stir welding (FSW) to join stringers to skin. The effects of process parameters on weld quality of 1.5-mm 7075-T6 stringers lap-joined on 2.3-mm 2024-T3 skins were investigated. Advancing and retreating side locations on the joint configuration were alternated to determine optimal design arrangements. The effects of travel and rotation speeds on weld quality and defect generation were also investigated. Weld quality was assessed by optical microscopy and bending tests. It was found that: (i) the increase of the welding speed or the decrease of the rotational speed resulted in a reduction of the hooking size and top plate thinning but did not eliminated them, (ii) double pass welds by overlapping the advancing sides improved significantly the weld quality by overriding the hooking defect, and (iii) change of the rotational direction for a counter clockwise with a left-threaded probe eliminated the top sheet thinning defect. Subsequently, FSW lap joints were produced using optimum conditions and underwent extensive mechanical testing program. Several assembly configurations including discontinuous and continuous welds as well as single and double pass welds were produced. The results obtained for cyclic fatigue performance of FSW panels are compared with riveted lap joints of identical geometry. S–N curves, bending behaviour, failure locations and defect characterisation are also discussed. It was found that: (i) the tensile strength of FSW joints approached that of the base material but with a significant reduction in the fatigue life, (ii) the probe plunge and removal locations served as the key crack nucleation sites in specimens with discontinuous welds, and (iii) double pass welds with overlapping advancing sides showed outstanding fatigue life and very good tensile properties. The present work provided some valuable insight into both the fabrication and application of FSW on stringer/skin lap joints.     

Effect of tool pin eccentricity on microstructure and mechanical properties in friction stir welded 7075 aluminum alloy thick plate

Four different tools with the pin eccentricity of 0.1 mm, 0.2 mm, 0.3 mm and 0.4 mm were designed to friction stir weld 10 mm thick AA7075-O plate. The effect of pin eccentricity on microstructure, secondary phase particles transformation and mechanical properties of the joints was investigated. The results show that the nugget area (A_NZ) increases firstly and then decreases with increasing the pin eccentricity. When the pin with 0.2 mm eccentricity is applied, the A_NZ is the largest; meanwhile the grains size is the smallest which is about 3 μm and secondary phase particles are the most dispersive in nugget zone compared with other tools. While the grains are coarsened to 7–11 μm as the eccentricity is more than 0.4 mm, some coarse hardening particles get to cluster in the thermo-mechanically affected zone. The joints produced by the pin with 0.2 mm eccentricity perform the highest tensile strength and elongation, which is attributed to better interfaces, finer grains and more dispersive secondary phase particles.     

Improving mechanical properties of pinless friction stir spot welded joints by eliminating hook defect

Hook defect (HD) seriously decreases the mechanical properties of friction stir spot welded (FSSW) joints. In this study, two methods were therefore used to eliminate the HD in pinless FSSW joints. The one is changing welding parameters such as rotating speed and dwell time. The other one is FSSW plus subsequent friction stir welding (FSSW-FSW), which is an innovative method proposed in this study. Experimental results showed that the HD in pinless FSSWed AA2024 joints was successfully eliminated by using FSSW-FSW, not by changing process parameters. The joints without HD exhibited a tensile–shear load of as much as 12 kN, which was higher than that of 6.9 kN in the joints with HD. Furthermore, it was proved that the tensile–shear load is not greatly improved only by increasing the nugget zone when HD still existed in the FSSW joints. In addition, the fracture morphology analysis demonstrated that the shear fracture of the FSSW-FSW joints took place along the boundary between the upper and lower sheets through the weld nugget, and the faying surface between the two sheets was completely sheared off.     

Inhomogeneity of microstructure and mechanical properties in the nugget of friction stir welded thick 7075 aluminum alloy joints

In this study, 20 mm thick AA7075-T6 alloy plates were joined by friction stir welding. The microstructure and mechanical properties of the nugget zone along the thickness direction from the top to the bottom was investigated. The results showed that the microstructure including the grain size, the degree of dynamic recrystallization, the misorientation angle distribution and the precipitation phase containing its size, type and content exhibited a gradient distribution along the thickness direction. The testing results of mechanical properties of the slices showed that the nugget was gradually weakened along the depth from the top to the bottom. The maximum ultimate tensile strength, yield strength and elongation of the slice in the nugget top-middle are obtained, which are 415 MPa, 255 MPa and 8.1%, respectively.