硅藻土-木桨纤维为助滤剂强化过滤过程的研究(英文)

In this paper, a study to enhance the filtration for solid/liquid materials difficult to be filtered, such as highly viscous, highly compactible or gel like materials, is presented. Filter aids diatomaceous earth and wood pulp cellulose are used to enhance the filtration by improving filter cake structure and properties in the filtration of a biological health product and a highly viscous chemical fiber polymer melt product. The property of solid/liquid systems, filtration at different flow rates, specific cake resistance, cake wetness, filtration rate, filtrate turbidity for filter aid selection and evaluation, and operation optimization are investigated. The results are successfully applied to industrial process, and can be used as a reference for similar filtration applications.     

陶瓷过滤管表面粉尘层清除过程的图像分析

Based on the analysis of high-speed video images, the detachment behavior of dust cake from the ceramic candle filter surface during pulse cleaning process is investigated. The influences of the dust cake loading,the reservoir pressure, and the filtration velocity on the cleaning effectiveness are analyzed. Experimental results show that there exists an optimum dust cake thickness for pulse-cleaning process. For thin dust cake, the patchy cleaning exists and the cleaning efficiency is low; if the dust cake is too thick, the pressure drop across the dust cake becomes higher and a higher reservoir pressure may be needed. At the same time there also exists an optimum reservoir pressure for a given filtration condition.     

关于过滤理论与滤饼可压缩性的探讨

This paper gives a study on the rates of filtration and cake formation and filter cakes permeability and compressiblity．A new calculating equation of filter cakes special resistance is advanced，It indicates that the permeability of filter cake is not only related with slurry concentration and its settling velocity，but also related with the pretreatment and chemical environment of slurry．     

Experimental study on the effects of big particles physical characteristics on the hydraulic transport inside a horizontal pipe

This paper presents an experimental study of the physical characteristic effects of large particles on hydraulic transport in a horizontal pipe. The particles are spherical and are large with respect to the diameter of the pipe (8%, 10%, 16%and 25%). Experiments were done to test the important parameters in solid transport (pressure, velocity, etc.). As a result, the relationship between the pressure gradient forces and the mixture velocity was sub-stantially different from the pure liquid flow. However, in a single-phase flow a monotonous behavior of the pres-sure drop curve is observed, and the curve of the solid particle flow attains its minimum at the critical velocity. The regimes are characterized with differential pressure measurements and visualizations.     

二氧化硫和二氧化碳在离子液体支撑液膜中的渗透率和选择性

Permeabilities and selectivities of gases such as carbon dioxide (CO2), sulfur dioxide (SO2), nitrogen (N2) and methane (CH4) in six imidazolium-based ionic liquids ([emim][BF4], [bmim][BF4], [bmim][PF6], [hmim][BF4], [bmim][Tf2N] and [emim][CF3SO3]) supported on polyethersulfone microfiltration membranes are investigated in a single gas feed system using nitrogen as the environment and reference component at temperature from 25 to 45ºC and pressure of N2 from 100 to 400 kPa. It is found that SO2 has the highest permeability in the tested supported ionic liquid membranes, being an order of magnitude higher than that of CO2, and about 2 to 3 orders of magnitude larger than those of N2 and CH4. The observed selectivity of SO2 over the two ordinary gas components is also striking. It is shown experimentally that the dissolution and transport of gas components in the supported ionic liq-uid membranes, as well as the nature of ionic liquids play important roles in the gas permeation. A nonlinear in-crease of permeation rate with temperature and operation pressure is also observed for all sample gases. By considering the factors that influence the permeabilities and selectivities of CO2 and SO2, it is expected to develop an optimal supported ionic liquid membrane technology for the isolation of acidic gases in the near future.     

Enhancement of fine particle filtration with efficient humidification

Filtration is one of the most effective methods to remove suspended fine particles from air. In filtration processes,pressure drop of compact dust cake causes problems in efficiency and economy, which has received increasing attention and still remains challenging. In this study, we developed a novel technique to intensify the filtration of fine particles with efficient humidification. Two strategies for humidification, including ultrasonic atomization and steam humidification(controlling of ambient humidity), were employed and proved to be both effective. The regeneration frequency of the filter could be reduced by 55% with ultrasonic atomization, while steam humidification could lead to a 78% reduction in regeneration frequency. The effect of operating conditions on pressure drop and the mass loading during filtration were investigated. The dust cake showed a loose and porous structure with an optimized droplet-to-particle ratio. With the ratio of 1.53 and 0.0282, the maximum mass loading was 552 g·m-2upon the ultrasonic atomization and 720 g·m-2upon the steam humidification. The results show that humidification could slow down the increase of pressure drop during filtration and improve the efficiency of process.     

多管陶瓷过滤器内耦合效应数值模拟

The Reynolds stress transport model and the Eulerian two-fluid model provided by the FLUENT code were applied to evaluate the gas-particle two-phase flow in the ceramic filter vessel. The ceramic filter vessel contains six candle filters, which are arranged in the form of equilateral hexagon. The variation of the areal density of the filter cake during the filtration and the back-pulse process were analyzed. The coupling effect between filters, gas and solid, filtration and pulse cleaning process were investigated, respectively. The numerical results show a good approach to predict the particle distribution in the vessel and the particle deposition on the filter element. This study provides the base for the intensive study on the analysis of the gas-particle flow in the filter vessel.     

等效滤饼过滤模型

Cake filtration has been widely used in many chemical processes with more non-Newtonian, highly viscous and compressible materials involved. Neither traditional nor modem filtration theory can be applied in practice ＂Equivalent cake filtration model＂ is a recently developed mathematical model to describe cake filtration for both Newtonian and non-Newtonian fluids, in either steady or unsteady filtration stages. This model has two strengths： （1） It can be used to determine equivalent capillary radii and predict filtration quality based on the properties of solid/liquid system and operation parameters; and （2） to calculate cake specific resistance and its variations with time at various cake thickness locations.     

精馏塔的压降测量研究(英文)

Pressure drops are of major importance for distillation/absorption columns. This paper mainly discusses how to correctly measure, interpret and use pressure drop data. The possible causes of incorrect pressure drop measurements are studied including the effects of pressure tap dimensions, locations, and vapor condensation etc. The effect of the static head of vapor on the pressure drop data and column pressures is evaluated. Variations of sec-tional pressure drops along the column are investigated based on the experimental data obtained from commercial size distillation columns at Fractionation Research, Inc. (FRI). For a packed column, it is found that the spacing between the liquid distributor and the top of the bed affects the overall pressure drop measurements, which is con-firmed by a fundamental fluid dynamics analysis.     

恒压过滤介质阻力分析

A mathematical model for constant pressure filtration is established. The distribution of hydraulic pressure within the cake and the medium resistance are measured. The medium resistance Rm is calculated from the suppositional filtration time Ore. It is demonstrated that Rm is nearly a constant for a given filter cloth.     

The Permeability Distribution (PD) Method for Filter Media Characterization

Cake filtration is frequently used for the removal of particulate solids from fluids in industrial processes. The build up of a filter cake is usually accompanied by a decrease in overall permeability of the filter leading to an increased pressure drop over the filter medium. For an incompressible filter cake that builds up on a homogeneous filter cloth (surface filtration mode), a linear pressure drop profile is expected over time. However, occasionally experiments show curved pressure drop profiles. Whereas pressure drop profiles with increasing slope are generally ascribed to cake compression and/or depth filtration, pressure drop profiles with decreasing slopes are only ascribed to inhomogeneities in the filter. Such inhomogeneities can arise due to filter cake patches and/or an inhomogeneous filter cloth itself. In this work a method is proposed that transforms the pressure drop profile of a filter into a permeability distribution (PD) of the filter medium, thus accounting for possible inhomogeneities of the medium. The determination of the PD is looked at as an inverse problem of an integral transformation. The method is applied to experimental filter pressure drop data of laboratory scale jet-pulse cleaned bag filter plants. It is found that even clean filter media can exhibit a significant permeability profile.     

Unified model for the prediction of consecutive solid–liquid filtration and expression at the constant pressure

Unified nonlinear model is proposed for the prediction of consecutive solid–liquid filtration and expression at the constant pressure. This model is based on the Darcy–Terzaghi filtration-consolidation equations modified to consider power-law pressure dependence of the specific cake resistance, and transforming Darcy law to the linear form. The model considers nonuniform structure of compressible filter cakes obtained by filtration and following expression. The profiles of local compressive pressure and local cake characteristics are simulated and compared for different moderately and highly compressible filter cakes (H.K. kaolin, CaCO₃, silica, activated sludge) based on the analytical and numerical solutions of the model. It is shown that the behavior of solid–liquid expression depends from the initial structure of compressed materials. Consolidation ratio U of the filter cakes with initially nonuniform structure formed by filtration differs from that of semi-solid materials with initially uniform structure. Different methods of determination of consolidation coefficient are analyzed and compared for nonuniformly structured filter cakes.     

节流前过冷度和压力对液氮节流特性的影响

节流在普冷领域应用广泛。其在基于林德循环、克劳德循环等低温液化循环、焦汤氦制冷系统、低温推进剂热力排气系统中也都有涉及。为了深入揭示低温流体相比室温气体的节流特殊性,设计并搭建了一套低温流体气液两相节流可视化试验系统。针对渐缩渐扩管型的节流元件,分析了节流前过冷度和压力对液氮节流特性的影响。研究表明：节流前压力一定,节流后温降及气相质量分数随节流前过冷度增加而增加;节流前过冷度一定,节流后温降及气相质量分数随节流前压力增大而增大;增大节流前压力,减小节流前过冷度,会减少节流后流体的单位质量制冷量。     

Filtration of solid and liquid aerosol mixtures: Pressure drop evolution and influence of solid/liquid ratio

Dust and droplet filtration is an essential process step in many industries. Although many studies have been dedicated to the mechanisms of dust filtration, little is known about the behaviour of an air filter when challenged with solid and liquid particles at the same time. This research article answers questions about the pressure drop during the filtration of a solid/liquid particle mixture, as well as on the influence of the respective solid and liquid particle concentrations.     

Low-temperature filtration of gases using multilayer cermet filters

The performance characteristics of highly efficient cermet filters with a multilayer membrane structure used for the treatment of nitrogen, argon, helium, methane, carbon monoxide and dioxide at temperatures up to 75 K are studied. It is shown that as the temperature decreases, their collection efficiency with respect to a finely dispersed aerosol decreases. At low Reynolds numbers, the variation of the gas-flow pressure drop through the filters is determined by the gas viscosity. The multilayer nickel-based membrane structure is stable to substantial temperature gradients and can be regenerated by blowing and heating. It is found that the filter collection efficiency for liquid gases is determined by the pore size of the fine-pore selective layer of the filters according to the sieving mechanism of collecting dispersed particles.     

液体燃料合成浆态反应器内部过滤的研究

在液体燃料合成浆态搅拌反应器中设置了以金属烧结板为过滤介质的内过滤器,实现固液分离。研究了压降、温度、搅拌转速、固含率、过滤介质孔径及颗粒粒径对过滤速率的影响。实验结果表明:在浆态反应器中进行内过滤可以得到澄清稳定的滤液;随着操作进行,滤饼厚度达到动态平衡,过滤速率最终趋于稳定;过滤速率随着压降、温度、过滤介质孔径、颗粒粒径的增大及搅拌转速、固含率的减小而增大。应用因次分析法建立过滤模型,通过麦夸特算法对实验数据进行最优拟合得到模型的参数值,统计检验以及模型计算值与实验值的比较表明该模型可靠。     

纤维素助滤剂的预敷过滤性能

对高黏度物料加入纤维素助滤剂的预敷过滤性能进行了研究,说明不同的预敷条件对预敷层的过滤性能会有很大影响。通过改变预敷压力和浓度,对纤维素滤饼层的过滤比阻、可压缩性系数和孔隙率进行了研究。实验表明,纤维素预敷层的比阻随压力增加而增加,随浓度增加而减小;孔隙率随压力增加而减小,随浓度增加而增加;可压缩性系数随浓度增加而增加。纤维素助滤剂为中等可压缩性物料,孔隙率大。研究结果可为高黏度物料用纤维素预敷过滤的工程应用提供参考。     

Design of a crossflow filtration system

This paper proposes design steps for a crossflow filtration system. The design s procedure is based primarily upon the particle size of the suspended matter, suction velocity, solid and liquid densities, liquid viscosity, filter cake thickness and the specific resistance of the filter cake. The critical shear stress is used to work out the design parameters such as axial velocity, pipe diameter or duct dimensions, filtration pressure and filtration area.     

金属丝网过滤器性能影响因素研究

对金属丝网过滤器性能的影响因素进行了综合分析,为过滤器的良好运行提供建议。在分析过滤机理的基础上,从过滤效率、压降、残余压降三个方面,分析了过滤器性能的影响因素,包括丝网结构、循环次数、过滤速度、流体浓度及温度、颗粒粒径、滤饼的可压缩性、最大允许压降、反吹压力等。结果表明,各因素之间互相影响,实际过滤过程中须综合考虑,以达到过滤器的预期性能。     

液力过滤与液力压密脱水的理论(Ⅱ)

将滤室固定不变的板框或箱式压滤机的操作过程分成滤饼过滤阶段和液力压密脱水阶段两个过程来研究。在滤饼过滤阶段 ,应用表面过滤机理 ,采用传统的鲁思过滤基本方程和平均过滤比阻的理论进行研究。在液力压密脱水阶段 ,应用达西定律建立了液力压密基本微分方程 ,根据研究得出滤饼渗透系数与孔隙率在压密脱水阶段的线性取代关系的结论 ;滤室固定的限制条件和物料平衡条件 ,推导出液力压密的脱水方程式。分析了影响液力压密脱水的时间因素和液力压密速率的各操作参数。建立了完整的液力过滤和压密脱水理论 ,为自动压滤机的设计提供了理论指导