SiC颗粒增强铝基复合材料的显微组织与力学性能

采用压铸浸渗法制备了体积分数为50%的SiC/Al-5.3Cu-0.8Mg-0.6Ag-0.5Mn耐热铝基复合材料.通过拉伸测试与组织观察,研究了高体积分数SiC颗粒增强对基体合金的显微组织与力学性能影响.结果表明,在基体Al-5.3Cu-0.8Mg-0.6Ag-0.5Mn合金中掺入高体积分数的SiC颗粒后,复合材料的时效硬化与拉伸性能得到了大幅度的提高,185 ℃峰时效处理后的抗拉强度从356 MPa增大到520 MPa.SiC/Al-5.3Cu-0.8Mg-0.6Ag-0.5Mn复合材料的组织致密,分布均匀,其断裂方式包括界面脱开、基体韧断和增强体开裂.高体积分数SiC颗粒的增强并不改变基体合金的时效析出过程,析出相由Ω相和少量θ＇相组成,但SiC颗粒与基体之间发生了界面反应,生成了纳米级的Al4C3化合物.     

SiC颗粒增强铝基复合材料的研究

研究讨论了用半固态搅拌铸造法制造SiCp／Al复合材料的制备工艺,并对所制得的复合材料进行了分析和性能测试。结果表明：用多层螺旋倾斜叶片搅拌棒对熔体适速搅拌,可增加SiCp的复合量,使SiCp与基体间浸润性良好,且分布较均匀。     

采用FSP制备新型非晶增强铝基复合材料的组织与性能

利用搅拌摩擦加工技术获得的新型非晶增强铝基复合材料,通过金相、扫描电镜、显微硬度及拉伸试验等对其显微组织结构及力学性能进行了试验和分析.试验结果表明,复合材料主要以层状结构组成,主要由母材和非晶带交替形成.复合材料显微硬度明显高于母材,并且复合材料的抗拉强度显著提高,当旋转速度达到750 r/min,抗拉强度达到最大值...     

SiC颗粒增强铝基复合材料物理及力学性能研究进展

SiC颗粒增强铝基复合材料既保持了金属特有的良好延展性、传热等特点,又具有陶瓷的耐高温性、耐磨损的要求。综述了SiC颗粒增强铝基复合材料的物理及力学性能,SiC颗粒增强铝基复合材料强化的物理模型主要有两种,即剪切滞后模型与Eshelby理论。     

搅拌摩擦成型对铝基复合材料性能影响

采用搅拌摩擦成型技术对铸造SiC颗粒增强铝基复合材料进行改性,从组织、力学性能和摩擦磨损性能方面进行对比分析。结果表明:搅拌摩擦成型技术能修复缺陷组织、细化晶粒,搅拌时的剪切力使得SiC颗粒被打碎并分散均匀,提高材料的力学性能,抗拉强度和屈服强度分别提高14%和16%;搅拌摩擦成型修复后材料摩擦系数的稳定性得到显著提高。     

纳米SiC颗粒增强AM60镁合金组织性能的研究

通过对纳米SiC颗粒的预处理,使用搅熔复合铸造工艺,制备了纳米SiC颗粒增强AM60铸造镁合金材料.研究了纳米SiC颗粒对镁合金的显微组织、力学性能和硬度等的影响.结果表明,在镁合金中添加纳米SiC颗粒能够细化其组织,提高材料的综合力学性能.当纳米SiC颗粒加入量(体积分数)为1.0%时,纳米颗粒增强AM60镁合金的抗拉强度、伸长率和硬度(HB)分别达到240 MPa、16.0%和53.9,较相同工艺下未加纳米颗粒的AM60分别提高了12.1%、40.3%和11.6%.同时对纳米SiC颗粒对镁合金的强化机理进行了探讨.     

搅拌摩擦加工制备镁基铝覆层材料的组织与性能

在采用多道次搅拌摩擦加工成功地在镁合金表面覆合一层铝层的基础上,利用光学显微镜、透射电子显微镜、扫描电子显微镜、能谱分析和电子万能材料试验机对界面组织、元素成分分布、界面结合力和断口形貌进行了分析,并分析了不同焊接速度对重叠区界面组织和性能的影响规律.结果表明,界面由N道次区、重叠区和N+1道次区组成,重叠区界面过渡层的厚度随着焊接速度的降低而增加.其过渡层由Al+Al₃Mg₂相和Mg+Al₁₂Mg₁₇相组成.重叠区界面的剪切力随着速度的降低而增加,断裂方式为塑性断裂.     

搅拌摩擦加工法制备铝基复合材料组织与性能研究

用搅拌摩擦加工法制备碳纳米管增强铝基复合材料,并对其组织及硬度进行了分析。结果表明:搅拌摩擦中心区晶粒尺寸与轴肩变形区相似,晶粒比较细小;搅拌摩擦区边界的晶粒组织发生了明显的塑性变形,晶粒被扭曲拉长。碳纳米管在搅拌摩擦中心区均匀分散,和基体结合良好。碳纳米管对基材有明显的强化作用,搅拌摩擦中心区硬度在55 HV左右,是纯铝的2倍。     

采用搅拌摩擦焊方法制备的非晶增强铝基复合材料的微观组织分析

利用金相、EDS、XRD及TEM试验等对采用源于搅拌摩擦焊方法的搅拌摩擦加工技术制备的非晶增强铝基复合材料的微观组织结构进行试验分析.结果表明,非晶增强体与基体5A06铝合金经过搅拌摩擦加工过程充分的搅拌作用,获得了层状混和组织结构.复合材料中存在大量的90~400 nm纳米级组织,主要由-αA l与-αA l非晶组织构成.纳米级组织的存在有助于复合材料性能的提高,而非晶结构的存在表明非晶增强体在搅拌摩擦加工过程中并未完全晶化.     

原位SiC颗粒增强MoSi2基复合材料的显微组织和力学性能

本文研究了原位SiC颗粒增强MoSi2基复合材料的组织结构和力学性能结果表明复合材料的组织为t-MoSi2基体上均匀分布β-SiC等轴颗粒,数量很少的球形小孔隙主要分布在SiC颗粒内,SiC颗粒尺寸为2-5μm.复合材料界面为直接的原子结合,无非晶层存在.复合材料的室温维氏硬度、断裂韧性、抗压强度及高温流变应力明显高于单一MoSi2,随着SiC体积分数的增加,维氏硬度、断裂韧性及高温流变应力提高,而抗压强度先增加后减少SiC体积分数从10%增加到45%,KIC从4.34提高到5.71 MPa     

Fabrication of Al/Al2Cu in situ nanocomposite via friction stir processing

The aim of present work is fabrication of Al/Al₂Cu in situ nanocomposite by friction stir processing (FSP) as well as investigation of FPS parameters such as rotational speed, travel speed, number of FSP passes, and pin profile on the microstructure, chemical reaction, and microhardness of Al based nanocomposite. The Al₂Cu particles were formed rapidly due to mechanically activated effect of FSP as well as high heat generation due to Al-Cu exothermic reaction. The microstructure of the nanocomposites consisted of a finer grained aluminium matrix (～15 µm), unreacted Cu nanoparticles (～40 nm), and reinforcement nanoparticles of Al₂Cu. Irregular morphology of Al₂Cu is attributed to the local melting during FSP. Pin diameter has a higher effect on the microstructure and hardness values. The hardness measurements exhibited enhancement by 57% compared with the base metal.     

Microstructure and wear performance of Al5083/CeO2/SiC mono and hybrid surface composites fabricated by friction stir processing

Friction stir processing (FSP) was utilized to produce surface composites by incorporating nano-sized cerium oxide (CeO₂) and silicon carbide (SiC) particles individually and in combined form into the Al5083 alloy matrix. The study signified the role of these reinforcements on microstructure and wear behavior of the resultant surface composite layers. The wear characteristics of the resultant mono and hybrid surface composite layers were investigated using a pin-on-disc wear tester at room temperature. The microstructural observations of FSPed regions and the worn out surfaces were performed by optical and scanning electron microscopy. Considerable grain refinement and uniform distribution of reinforcement particles were achieved inside the nugget zone. All the composite samples showed higher hardness and wear resistance compared to the base metal. Among the composite samples, the hybrid composite (Al5083/CeO₂/SiC) revealed the highest wear resistance and the lowest friction coefficient, whereas the Al5083/SiC composite exhibited the highest hardness, i.e., 1.5 times as hard as that of the Al5083 base metal. The enhancement in wear behavior of the hybrid composites was attributed to the solid lubrication effect provided by CeO₂ particles. The predominant wear mechanism was identified as severe adhesive in non-composite samples, which changed to abrasive wear and delamination in the presence of reinforcing particles.     

钛钢复合板搅拌摩擦焊接接头组织与力学性能

采用搅拌摩擦焊对接工艺焊接厚度为2 mm的TA2-Q235B钛钢复合板。采用光学显微镜和扫描电子显微镜观察焊接接头显微组织及断口形貌,并采用拉伸试验机和显微硬度计测试焊接接头力学性能及不同区域的显微硬度。结果表明,钛钢复合板焊接接头从上到下分为上部钢焊接区,中部钛钢混合区及下部钛焊接区3个区域,其中钛钢混合区呈交替层叠状结构。当轴肩旋转速度为300 r/min,焊接速度为40 mm/min时,焊接接头的抗拉强度为386 MPa,达到母材强度的80%以上,焊接区域的硬度平均值为243.5 HV,焊接接头断裂源于结合较弱的前进侧热机影响区域。     

亚共析钢搅拌摩擦加工组织与力学性能

采用K40钨钴硬质合金搅拌头对3 mm厚热轧退火态亚共析钢板进行了搅拌摩擦加工,对加工区域的宏观形貌、微观组织及力学性能进行了分析．结果表明,搅拌区和热力影响区为先共析块状铁素体、“针状”铁素体及珠光体,组织转变受动态再结晶和相变共同作用,热影响区组织为等轴状铁素体和片层状珠光体．搅拌摩擦加工对各区域中珠光体及析出渗碳体的分布形态影响显著．搅拌摩擦加工后试样显微硬度明显增加,抗拉强度相比母材提高8.2%,断裂位置位于母材处,加工前后试样断裂形式均为微孔聚合韧性断裂．固溶强化与相变强化对硬度和抗拉强度的提高起主要作用．     

搅拌速度对搅拌摩擦工艺制备的Cu/B4C表面复合材料显微组织和滑动磨损行为的影响（英文）

采用搅拌摩擦工艺合成Cu/B4C表面复合材料,并分析搅拌速度对该复合材料显微组织和滑动磨损行为的影响。搅拌速度以200 r/min从800变化至1200 r/min,横向速度、轴向力、沟槽宽度及搅拌头外形保持不变。采用光学和扫描电子显微镜对所制备表面复合材料的显微组织进行观察。采用销盘滑动磨损试验装置研究该表面复合材料的滑动磨损性能。结果表明:搅拌速度对表面材料的面积和B4C颗粒的分布具有显著影响。在较高的搅拌速度下此复合材料中B4C颗粒分布均匀;而在低搅拌速度下B4C颗粒分布均匀性较差。此外,本文报道搅拌速度对复合材料的颗粒尺寸、硬度、磨损率、磨损表面和磨屑的影响。     

Effect of second-phase particle size and presence of vibration on AZ91/SiC surface composite layer produced by FSP

An improved method of friction stir processing (FSP) was introduced for the processing of AZ91 magnesium alloy specimens. This novel process was called “friction stir vibration processing (FSVP)”. FSP and FSVP were utilized to develop surface composites on the studied alloy while SiC nanoparticles were applied as second-phase particles. The effect of reinforcing SiC particles with different sizes (30 and 300 nm) on different characteristics of the composite surface was studied. The results indicated that the microstructure was refined and mechanical properties such as hardness, ductility, and strength were enhanced as FSVP was applied. Furthermore, it was concluded that the effect of reinforcing particles with a size of 30 nm on the microstructure and mechanical properties of the surface composite was more obvious than that of particles with a size of 300 nm. It was also found that mechanical properties and microstructure of FSV-processed specimens were improved as vibration frequency increased. The hardness value in the stir zone was about 157 MPa for the FSV-processed specimen at a vibration frequency of 50 Hz, while this value was around 116 MPa for the FSV-processed specimen at a vibration frequency of 25 Hz.     

搅拌摩擦加工修复AA5083/T2紫铜爆炸复合板界面

基于多道次搅拌摩擦加工(M-FSP)修复AA5083/T2紫铜爆炸复合板的界面缺陷,探讨界面形貌和界面结合机制.结果表明,搅拌摩擦加工过程中的高旋转速度和低前进速度会产生更多的热量.当旋转速度设定在1200 r/min,前进速度设定在30 mm/min,搭边量设定在2/24时,AA5083/T2紫铜复合板经多道次搅拌摩...     

搅拌摩擦加工原位反应制备Al_3Ti-Al表面复合层

通过在铝合金1100-H14表面加工矩形凹槽并添加微米级钛粉再进行搅拌摩擦加工(friction stir processing,FSP)的方法,在铝合金表面获得Al3Ti-Al复合层.采用扫描电镜(SEM),能谱分析(EDS)以及X射线衍射(XRD)对表面复合层微观结构及相组成进行了分析,并对复合层的显微硬度进行了检测.结果表明,在FSP强烈的热、力耦合作用下,钛粉产生了碎化,破碎后的钛颗粒与铝产生快速原位反应,生成微米和亚微米级Al3Ti颗粒,残留的钛颗粒和细小的Al3Ti颗粒一同均匀地分布于铝合金基体中,从而使得铝合金表面的硬度得到提高,其平均值达到了71.39HV,为基体硬度的2.1倍.     

30 mm 7A05铝合金搅拌摩擦焊接头组织及力学性能

采用搅拌摩擦焊方法利用新型搅拌头对30 mm厚的7A05-T6铝合金进行了单道对接,焊后分析讨论了焊缝接头微观组织和力学性能.结果表明,接头焊核区发生动态再结晶,生成细小的等轴晶粒;焊缝两侧热力影响区受机械和热的双重作用,组织存在较大差异,前进侧为窄条状组织,后退侧为扁平状组织;热影响区晶粒粗化;在焊接30 mm板时,工艺参数范围较窄,旋转频率为360 r/min,焊接速度为100 mm/min时,可获得无缺陷、成形好的焊缝;接头抗拉强度为367.7 MPa、屈服强度为280.8 MPa、断后伸长率为14.4%高于母材,接头抗拉强度可达母材的95%.接头显微硬度的分布呈类似W形分布,热影响区软化趋势比较明显.